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Mo adsorption and 
Tc elution from zirconium-based material in Mo/Tc generator column using neutron-irradiated natural molybdenumAwaludin, R.*; Gunawan, A. H.*; Lubis, H.*; Sriyono*; Herlina*; Mutalib, A.*; Kimura, Akihiro; Tsuchiya, Kunihiko; Tanase, Masakazu*; Ishihara, Masahiro
Journal of Radioanalytical and Nuclear Chemistry, 303(2), p.1481 - 1483, 2015/02
Times Cited Count：9 Percentile：60.64(Chemistry, Analytical)In this study, the Mo adsorption and Tc elution mechanism were investigated using SEM-EDS to analyze the elemental composition of the material surfaces before Mo adsorption, after Mo adsorption and after Tc elution using saline solution. The results were compared with the value of adsorption capacity of the material to irradiated natural Mo and elution yield of Tc. From the changes of elemental composition in the surface, it was found that molybdate ions were adsorbed into the adsorbent by ion exchange with Cl
ion in the material. On the other hand, it was also revealed that Tc can be eluted from the material column in TcO
since oxidizing agent was needed in the elution process.
Tc production from (n,
)Mo based on solvent extraction and column chromatographyKimura, Akihiro; Awaludin, R.*; Shiina, Takayuki*; Tanase, Masakazu*; Kawauchi, Yukimasa*; Gunawan, A. H.*; Lubis, H.*; Sriyono*; Ota, Akio*; Genka, Tsuguo; et al.
Proceedings of 6th International Symposium on Material Testing Reactors (ISMTR-6) (Internet), 7 Pages, 2013/10
JP, 2011-173260
Patent publication (In Japanese)
This research is development of Tc production. Tc is generated by decay of Mo. The supply of Mo in Japan depends entirely on the import from foreign countries. Thus, it is needed to supply Mo stably by the domestic manufacturing. A practical production of Tc was tried by the method with 1 Ci of Mo produced in MPR-30. The results showed that the recovery yields were approximately 70%. The concentration of the product obtained was estimated to be corresponding to about 30 GBq (800 mCi)/ml when 150g of MoO
was irradiated for 5 days in MPR-30. Impurity of Mo was less than 4.4
10
%, which was lower than that of Japanese tentative regulation criteria. The radiochemical purity was higher than 99.8% that cleared the tentative regulation (95%) of Japan.
Sasaki, Michiya*; Yamada, Ryohei; Akata, Naofumi*; Tokonami, Shinji*; Hosoda, Masahiro*; Iwaoka, Kazuki*; Chanis, P.*; Kudo, Hiromi*; Sahoo, K.*; Iskandar, D.*; et al.
no journal, ,
Recently, Mamuju city in Sulawesi Island, Indonesia and its surrounding area is known as the high background radiation area, and is regarded as a possible area for an epidemiological study. In this study we have measured the hourly dose rates of individuals and the environment with the D-shuttle dosimeter, which has been developed by the Chiyoda Technol Corporation. With the aid of local residents living at Botteng village, which is located south of Mamuju city, short term and long term measurements were conducted for three days and nine months, respectively. Two volunteers have equipped the D-shuttle for the short term measurement, and seven families supported the short and long term measurements of the environmental dose rate, for both inside and outside the house. From our results, since some variation was observed regarding with day or night, correlation with radon concentration was suggested.
