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JAEA Reports

Report of summer holiday practical training on 2022

Ishitsuka, Etsuo; Ho, H. Q.; Kitagawa, Kanta*; Fukuda, Takahito*; Ito, Ryo*; Nemoto, Masaya*; Kusunoki, Hayato*; Nomura, Takuro*; Nagase, Sota*; Hashimoto, Haruki*; et al.

JAEA-Technology 2023-013, 19 Pages, 2023/06

JAEA-Technology-2023-013.pdf:1.75MB

Eight people from five universities participated in the 2022 summer holiday practical training with the theme of "Technical development on HTTR". The participants practiced the feasibility study for nuclear battery, the burn-up analysis of HTTR core, the feasibility study for $$^{252}$$Cf production, the analysis of behavior on loss of forced cooling test, and the thermal-hydraulic analysis near reactor pressure vessel. In the questionnaire after this training, there were impressions such as that it was useful as a work experience, that some students found it useful for their own research, and that discussion with other university students was a good experience. These impressions suggest that this training was generally evaluated as good.

Journal Articles

Development of nondestructive elemental analysis system for Hayabusa2 samples using muonic X-rays

Osawa, Takahito; Nagasawa, Shunsaku*; Ninomiya, Kazuhiko*; Takahashi, Tadayuki*; Nakamura, Tomoki*; Wada, Taiga*; Taniguchi, Akihiro*; Umegaki, Izumi*; Kubo, Kenya*; Terada, Kentaro*; et al.

ACS Earth and Space Chemistry (Internet), 7(4), p.699 - 711, 2023/04

 Times Cited Count:4 Percentile:93.95(Chemistry, Multidisciplinary)

The concentrations of carbon and other major elements in asteroid samples provide very important information on the birth of life on the Earth and the solar-system evolution. Elemental analysis using muonic X-rays is one of the best analytical methods to determine the elemental composition of solid materials, and notably, is the only method to determine the concentration of light elements in bulk samples in a non-destructive manner. We developed a new analysis system using muonic X-rays to measure the concentrations of carbon and other major elements in precious and expectedly tiny samples recovered from the asteroid Ryugu by spacecraft Hayabusa2. Here we report the development process of the system in 4 stages and their system configurations, The analysis system is composed of a stainless-steel analysis chamber, an acrylic glove box for manipulating asteroid samples in a clean environment, and Ge semiconductor detectors arranged to surround the analysis chamber. The performance of the analysis system, including the background level, which is crucial for the measurement, was greatly improved from the first stage to the later ones. Our feasibility study showed that the latest model of our muonic X-ray analysis system is capable of determining the carbon concentration in Hayabusa2's sample model with an uncertainty of less than 10 percent in a 6-day measurement.

Journal Articles

Evolution of austenite lattice parameter during isothermal transformation in a 0.4 C low alloyed steel

Wang, Y.*; Tomota, Yo*; Omura, Takahito*; Gong, W.; Harjo, S.

Materialia, 27, p.101685_1 - 101685_9, 2023/03

Journal Articles

Dynamical response of transition-edge sensor microcalorimeters to a pulsed charged-particle beam

Okumura, Takuma*; Azuma, Toshiyuki*; Bennet, D. A.*; Caradonna, P.*; Chiu, I.-H.*; Doriese, W. B.*; Durkin, M. S.*; Fowler, J. W.*; Gard, J. D.*; Hashimoto, Tadashi; et al.

IEEE Transactions on Applied Superconductivity, 31(5), p.2101704_1 - 2101704_4, 2021/08

 Times Cited Count:1 Percentile:11.15(Engineering, Electrical & Electronic)

A superconducting transition-edge sensor (TES) microcalorimeter is an ideal X-ray detector for experiments at accelerator facilities because of good energy resolution and high efficiency. To study the performance of the TES detector with a high-intensity pulsed charged-particle beam, we measured X-ray spectra with a pulsed muon beam at the Japan Proton Accelerator Research Complex (J-PARC) in Japan. We found substantial temporal shifts of the X-ray energy correlated with the arrival time of the pulsed muon beam, which was reasonably explained by pulse pileup due to the incidence of energetic particles from the initial pulsed beam.

Journal Articles

Deexcitation dynamics of muonic atoms revealed by high-precision spectroscopy of electronic $$K$$ X rays

Okumura, Takuma*; Azuma, Toshiyuki*; Bennet, D. A.*; Caradonna, P.*; Chiu, I. H.*; Doriese, W. B.*; Durkin, M. S.*; Fowler, J. W.*; Gard, J. D.*; Hashimoto, Tadashi; et al.

Physical Review Letters, 127(5), p.053001_1 - 053001_7, 2021/07

 Times Cited Count:13 Percentile:79.44(Physics, Multidisciplinary)

We observed electronic $$K$$X rays emitted from muonic iron atoms using a superconducting transition-edge-type sensor microcalorimeter. The energy resolution of 5.2 eV in FWHM allowed us to observe the asymmetric broad profile of the electronic characteristic $$K$$$$alpha$$ and $$K$$$$beta$$ X rays together with the hypersatellite $$K$$$$alpha$$ X rays around 6 keV. This signature reflects the time-dependent screening of the nuclear charge by the negative muon and the $$L$$-shell electrons, accompanied by electron side-feeding. Assisted by a simulation, this data clearly reveals the electronic $$K$$- and $$L$$-shell hole production and their temporal evolution during the muon cascade process.

Journal Articles

Continuous and discontinuous yielding behaviors in ferrite-cementite steels

Wang, Y.*; Tomota, Yo*; Omura, Takahito*; Gong, W.*; Harjo, S.; Tanaka, Masahiko*

Acta Materialia, 196, p.565 - 575, 2020/09

 Times Cited Count:31 Percentile:90.48(Materials Science, Multidisciplinary)

Journal Articles

Influence of carbon concentration and magnetic transition on the austenite lattice parameter of 30Mn-C steel

Tomota, Yo*; Murakami, Toshio*; Wang, Y. X.*; Omura, Takahito*; Harjo, S.; Su, Y. H.; Shinohara, Takenao

Materials Characterization, 163, p.110243_1 - 110243_8, 2020/05

 Times Cited Count:4 Percentile:32.96(Materials Science, Multidisciplinary)

Journal Articles

${it In situ}$ neutron diffraction on ferrite and pearlite transformations for a 1.5Mn-1.5Si-0.2C steel

Tomota, Yo*; Wang, Y.*; Omura, Takahito*; Sekido, Nobuaki*; Harjo, S.; Kawasaki, Takuro; Gong, W.*; Taniyama, Akira*

Tetsu To Hagane, 106(5), p.262 - 271, 2020/05

 Times Cited Count:0 Percentile:0(Metallurgy & Metallurgical Engineering)

Journal Articles

Real time observation of martensite transformation for a 0.4C low alloyed steel by neutron diffraction

Wang, Y.*; Tomota, Yo*; Omura, Takahito*; Morooka, Satoshi; Gong, W.*; Harjo, S.

Acta Materialia, 184, p.30 - 40, 2020/02

 Times Cited Count:26 Percentile:86.78(Materials Science, Multidisciplinary)

Journal Articles

Non-destructive elemental analysis of a carbonaceous chondrite with direct current Muon beam at MuSIC

Terada, Kentaro*; Sato, Akira*; Ninomiya, Kazuhiko*; Kawashima, Yoshitaka*; Shimomura, Koichiro*; Yoshida, Go*; Kawai, Yosuke*; Osawa, Takahito; Tachibana, Shogo*

Scientific Reports (Internet), 7(1), p.15478_1 - 15478_6, 2017/11

AA2017-0455.pdf:1.15MB

 Times Cited Count:21 Percentile:68.68(Multidisciplinary Sciences)

Electron- or X-ray-induced characteristic X-ray analysis has been widely used to determine chemical compositions of materials in vast research fields. In recent years, analysis of characteristic X-rays from muonic atoms, in which a muon is captured, has attracted attention because both a muon beam and a muon-induced characteristic X-ray have high transmission abilities. Here we report the first non-destructive elemental analysis of a carbonaceous chondrite using one of the world-leading intense direct current muon beam source (MuSIC; MUon Science Innovative Channel). We successfully detected characteristic muonic X-rays of Mg, Si, Fe, O, S and C from Jbilet Winselwan CM chondrite, of which carbon content is about 2 wt percent, and the obtained elemental abundance pattern was consistent with that of CM chondrites.

Journal Articles

Hardness modification of Al-Mg-Si alloy by using energetic ion beam irradiation

Ueyama, Daichi*; Saito, Yuichi; Ishikawa, Norito; Omura, Takahito*; Semboshi, Satoshi*; Hori, Fuminobu*; Iwase, Akihiro*

Nuclear Instruments and Methods in Physics Research B, 351, p.1 - 5, 2015/05

 Times Cited Count:6 Percentile:39.96(Instruments & Instrumentation)

Journal Articles

Radiation-induced swelling and softening in magnesium aluminate spinel irradiated with high-flux Cu$$^{-}$$ ions

Lee, C. G.; Omura, Takahito*; Takeda, Yoshihiko*; Matsuoka, Saburo*; Kishimoto, Naoki*

Journal of Nuclear Materials, 326(2-3), p.211 - 216, 2004/03

 Times Cited Count:4 Percentile:29.26(Materials Science, Multidisciplinary)

Magnesium aluminate spinel of single crystal was irradiated with 60 keV Cu$$^{-}$$ at a dose rate up to 100 $$mu$$A/cm$$^{2}$$, to a total dose of 3$$times$$10$$^{16}$$ ions/cm$$^{2}$$, in order to study changes in hardness and step-height swelling by high-flux implantation. Hardness determined by nano-indentation measurements steeply decreased with implantation. There is a strong negative correlation between dose-rate dependences of the hardness and the step-height swelling: the former decreases as the latter increases. The Rutherford Backscattering Spectrometry (RBS)/channeling measurements showed that the spinel is not completely amorphized over the dose-rate range in this study, and the radiation-induced softening observed is not due to amorphization. Results of optical absorbance suggested that radiation-induced point defects and their clusters on the anion sublattices of the spinel played an important role in the radiation-induced swelling under high-flux ion implantation.

Oral presentation

Development on non-destructive muonic X-ray analysis of carbonaceous chondrites; Feasibility test for returned samples from C-type asteroids

Terada, Kentaro*; Sato, Akira*; Ninomiya, Kazuhiko*; Kawashima, Yoshitaka*; Shimomura, Koichiro*; Tomono, Dai*; Kawai, Yosuke*; Osawa, Takahito; Tachibana, Shogo*

no journal, , 

In recent years, analysis of characteristic X-rays from muonic atoms, in which a muon is captured, has attracted attention because both a muon beam and a muon-induced characteristic X-ray have high transmission abilities, of which energies are about 200 times higher. From these features, a muonic X-ray analysis has great advantages in several ways. At the conference, we will report on our recent progress of muonic X-ray analysis and discuss on a future prospect for applications for Earth and planetary science.

Oral presentation

Development of nondestructive three-dimensional elemental imaging method based muon X-ray measurement using CdTe-DSD at J-PARC

Chiu, I.-H. ; Osawa, Takahito; Takeda, Shinichiro*; Katsuragawa, Miho*; Takahashi, Tadayuki*; Watanabe, Shin*; Mizumoto, Kazumi*; Saito, Tsutomu*; Kubo, Kenya*; Umegaki, Izumi*; et al.

no journal, , 

no abstracts in English

Oral presentation

Development of a 3D elemental imaging system with muonic X-ray measurement using the CdTe detectors

Chiu, I.-H. ; Osawa, Takahito; Takeda, Shinichiro*; Katsuragawa, Miho*; Takahashi, Tadayuki*; Watanabe, Shin*; Kubo, Kenya*; Mizumoto, Kazumi*; Saito, Tsutomu*; Umegaki, Izumi*; et al.

no journal, , 

Non-destructive elemental analysis method has been developed for the materials by high-energy muon-characteristic X-rays measurement. To further improve the method, we have also utilized two-dimensional cadmium telluride hard X-ray detectors (CdTe-DSDs) for the muonic X-rays measurement to obtain the 3D elemental distribution of the sample. In this work, a 3D imaging system has been created using four CdTe-DSDs. The experiment of 3D elemental imaging for archaeological materials was performed using a negative muon beam at J-PARC/MUSE, and the three-dimensional distribution of silicon and oxygen was confirmed. This presentation introduces the research progress so far.

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