Validation of measured microwave absorption and temperature change for development of a single-mode-type microwave heating thermogravimetry apparatus

Karisma, A. D.*; Hamaba, Taishu*; Fukasawa, Tomonori*; Huang, A.-N.*; Segawa, Tomoomi; Fukui, Kunihiro*

Review of Scientific Instruments, 88(2), p.024101_1 - 024101_8, 2017/02

https://doi.org/10.1063/1.4974813

Microwave heating direct denitration method is used in the nuclear fuel reprocessing process. In order to develop a single-mode-type microwave heating thermogravimetry apparatus which can perform detailed analysis of the characteristics of microwave heating, the temperature dependence of microwave absorption is verified. The temperature distribution, microwave absorption efficiency, and dielectric properties of a CuO pellet that was heated by the microwave irradiation were investigated. The temperature distribution in the CuO pellet due to one-way travel of the microwave in the apparatus was accurately reproduced by a three-dimensional numerical simulation of the electromagnetic field. The numerically determined temperature dependency of the CuO absorption efficiency was found to be in very good agreement with published data.