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Otsuki, Ryusei*; Nasu, Shoichi*; Fujimori, Ryosuke*; Anada, Kinji*; Ohashi, Kentaro*; Yamamoto, Ryoichi*; Fujii, Kimio; Okubo, Keisuke*
Funtai Oyobi Fummatsu Yakin, 51(8), p.622 - 625, 2004/08
Effects of carbon materials on weight yield of (C
+C
) and weight ratios of C to (C+C) in soot were examined by the Joule resistive heating of four kinds of carbon materials at He gas pressures from 0.7
10
8.010Pa for collector radii of 45, 50 and 55mm. The yields were in the range of 1 to 8% for graphite with hexagonal lattice, and better than those for glassy carbon. The most effective He gas pressure for the fullerene yield were in the range of 4.05.310Pa. Any collector radii dependence of the yields was not observed. The weight ratios of C to (C+C) were about 60 to 70%, and showed neither He gas pressure depenndennce nor collector radii depenndence four kinds of carbon materials.
Otsuki, Ryusei*; Nasu, Shoichi*; Ohashi, Kentaro*; Yamamoto, Ryoichi*; Fujii, Kimio; Okubo, Keisuke*
Funtai Oyobi Fummatsu Yakin, 51(8), p.626 - 629, 2004/08
The He, Ar and the Penning gas pressureeffects on the preparation yieldsof the fullerenes were investigated by means of the arc discharge method using graphite(PGX) anode buried in a tungsten rod and tungsten cathode for collector radii of 50mm. The maximum yield showed about 13-14 % at 67KPa in He gas. The yields in the mixtures of He and Ne gases (the Penning effect) were similar to those obtained in He gas. Weight ratios of C to (C+C) were about 20% in Ar gas, while those in He and Penning gas were about 60%. Ultra sonic vibration was effective to separate C from soot.
Otsuki, Ryusei*; Nasu, Shoichi*; Matsushita, Masaki*; Fujii, Kimio; Ohashi, Kentaro*; Yamamoto, Ryoichi*
Funtai Oyobi Fummatsu Yakin, 51(8), p.633 - 634, 2004/08
We examined effects of deposition temperatures and collector radii onthe yields of fullerenes by arc discharge. Yields of fullerenes were 7-10%, 4-6% and 0.5-1% in the liquid nitrogen-cooling, water-cooling, non-cooling, respectively, and were better with a collector radius of 50mm than with that of 30mm. The weight ratios of C/C are about one for all runs of experiments.
