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Development of analytical method for Sr-90 using ICP-MS; Aim for Sr-90 measurement for otolith

Koarai, Kazuma   ; Matsueda, Makoto   ; Aoki, Jo; Yanagisawa, Kayo*; Terashima, Motoki  ; Fujiwara, Kenso ; Kino, Yasushi*; Oka, Toshitaka   ; Takahashi, Atsushi*; Suzuki, Toshihiko*; Shimizu, Yoshinaka*; Chiba, Mirei*; Osaka, Ken*; Sasaki, Keiichi*; Sekine, Tsutomu*; Fukumoto, Manabu*; Shinoda, Hisashi*; Kitamura, Akihiro   ; Abe, Hironobu 

Rapid analysis of $$^{90}$$Sr in bone and tooth samples of cattle were achieved by an inductively coupled plasma mass spectrometry (ICP-MS) coupled with mass shift and solid phase extraction techniques. Limit of detection (LOD) in the ICP-MS measurement of 0.1 g samples was lower than that of the radioactivity measurement. Analytical time of the ICP-MS method was reduced from 20 days to 11 hours, compared with the radiometric method. The ICP-MS method was improved by ICP-MS/MS and oxygen-ammonia mixed gas reaction.

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