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Influence of Zn injection on PWSCC crack growth rates and oxide film properties of Alloy 600

600合金のPWSCC亀裂進展速度及び酸化皮膜特性に及ぼす亜鉛注入の影響

知見 康弘; 佐藤 賢二*; 笠原 茂樹; 梅原 隆司*; 塙 悟史

Chimi, Yasuhiro; Sato, Kenji*; Kasahara, Shigeki; Umehara, Ryuji*; Hanawa, Satoshi

一次系冷却水中での応力腐食割れ(PWSCC)進展挙動への亜鉛注入の影響を調べるため、加圧水型軽水炉(PWR)一次系水模擬環境での10%冷間加工600合金の亀裂進展試験を、320$$^{circ}$$C、低濃度(5$$sim$$10ppb)の亜鉛注入、溶存水素濃度(DH)5, 30、及び50cc/kgH$$_{2}$$Oの条件下で実施した。その結果、亀裂進展速度のDH依存性が亜鉛注入なしの試験データに基づく亀裂進展速度の予測値と同様の傾向を示し、実機環境を模擬した低濃度亜鉛注入が亀裂進展挙動に及ぼす影響はほとんど見られなかった。そこで、亀裂進展試験後の試験片の亀裂内及び表面に生成した酸化皮膜の微細組織分析を実施したところ、試験片表面の酸化皮膜からは亜鉛が検出されたが、亀裂内に生成した酸化皮膜からは亜鉛が検出されなかった。このことから、亀裂先端部の酸化皮膜への亜鉛の取り込みがないことが亀裂進展挙動への亜鉛注入の影響が見られない原因であることがわかった。

To investigate the influence of Zinc (Zn) injection on primary water stress corrosion cracking (PWSCC) growth behavior, crack growth tests of 10% cold-worked Alloy 600 were performed in simulated primary water environment of pressurized water reactor (PWR) at 320$$^{circ}$$C with a low-concentration (5-10 ppb) Zn injection under dissolved hydrogen (DH) conditions of 5, 30, and 50 cc/kgH$$_{2}$$O. As a result of the crack growth tests, DH-dependence of crack growth rate (CGR) showed a similar tendency to the predicted CGR based on the CGR data without Zn injection, indicating almost no effect of a low-concentration Zn injection on the crack growth behavior. Moreover, the microstructural analyses of oxide films formed inside the crack and on the specimen surface were conducted, and the intake of Zn in the oxides was detected on the specimen surface, but not detected inside the crack. This result was considered to be the cause of no Zn injection effect on the crack growth behavior.

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