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JAEA Reports

Cleaning of the inner surface for Separated-type Drift Tube Linac with Dilute Hydrochloric Acid

Arai, Sora; Kosaka, Satoshi*; Nemoto, Yasuo*; Kitamura, Ryo

JAEA-Technology 2023-009, 18 Pages, 2023/05

JAEA-Technology-2023-009.pdf:1.89MB

The linac located at the head of the J-PARC accelerators and required to provide the stable and high-quality beam. One of the accelerating cavities in the linac is the Separated-type Drift Tube Linac (SDTL). It is important to appropriately apply the RF power into the cavity for the stable operation. However, after the recovery from the Great East Japan Earthquake, the RF power could not be applied into the cavities for several SDTL cavities because the voltage standing wave ratio increased around the designed operating power. The investigation revealed that the inner surface of the cavity was exposed to high humidity and the backflow of oil from the rotary pump for a long period of time after the earthquake. It was suggested that the residue on the inner surface caused the multipactor resulted in the failure when the power was applied. The residue was wiped out with organic solvents and acids, resulted in solving the failure. This report describes the method and results of the cleaning for the cavity in 2021.

JAEA Reports

How to confirm the polarity of the DTQ in the J-PARC DTL

Kosaka, Satoshi*; Arai, Sora; Nemoto, Yasuo*; Kitamura, Ryo

JAEA-Technology 2023-003, 34 Pages, 2023/05

JAEA-Technology-2023-003.pdf:3.79MB

The negative hydrogen (H$$^{-}$$) ion beam is accelerated with a peak current of 50 mA in the J-PARC linac. The linac consists of the H- ion source and four kinds of accelerating cavities; a radio-frequency quadrupole linac (RFQ), a drift-tube linac (DTL), a separated-DTL (SDTL), and an annular-ring coupled structure linac (ACS). The accelerating electric field exists between the drift-tubes in the tank of the DTL. The quadrupole magnet for the beam focusing (DTQ) is installed in the drift-tube. The DTQ at J-PARC employs electromagnets to generate the magnetic field. It is important to set correctly the polarity of the magnetic field of the DTQ for tuning the beam. In this paper, we report the method of confirming the magnetic field polarity of DTQ, that is, the current wiring polarity by measuring DC current using a clamp meter on the power supply side and visually confirming the cable wiring connection on the electromagnet side.

Journal Articles

Oxygen reduction activity and interfacial structures of La$$_{0.8}$$Sr$$_{0.2}$$CoO$$_{3}$$ at initial electrochemical process in an alkaline solution

Matsuzaki, Akira*; Hirayama, Masaaki*; Oguchi, Shoya*; Komo, Mamoru*; Ikezawa, Atsunori*; Suzuki, Kota*; Tamura, Kazuhisa; Arai, Hajime*; Kanno, Ryoji*

Electrochemistry (Internet), 90(10), p.107001_1 - 107001_8, 2022/10

 Times Cited Count:0 Percentile:0.01(Electrochemistry)

Oxygen reduction and evolution reactions (ORR and OER) of perovskite-type La$$_{0.8}$$Sr$$_{0.2}$$CoO$$_{3}$$ were characterized using two-dimensional model electrodes with different reaction planes. Synthesized by pulsed laser deposition, these thin and flat electrodes can reveal the reaction plane dependence of the ORR activity. From steady-state polarization measurements in KOH (aq.), the ORR activity was the highest on the (001) film during the first ORR/OER cycle, and it decreased significantly during the second cycle. In-situ synchrotron X-ray diffraction clarified crystal structure changes in the bulk and surface regions of La$$_{0.8}$$Sr$$_{0.2}$$CoO$$_{3}$$, and these changes are associated with forming oxygen defects during the initial electrochemical process. Furthermore, the La$$_{0.8}$$Sr$$_{0.2}$$CoO$$_{3}$$ surface partially decomposed upon reacting. Therefore, the interfacial structures formed in the electrochemical reaction field is important for enhancing ORR and OER activities.

Journal Articles

Multipole polaron in the devil's staircase of CeSb

Arai, Yosuke*; Kuroda, Kenta*; Nomoto, Takuya*; Tin, Z. H.*; Sakuragi, Shunsuke*; Bareille, C.*; Akebi, Shuntaro*; Kurokawa, Kifu*; Kinoshita, Yuto*; Zhang, W.-L.*; et al.

Nature Materials, 21(4), p.410 - 415, 2022/04

 Times Cited Count:7 Percentile:77.62(Chemistry, Physical)

Journal Articles

Spin excitations coupled with lattice and charge dynamics in La$$_{2-x}$$Sr$$_{x}$$CuO$$_{4}$$

Ikeuchi, Kazuhiko*; Wakimoto, Shuichi; Fujita, Masaki*; Fukuda, Tatsuo; Kajimoto, Ryoichi; Arai, Masatoshi*

Physical Review B, 105(1), p.014508_1 - 014508_7, 2022/01

 Times Cited Count:2 Percentile:34.67(Materials Science, Multidisciplinary)

Journal Articles

Coexistence of two components in magnetic excitations of La$$_{2-x}$$Sr$$_{x}$$CuO$$_{4}$$ ($$x$$ = 0.10 and 0.16)

Sato, Kentaro*; Ikeuchi, Kazuhiko*; Kajimoto, Ryoichi; Wakimoto, Shuichi; Arai, Masatoshi*; Fujita, Masaki*

Journal of the Physical Society of Japan, 89(11), p.114703_1 - 114703_7, 2020/11

 Times Cited Count:6 Percentile:50.41(Physics, Multidisciplinary)

Journal Articles

Devil's staircase transition of the electronic structures in CeSb

Kuroda, Kenta*; Arai, Yosuke*; Rezaei, N.*; Kunisada, So*; Sakuragi, Shunsuke*; Alaei, M.*; Kinoshita, Yuto*; Bareille, C.*; Noguchi, Ryo*; Nakayama, Mitsuhiro*; et al.

Nature Communications (Internet), 11, p.2888_1 - 2888_9, 2020/06

 Times Cited Count:20 Percentile:75.49(Multidisciplinary Sciences)

Journal Articles

Extraction mechanism of lanthanide ions into silica-based microparticles studied by single microparticle manipulation and microspectroscopy

Otaka, Toshiki*; Sato, Tatsumi*; Ono, Shimpei; Nagoshi, Kohei; Abe, Ryoji*; Arai, Tsuyoshi*; Watanabe, So; Sano, Yuichi; Takeuchi, Masayuki; Nakatani, Kiyoharu*

Analytical Sciences, 35(10), p.1129 - 1133, 2019/10

 Times Cited Count:9 Percentile:40.49(Chemistry, Analytical)

Journal Articles

Q dependence of magnetic resonance mode on FeTe$$_{0.5}$$Se$$_{0.5}$$ studied by inelastic neutron scattering

Ishikado, Motoyuki*; Kodama, Katsuaki; Kajimoto, Ryoichi; Nakamura, Mitsutaka; Inamura, Yasuhiro; Ikeuchi, Kazuhiko*; Ji, S.*; Arai, Masatoshi*; Shamoto, Shinichi

Condensed Matter (Internet), 4(3), p.69_1 - 69_10, 2019/09

The enhancement magnetic resonance mode of FeTe$$_{0.5}$$Se$$_{0.5}$$ is limited around Q = ($$pi$$, 0). Q dependence is found to be consistent with a theoretical simulation of the magnetic resonance mode with the sign-reversing order parameter of s$$pm$$wave.

Journal Articles

Microscopic analyses of complexes formed in adsorbent for Mo and Zr separation chromatography

Abe, Ryoji*; Nagoshi, Kohei*; Arai, Tsuyoshi*; Watanabe, So; Sano, Yuichi; Matsuura, Haruaki*; Takagi, Hideaki*; Shimizu, Nobutaka*; Koka, Masashi*; Sato, Takahiro*

Nuclear Instruments and Methods in Physics Research B, 404, p.173 - 178, 2017/08

 Times Cited Count:5 Percentile:44.54(Instruments & Instrumentation)

Journal Articles

Lithium intercalation and structural changes at the LiCoO$$_{2}$$ surface under high voltage battery operation

Taminato, So*; Hirayama, Masaaki*; Suzuki, Kota*; Tamura, Kazuhisa; Minato, Taketoshi*; Arai, Hajime*; Uchimoto, Yoshiharu*; Ogumi, Zempachi*; Kanno, Ryoji*

Journal of Power Sources, 307, p.599 - 603, 2016/03

 Times Cited Count:34 Percentile:71.85(Chemistry, Physical)

An epitaxial-film model electrode of LiCoO$$_{2}$$(104) was fabricated on SrRuO$$_{3}$$(100)/Nb:SrTiO$$_{3}$$(100) using pulsed laser deposition. The 50 nm thick LiCoO$$_{2}$$(104) film exhibited lithium (de-)intercalation activity with a first discharge capacity of 119 mAh g$$^{-1}$$ between 3.0 and 4.4 V, followed by a gradual capacity fading with subsequent charge-discharge cycles. In contrast, a 3.2 nm thick Li$$_{3}$$PO$$_{4}$$-coated film exhibited a higher intercalation capacity of 148 mAh g$$^{-1}$$ with superior cycle retention than the uncoated film. In situ surface X-ray diffraction measurements revealed a small lattice change at the coated surface during the (de-)intercalation processes compared to the uncoated surface. The surface modification of LiCoO$$_{2}$$ by the Li$$_{3}$$PO$$_{4}$$ coating could lead to improvement of the structural stability at the surface region during lithium (de-)intercalation at high voltage.

Journal Articles

Discovery of a selective Cs$$^{+}$$ binding site of a $$beta$$-lactamase from the halophile by anomalous X-ray diffraction

Arai, Shigeki; Shibazaki, Chie; Shimizu, Rumi; Adachi, Motoyasu; Tamada, Taro; Tokunaga, Hiroko*; Ishibashi, Matsujiro*; Tokunaga, Masao*; Kuroki, Ryota

Kyushu Shinkurotoronko Kenkyu Senta Nempo, 2014, p.17 - 19, 2016/03

no abstracts in English

Journal Articles

MAGIC chopper; Basic concept and experimental evaluation

Nakamura, Mitsutaka; Ikeuchi, Kazuhiko*; Kajimoto, Ryoichi; Kambara, Wataru; Krist, T.*; Shinohara, Takenao; Arai, Masatoshi; Iida, Kazuki*; Kamazawa, Kazuya*; Inamura, Yasuhiro; et al.

JAEA-Conf 2015-002, p.339 - 348, 2016/02

We have developed a new Fermi chopper referred to as Magic chopper to realize the full optimization of the experimental condition for Multi-Ei method in a chopper spectrometer. In this study, the theoretical aspects of MAGIC chopper concept will be initially presented, and the performances of MAGIC chopper will be evaluated by both Monte Carlo simulation and neutron transmission experiment.

Journal Articles

Recent progress in the chopper spectrometer 4SEASONS at J-PARC

Kajimoto, Ryoichi; Nakamura, Mitsutaka; Inamura, Yasuhiro; Kamazawa, Kazuya*; Ikeuchi, Kazuhiko*; Iida, Kazuki*; Ishikado, Motoyuki*; Nakajima, Kenji; Kawamura, Seiko; Nakatani, Takeshi; et al.

JAEA-Conf 2015-002, p.319 - 329, 2016/02

Journal Articles

SENJU; A New time-of-flight single-crystal neutron diffractometer at J-PARC

Ohara, Takashi; Kiyanagi, Ryoji; Oikawa, Kenichi; Kaneko, Koji; Kawasaki, Takuro; Tamura, Itaru; Nakao, Akiko*; Hanashima, Takayasu*; Munakata, Koji*; Moyoshi, Taketo*; et al.

Journal of Applied Crystallography, 49(1), p.120 - 127, 2016/02

 Times Cited Count:51 Percentile:95.86(Chemistry, Multidisciplinary)

Journal Articles

Microstructure and residual strain distribution in cast duplex stainless steel studied by neutron imaging

Su, Y. H.; Oikawa, Kenichi; Kawasaki, Takuro; Kai, Tetsuya; Shiota, Yoshinori*; Sato, Hirotaka*; Shinohara, Takenao; Tomota, Yo*; Harada, Masahide; Kiyanagi, Ryoji; et al.

JPS Conference Proceedings (Internet), 8, p.031015_1 - 031015_5, 2015/09

In this study, neutron imaging experiment was performed using NOBORU, BL10 of MLF at J-PARC. Four kinds of cast duplex stainless steel with ferrite and austenite microstructure were studied here, which were produced by different casting method at different temperature. Firstly, two-dimensional scintillation detector using wavelength-shifting fibers with pixel size of 0.52 mm $$times$$ 0.52 mm and illuminated area 55 mm $$times$$ 55 mm was used for data collection. Then, measurement by Micro Pixel Chamber based neutron imaging detector having higher spatial resolution about 0.2 mm was conducted. Data analysis code RITS (Rietveld Imaging of Transmission Spectra) will be used for microstructure including crystalline phase, lattice strain, crystallite size, texture evaluation.

Journal Articles

Background caused by continuously emitted high-energy neutrons at the chopper spectrometer 4SEASONS

Kajimoto, Ryoichi; Nakamura, Mitsutaka; Inamura, Yasuhiro; Kamazawa, Kazuya*; Ikeuchi, Kazuhiko*; Iida, Kazuki*; Ishikado, Motoyuki*; Nakajima, Kenji; Harada, Masahide; Arai, Masatoshi

JPS Conference Proceedings (Internet), 8, p.036001_1 - 036001_6, 2015/09

Journal Articles

Neutron scattering study of spin fluctuations in La$$_{2-x}$$Sr$$_{x}$$CuO$$_{4}$$ by four-dimensional mapping of neutron cross-sections using the 4SEASONS chopper spectrometer

Wakimoto, Shuichi; Ikeuchi, Kazuhiko*; Arai, Masatoshi; Fujita, Masaki*; Kajimoto, Ryoichi; Kawamura, Sho*; Matsuura, Masato*; Nakajima, Kenji; Yamada, Kazuyoshi*

JPS Conference Proceedings (Internet), 8, p.034013_1 - 034013_6, 2015/09

Journal Articles

Nucleoside diphosphate kinase from psychrophilic ${it Pseudoalteromonas}$ sp. AS-131 isolated from Antarctic Ocean

Yonezawa, Yasushi*; Nagayama, Aiko*; Tokunaga, Hiroko*; Ishibashi, Matsujiro*; Arai, Shigeki; Kuroki, Ryota; Watanabe, Keiichi*; Arakawa, Tsutomu*; Tokunaga, Masao*

Protein Journal, 34(4), p.275 - 283, 2015/08

 Times Cited Count:4 Percentile:11.12(Biochemistry & Molecular Biology)

Nucleoside diphosphate kinase isolated from psychrophilic ${it Pseudoalteromonas}$ sp. AS-131 (ASNDK) was expressed in ${it Escherichia coli}$ and purified to homogeneity. Comparing to mesophilic NDK isolated from ${it Pseudomonas aeruginosa}$, ASNDK exhibited highly elevated thermolability: (1) ${it E. coli}$ expression at 37$$^{circ}$$C as a denatured insoluble form, and (2) 30$$^{circ}$$C lower optimum temperature of enzymatic activity. The subunit structure of ASNDK was suggested to be dimer, as in NDKs isolated from moderate halophiles.

Journal Articles

Structure of a highly acidic $$beta$$-lactamase from the moderate halophile ${it Chromohalobacter}$ sp.560 and the discovery of a Cs$$^{+}$$-selective binding site

Arai, Shigeki; Yonezawa, Yasushi*; Okazaki, Nobuo*; Matsumoto, Fumiko*; Shibazaki, Chie; Shimizu, Rumi; Yamada, Mitsugu*; Adachi, Motoyasu; Tamada, Taro; Kawamoto, Masahide*; et al.

Acta Crystallographica Section D, 71(3), p.541 - 554, 2015/03

 Times Cited Count:7 Percentile:50.76(Biochemical Research Methods)

The crystal structure of halophilic $$beta$$-lactamase from ${it Chromohalobacter}$ sp.560 (HaBLA) was determined using X-ray crystallography. Moreover, the locations of bound Sr$$^{2+}$$ and Cs$$^{+}$$ ions were identified by anomalous X-ray diffraction. The location of one Cs$$^{+}$$ specific binding site was identified on HaBLA even in the presence of 9-fold molar excess of Na$$^{+}$$ (90 mM Na$$^{+}$$ /10 mM Cs$$^{+}$$). This Cs$$^{+}$$ binding site is formed by two main-chain O atoms and an aromatic ring of a side chain of Trp. An aromatic ring of Trp interacts with Cs$$^{+}$$ by the cation-$$pi$$ interaction. The observation of a selective and high-affinity Cs$$^{+}$$ binding site provides important information that is useful for designing artificial Cs$$^{+}$$ binding sites useful in bioremediation of radioactive isotopes.

256 (Records 1-20 displayed on this page)