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Journal Articles

New measurement system based on small-angle neutron scattering for structural analysis of light-responsive materials

Iwase, Hiroki*; Akamatsu, Masaaki*; Inamura, Yasuhiro; Sakaguchi, Yoshifumi*; Morikawa, Toshiaki*; Kasai, Satoshi*; Ouchi, Keiichi*; Kobayashi, Kazuki*; Sakai, Hideki*

Journal of Applied Crystallography, 56(1), p.110 - 115, 2023/02

 Times Cited Count:2 Percentile:85.44(Chemistry, Multidisciplinary)

With the increasing importance of light-responsive materials, it is vital to analyze the relationship between function and structural changes induced by light irradiation. Small-angle scattering (SAS) is effective for such structural analysis. However, quantitatively capturing local molecular structure formation and molecular reactions at a scale of less than 1 nm via SAS is difficult. In this study, to analyze the structure of non-equilibrium phenomena in light-responsive materials, a new sample environment has been developed for a time-of-flight small- and wide-angle neutron scattering instrument (TAIKAN), comprising a UV-Vis irradiation system, UV-Vis absorption measurement equipment and photodetector. Simultaneous measurement of small-angle neutron scattering and UV-Vis absorption was achieved. This system was used to demonstrate the in situ observation of UV-Vis irradiation-induced structural change of micelles formed by a light-responsive surfactant sample in an aqueous solution.

Journal Articles

Sample environment at the J-PARC MLF

Kawamura, Seiko; Oku, Takayuki; Watanabe, Masao; Takahashi, Ryuta; Munakata, Koji*; Takata, Shinichi; Sakaguchi, Yoshifumi*; Ishikado, Motoyuki*; Ouchi, Keiichi*; Hattori, Takanori; et al.

Journal of Neutron Research, 19(1-2), p.15 - 22, 2017/11

Sample environment (SE) team at the Materials and Life Science Experimental Facility (MLF) in J-PARC has worked on development and operation of SE equipment and devices. All the members belong to one sub-team at least, such as Cryogenic and magnet, High temperature, High pressure, Soft matter and special environment including Pulse magnet, Hydrogen environment, Light irradiation and $$^3$$He spin filter. Cryostats, a magnet, furnaces, a VX-6-type Paris-Edinburgh press and a prototype of a Spin-Exchange Optical Pumping (SEOP) based $$^3$$He spin filter for polarized neutron beam experiments are in operation. Furthermore, a prototype of compact power supply for a pulsed magnet system is currently developed. In the J-PARC Research Building, several pieces of equipment for softmatter research such as a rheometer and a gas and vapor adsorption measurement instrument have been prepared.

JAEA Reports

Development of reconstitution technique of irradiated specimen; Progress report for FY1993 on cooperated research between JAERI and IHI

Onizawa, Kunio; Fukaya, Kiyoshi; Nishiyama, Yutaka; Suzuki, Masahide; Shibata, Katsuyuki; Kosaka, Atsuo; *; *; *; *; et al.

JAERI-Tech 94-017, 58 Pages, 1994/09

JAERI-Tech-94-017.pdf:2.74MB

no abstracts in English

Journal Articles

Fatigue evaluation of the JT-60 vacuum vessel under the dynamic electromagnetic forces

; ; ; *; *; *

Nucl.Eng.Des., 74(3), p.325 - 337, 1982/00

 Times Cited Count:0 Percentile:0.02(Nuclear Science & Technology)

no abstracts in English

Oral presentation

Current status and plan of the beamline common sample environment at J-PARC MLF

Oku, Takayuki; Watanabe, Masao; Kawamura, Seiko; Aso, Tomokazu; Takahashi, Ryuta*; Sakai, Kenji; Yamauchi, Yasuhiro*; Nakamura, Masatoshi*; Munakata, Koji*; Ishikado, Motoyuki*; et al.

no journal, , 

Sample environment (SE) team is organized at the MLF of the J-PARC. SE equipment are prepared and the users are supported by the SE team. SE team consists of sub-team of (1) low temperature & magnetic field, (2) high temperature, (3) high pressure, (4) soft matter, (5) pulsed magnet, (6) light irradiation, (7) $$^{3}$$He spin filter. In this presentation, we will present the current status of the sample environmental equipment, the future plan and the support activities for users.

Oral presentation

Current status and plan of the common sample environment equipment

Watanabe, Masao; Oku, Takayuki; Kawamura, Seiko; Takata, Shinichi; Takahashi, Ryuta*; Sakai, Kenji; Yamauchi, Yasuhiro*; Nakamura, Masatoshi*; Munakata, Koji*; Ishikado, Motoyuki*; et al.

no journal, , 

Sample environment (SE) team is organized at the MLF of the J-PARC. SE equipment are prepared and the users are supported by the SE team. BL Common SE equipment includes (1) not frequently used but essential equipment, (2) very expensive equipment, (3) equipment that requires specialized knowledge and skills. SE team consists of sub-team of (1) low temperature & magnetic field, (2) high temperature, (3) high pressure, (4) soft matter, (5) pulsed magnet, (6) light irradiation, (7) $$^{3}$$He spin filter. In this presentation, we will present the current status of the sample environmental equipment, the future plan and the support activities for users.

Oral presentation

Sample environment at J-PARC MLF

Oku, Takayuki; Watanabe, Masao; Sakaguchi, Yoshifumi*; Kawamura, Seiko; Takahashi, Ryuta*; Yamauchi, Yasuhiro*; Nakamura, Masatoshi*; Ishikado, Motoyuki*; Ouchi, Keiichi*; Arima, Hiroshi*; et al.

no journal, , 

Sample environment team at the Materials and Life Science Experimental Facility in J-PARC has worked on development and operation of cryogenics, magnets, high temperature, high pressure, soft matter related items and special environment including pulsed magnets, light irradiators and He-3 spin filters. In the talk, our status is presented, and issues are addressed.

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