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Iwata, Keiko; Takamizawa, Hisashi; Ha, Yoosung; Shimodaira, Masaki; Okamoto, Yoshihiro; Honda, Mitsunori; Katsuyama, Jinya; Nishiyama, Yutaka
Nuclear Instruments and Methods in Physics Research B, 511, p.143 - 152, 2022/01
Times Cited Count:1 Percentile:33.4(Instruments & Instrumentation)Takamizawa, Hisashi; Hata, Kuniki; Nishiyama, Yutaka; Toyama, Takeshi*; Nagai, Yasuyoshi*
Journal of Nuclear Materials, 556, p.153203_1 - 153203_10, 2021/12
Times Cited Count:3 Percentile:31.78(Materials Science, Multidisciplinary)Solute clusters (SCs) formed in pressurized water reactor surveillance test specimens neutron-irradiated to a fluence of 1 10 n/cm were analyzed via atom probe tomography to understand the effect of silicon on solute clustering and irradiation embrittlement of reactor pressure vessel steels. In high-Cu bearing materials, Cu atoms were aggregated at the center of cluster surrounded by the Ni, Mn, and Si atoms like a core-shell structure. In low-Cu bearing materials, Ni, Mn, and Si atoms formed cluster and these solutes were not comprised core-shell structure in SCs. While the number of Cu atoms in clusters was decreased with decreasing nominal Cu content, the number of Si atoms had clearly increased. The cluster radius () and number density () decreased and increased, respectively, with increasing nominal Si content. The shift in the reference temperature for nil-ductility transition (RT) showed a good correlation with the square root of volume fraction () multiplied by r (). This suggested that the dislocation cutting through the particles mechanism dominates the precipitation hardening responsible for irradiation embrittlement. The negative relation between the nominal Si content and RT indicated that increasing of nominal Si content reduces the degree of embrittlement.
Takamizawa, Hisashi; Nishiyama, Yutaka
Journal of Pressure Vessel Technology, 143(5), p.051502_1 - 051502_8, 2021/10
Times Cited Count:3 Percentile:30.36(Engineering, Mechanical)no abstracts in English
Ha, Yoosung; Shimodaira, Masaki; Takamizawa, Hisashi; Tobita, Toru; Katsuyama, Jinya; Nishiyama, Yutaka
Proceedings of ASME 2021 Pressure Vessels and Piping Conference (PVP 2021) (Internet), 6 Pages, 2021/07
Iwata, Keiko; Hata, Kuniki; Tobita, Toru; Hirota, Takatoshi*; Takamizawa, Hisashi; Chimi, Yasuhiro; Nishiyama, Yutaka
Proceedings of ASME 2021 Pressure Vessels and Piping Conference (PVP 2021) (Internet), 7 Pages, 2021/07
Hata, Kuniki; Takamizawa, Hisashi; Hojo, Tomohiro*; Ebihara, Kenichi; Nishiyama, Yutaka; Nagai, Yasuyoshi*
Journal of Nuclear Materials, 543, p.152564_1 - 152564_10, 2021/01
Times Cited Count:12 Percentile:91.16(Materials Science, Multidisciplinary)Reactor pressure vessel (RPV) steels for pressurized water reactors (PWRs) with bulk P contents ranging from 0.007 to 0.012wt.% were subjected to neutron irradiation at fluences ranging from 0.3 to 1.210 n/cm (E 1 MeV) in PWRs or a materials testing reactor (MTR). Grain-boundary P segregation was analyzed using Auger electron spectroscopy (AES) on intergranular facets and found to increase with increasing neutron fluence. A rate theory model was also used to simulate the increase in grain-boundary P segregation for RPV steels with a bulk P content up to 0.020wt.%. The increase in grain-boundary P segregation in RPV steel with a bulk P content of 0.015wt.% (the maximum P concentration found in RPV steels used in Japanese nuclear power plants intended for restart) was estimated to be less than 0.1 in monolayer coverage at 1.010 n/cm (E 1 MeV). A comparison of the PWR data with the MTR data showed that neutron flux had no effect upon grain-boundary P segregation. The effects of grain-boundary P segregation upon changes in irradiation hardening and ductile-brittle transition temperature (DBTT) shifts were also discussed. A linear relationship between irradiation hardening and the DBTT shift with a slope of 0.63 obtained for RPV steels with a bulk P content up to 0.026wt.%, which is higher than that of most U.S. A533B steels. It is concluded that the intergranular embrittlement is unlikely to occur for RPV steels irradiated in PWRs.
Suzudo, Tomoaki; Takamizawa, Hisashi; Nishiyama, Yutaka; Caro, A.*; Toyama, Takeshi*; Nagai, Yasuyoshi*
Journal of Nuclear Materials, 540, p.152306_1 - 152306_10, 2020/11
Times Cited Count:9 Percentile:75.92(Materials Science, Multidisciplinary)Spinodal decomposition in thermally aged Fe-Cr alloys leads to significant hardening, which is the direct cause of the so-called 475C-embrittlement. To illustrate how spinodal decomposition induces hardening by atomistic interactions, we conducted a series of numerical simulations as well as reference experiments. The numerical results indicated that the hardness scales linearly with the short-range order (SRO) parameter, while the experimental result reproduced this relationship within statistical error. Both seemingly suggest that neighboring Cr-Cr atomic pairs essentially cause hardening, because SRO is by definition uniquely dependent on the appearance probability of such pairs. A further numerical investigation supported this notion, as it suggests that the dominant cause of hardening is the pinning effect of dislocations passing over such Cr-Cr pairs.
Takamizawa, Hisashi; Nishiyama, Yutaka; Hirano, Takashi*
Proceedings of ASME 2020 Pressure Vessels and Piping Conference (PVP 2020) (Internet), 7 Pages, 2020/08
no abstracts in English
Ha, Yoosung; Takamizawa, Hisashi; Katsuyama, Jinya; Hanawa, Satoshi; Nishiyama, Yutaka
Nuclear Instruments and Methods in Physics Research B, 461, p.276 - 282, 2019/12
Times Cited Count:4 Percentile:32.64(Instruments & Instrumentation)Takamizawa, Hisashi; Katsuyama, Jinya; Ha, Yoosung; Tobita, Toru; Nishiyama, Yutaka; Onizawa, Kunio
Proceedings of 2019 ASME Pressure Vessels and Piping Conference (PVP 2019) (Internet), 8 Pages, 2019/07
no abstracts in English
Tobita, Toru; Nishiyama, Yutaka; Onizawa, Kunio
JAEA-Data/Code 2018-013, 60 Pages, 2018/11
Mechanical properties of materials including fracture toughness are extremely important for evaluating the structural integrity of reactor pressure vessels (RPVs). In this report, the published data of mechanical properties of nuclear RPVs steels, including neutron irradiated materials, acquired by the Japan Atomic Energy Agency (JAEA), specifically tensile test data, Charpy impact test data, drop-weight test data, and fracture toughness test data, are summarized. There are five types of RPVs steels with different toughness levels equivalent to JIS SQV2A (ASTM A533B Class 1) containing impurities in the range corresponding to the early plant to the latest plant. In addition to the base material of RPVs, the mechanical property data of the two types of stainless overlay cladding materials used as the lining of the RPV are summarized as well. These mechanical property data are organized graphically for each material and listed in tabular form to facilitate easy utilization of data.
Ha, Yoosung; Tobita, Toru; Otsu, Takuyo; Takamizawa, Hisashi; Nishiyama, Yutaka
Journal of Pressure Vessel Technology, 140(5), p.051402_1 - 051402_6, 2018/10
Times Cited Count:6 Percentile:32.89(Engineering, Mechanical)Ha, Yoosung; Tobita, Toru; Takamizawa, Hisashi; Hanawa, Satoshi; Nishiyama, Yutaka
Proceedings of 2018 ASME Pressure Vessels and Piping Conference (PVP 2018), 6 Pages, 2018/07
Chimi, Yasuhiro; Iwata, Keiko; Tobita, Toru; Otsu, Takuyo; Takamizawa, Hisashi; Yoshimoto, Kentaro*; Murakami, Takeshi*; Hanawa, Satoshi; Nishiyama, Yutaka
JAEA-Research 2017-018, 122 Pages, 2018/03
Warm pre-stress (WPS) effect is a phenomenon that after applying a load at a high temperature fracture does not occur in unloading during cooling, and then the fracture toughness in reloading at a lower temperature increases effectively. Engineering evaluation models to predict an apparent fracture toughness in reloading are established using experimental data with linear elasticity. However, there is a lack of data on the WPS effect for the effects of specimen size and surface crack in elastic-plastic regime. In this study, fracture toughness tests were performed after applying load-temperature histories which simulate pressurized thermal shock transients to confirm the WPS effect. The experimental results of an apparent fracture toughness tend to be lower than the predictive results using the engineering evaluation models in the case of a high degree of plastic deformation in preloading. Considering the plastic component of preloading can refine the engineering evaluation models.
Iwata, Keiko; Takamizawa, Hisashi; Ha, Yoosung; Okamoto, Yoshihiro; Shimoyama, Iwao; Honda, Mitsunori; Hanawa, Satoshi; Nishiyama, Yutaka
Photon Factory Activity Report 2017, 2 Pages, 2018/00
no abstracts in English
Chimi, Yasuhiro; Kasahara, Shigeki; Seto, Hitoshi*; Kitsunai, Yuji*; Koshiishi, Masato*; Nishiyama, Yutaka
Proceedings of the 18th International Conference on Environmental Degradation of Materials in Nuclear Power Systems - Water Reactors, Vol.2, p.1039 - 1054, 2018/00
Times Cited Count:2 Percentile:58(Materials Science, Multidisciplinary)In order to understand irradiation-assisted stress corrosion cracking (IASCC) growth behavior, crack growth rate (CGR) tests have been performed in simulated Boiling Water Reactor water conditions at 288C on neutron-irradiated 316L stainless steels (SSs) at 12-14 dpa. After the tests, the microstructures near the crack tip of the specimens are examined with scanning transmission electron microscope (FE-STEM). In comparison with a previous study at 2 dpa, this result shows a less benefit of low electrochemical corrosion potential (ECP) conditions on CGR. A crack tip immersed over 1000 hours was filled with oxides, while almost no oxide film was observed near the crack front in the low-ECP conditions. In addition, a high density of deformation twins and dislocations were found near the fracture surface of the crack front. It is considered that both localized deformation and oxidation are possible dominant factors for the SCC growth in highly irradiated SSs.
Ha, Yoosung; Tobita, Toru; Takamizawa, Hisashi; Nishiyama, Yutaka
Proceedings of 2017 ASME Pressure Vessels and Piping Conference (PVP 2017) (CD-ROM), 5 Pages, 2017/07
The applicability of miniature-C(T) (Mini-C(T)) specimens to fracture toughness evaluation was investigated for neutron-irradiated reactor pressure vessel (RPV) steel. value determined from irradiated Mini-C(T) specimens was in good agreement with that determined from the irradiated pre-cracked Charpy-type (PCCv) specimens. Also, the scatter of the 1T-equivalent fracture toughness values obtained from the irradiated Mini-C(T) specimens was not significantly different from that obtained from the irradiated PCCv. values determined from Mini-C(T) specimens agreed very well with the correlation between Charpy 41J transition temperature and of commercially manufactured RPV steels.
Kasahara, Shigeki; Kitsunai, Yuji*; Chimi, Yasuhiro; Chatani, Kazuhiro*; Koshiishi, Masato*; Nishiyama, Yutaka
Journal of Nuclear Materials, 480, p.386 - 392, 2016/11
Times Cited Count:0 Percentile:0.01(Materials Science, Multidisciplinary)This paper addresses influence of two different temperature profiles during startup periods in the Japan Materials Testing Reactor and a boiling water reactor upon microstructural evolution and mechanical properties of austenitic stainless steel irradiated with neutrons to about 1 dpa and 3 dpa. Tensile tests at 290C and Vickers hardness tests at room temperature were carried out, and their microstructures were observed by FEG-TEM. Influence of difference in the temperature profiles was observed obviously in interstitial cluster formation, in particular, growth of Frank loops. The influence was also found certainly in loss of strain hardening capacity and ductility, although the influence on the yield strength and the Vickers hardness was not clearly observed. As a result, Frank loops, which were observed in austenitic stainless steel irradiated at doses of 1 dpa or more, were considered to contribute to deformation of the austenitic stainless steel.
Takamizawa, Hisashi; Ito, Hiroto; Nishiyama, Yutaka
Journal of Nuclear Materials, 479, p.533 - 541, 2016/10
Times Cited Count:6 Percentile:49.29(Materials Science, Multidisciplinary)To understand neutron irradiation embrittlement in high fluence regions, statistical analysis using the Bayesian nonparametric (BNP) method was performed for the Japanese surveillance and material test reactor irradiation database. The BNP method is essentially expressed as an infinite summation of normal distributions, with input data being subdivided into clusters with identical statistical parameters (such as mean and standard deviation) for each cluster to estimate shifts in ductile-to-brittle transition temperature (DBTT). Clusters typically depend on chemical compositions, irradiation conditions, and the irradiation embrittlement. Specific variables contributing to the irradiation embrittlement include the content of Cu, Ni, P, Si, and Mn in the pressure vessel, neutron flux, neutron fluence, and irradiation temperatures. It was found through numerous examinations that the measured shifts of DBTT correlated well with calculated ones. Data associated with the same materials were subdivided into the same clusters even if neutron fluences were significantly disparate among the results. This indicates that slowly developing or late-onset embrittlement mechanisms were not evident in the present study.
Chimi, Yasuhiro; Takamizawa, Hisashi; Kasahara, Shigeki*; Iwata, Keiko; Nishiyama, Yutaka
Nuclear Engineering and Design, 307, p.411 - 417, 2016/10
Times Cited Count:0 Percentile:0.01(Nuclear Science & Technology)To investigate influential parameters for irradiation-assisted stress corrosion cracking (IASCC) growth behavior, we attempt to analyze statistically existing data on the crack growth rate (CGR) in irradiated austenitic stainless steels (SSs) in boiling water reactor (BWR) environments using the Bayesian nonparametric (BNP) method. From the probability distribution of CGR and some input parameters, such as yield stress of irradiated material (), stress intensity factor (), electrochemical corrosion potential (ECP), and fast neutron fluence, the mean CGR is estimated and compared with the measured CGR. The analytical results show good reproducibility of the measured CGR. The results also indicate the possible neutron fluence effects on CGR in high CGR region (i.e., high neutron fluence condition) by radiation-induced segregation (RIS), localized deformation, and/or other mechanisms than radiation hardening.