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Ishikado, Motoyuki; Shamoto, Shinichi; Kito, Hijiri*; Iyo, Akira*; Eisaki, Hiroshi*; Ito, Toshimitsu*; Tomioka, Yasuhide*
Physica C, 470(Suppl.1), p.S322 - S323, 2010/12
Times Cited Count:3 Percentile:17.17(Physics, Applied)Single crystals of oxygen deficient oxypnictide superconductor PrFeAsO have been grown by using belt-type anvil high pressure synthesis apparatus. Superconducting transition temperature () of the obtained single crystal is 45 K, and typical size is about 800 1000 30 . In-plane electrical resistivity shows almost proportional to temperature as well as the copper oxide high temperature superconductors, suggesting the existence of effects of strong inelastic scattering like copper oxide high temperature superconductor. In addition, we obtained non-superconducting parent single crystal by annealing the as-grown single crystal under ambient pressure. Resistivity of parent single crystal is characterized by the kink near 150 K corresponding to the structural transition, and the structure near 12 K, which is thought to be originating from the magnetic order of Pr ion.
Ishida, Shigeyuki*; Nakajima, Masamichi*; Tomioka, Yasuhide*; Ito, Toshimitsu*; Miyazawa, Kiichi*; Kito, Hijiri*; Lee, C.-H.*; Ishikado, Motoyuki; Shamoto, Shinichi; Iyo, Akira*; et al.
Physical Review B, 81(9), p.094515_1 - 094515_6, 2010/03
Times Cited Count:21 Percentile:64.67(Materials Science, Multidisciplinary)Characteristic normal-state charge transport is found in the oxygen-deficient iron-arsenides FeAsO (: La and Nd) with the highest 's among known Fe-based superconductors. The effect of "doping" in this system is mainly on the carrier scattering, quite distinct from that in high- cuprates. In the superconducting regime of the La system with maximum = 28 K, the low-temperature resistivity is dominated by a term. On the other hand, in the Nd system with higher than 40 K, the carriers are subject to stronger scattering showing -linear resistivity and small magnetoresistance. Such strong scattering appears crucial for high- superconductivity in the iron-based system.
Ishikado, Motoyuki; Shamoto, Shinichi; Kito, Hijiri*; Iyo, Akira*; Eisaki, Hiroshi*; Ito, Toshimitsu*; Tomioka, Yasuhide*
Physica C, 469(15-20), p.901 - 904, 2009/10
Times Cited Count:23 Percentile:66.35(Physics, Applied)We have successfully grown single crystals of oxygen deficient oxypnictide superconductor PrFeAsO by belt-type anvil apparatus using high pressure synthesis method.
Shirage, P. M.*; Miyazawa, Kiichi*; Ishikado, Motoyuki; Kiho, Kunihiro*; Lee, C.-H.*; Takeshita, Nao*; Matsuhata, Hirofumi*; Kumai, Reiji*; Tomioka, Yasuhide*; Ito, Toshimitsu*; et al.
Physica C, 469(9-12), p.355 - 369, 2009/06
Times Cited Count:40 Percentile:79.94(Physics, Applied)We have utilized a high-pressure (HP) technique to synthesize a series of newly-discovered iron (nickel)-based superconductors. The effect of (O)-deficiency, variation of ions, and the external pressure on are examined. All the experimental data indicate strong correlation between the crystal structure and the superconductivity of the oxypnictide superconductors. Upper critical field measurement on single crystalline sample of PrFeAsO shows the superconducting anisotropy of 5, which is smaller than cuprates. We also demonstrate that HP technique is applicable for the so-called "122" systems.
Fernandez-Baca, J. A.*; Dai, P.*; Wakabayashi, Nobuyoshi*; Plummer, E. W.*; Katano, Susumu; Tomioka, Yasuhide*; Tokura, Yoshinori*
Journal of the Physical Society of Japan, Vol.70, Supplement A, p.85 - 87, 2001/00
no abstracts in English
Ishikado, Motoyuki; Shamoto, Shinichi; Kito, Hijiri*; Iyo, Akira*; Eisaki, Hiroshi*; Ito, Toshimitsu*; Tomioka, Yasuhide*
no journal, ,
Single crystals of oxygen deficient oxypnictide superconductor PrFeAsO were grown by high pressure method using belt-type anvil apparatus. Grown crystals have shiny ab-plane surfaces. Typical crystal size is about 800100020 mm, which is one order larger than the previous reported LnFeAs(O,F) single crystal size. Upper critical field obtained from resistivity measurement under magnetic field yields anisotropy of 5, which is consistent with other group's reported result. In the session, we will talk details of the method of doping control of the single crystal and doping dependences of anisotropy.
Ishikado, Motoyuki; Shamoto, Shinichi; Kito, Hijiri*; Iyo, Akira*; Eisaki, Hiroshi*; Ito, Toshimitsu*; Tomioka, Yasuhide*
no journal, ,
In the previous meeting, we have grown single crystals of oxygen deficient oxypnictide high temperature superconductor PrFeAsO, and characterized anisotropy from resistivity under magnetic field. Anisotropy of upper critical field (H) is 5 and is consistent with other group's reported value. In this study, we succeeded to control doping by adjusting the oxygen content. We measured resistivity under magnetic field and estimated anisotropy of the doping controled single crystals, and revealed that anisotropy is not doping dependent. In the session, we report details of doping control, characterization such as resistivity and XRD, estimation of anisotropy.
Ishikado, Motoyuki; Shamoto, Shinichi; Kito, Hijiri*; Iyo, Akira*; Eisaki, Hiroshi*; Tomioka, Yasuhide*; Ito, Toshimitsu*
no journal, ,
Since the discovery of iron-based superconductor, extensive research have been done in order to clarify mechanism of superconductivity. But the research have been done mainly on 122 system because of easy availability of single crystal. So far, we have succeeded to grow single crystals of PrFeAsO high-Tc superconductor by high-pressure synthesis method. In the previous talk, we succeeded to control doping by tuning oxygen content of the single crystals, and characterized anisotropy by resistivity measurement under magnetic field. And reported that the anisotropy of iron-based superconductor dose not depend on doping different from cuprates. This time, we measure transport properties, especially for doping dependences of Hall coefficient, and discuss relationship between Hall coefficient and SDW transition on underdoping regime.