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Yamashita, Keishiro*; Komatsu, Kazuki*; Ohara, Takashi; Munakata, Koji*; Irifune, Tetsuo*; Shimmei, Toru*; Sugiyama, Kazumasa*; Kawamata, Toru*; Kagi, Hiroyuki*
High Pressure Research, 42(1), p.121 - 135, 2022/03
Times Cited Count:4 Percentile:50.56(Physics, Multidisciplinary)Hattori, Takanori; Kawamura, Seiko; Kawasaki, Takuro
High Pressure Research, 42(2), p.226 - 235, 2022/00
Times Cited Count:0 Percentile:0.00(Physics, Multidisciplinary)We have developed a hybrid piston cylinder cell for quasi-elastic neutron scattering (QENS) experiments up to about 1 GPa. It consists of a fretted cylinder made of the high tensile steel (SNCM439) liner and the Al alloy (NA700) jacket. Performance tests revealed that the cell can withstand a pressure of 0.8 GPa without irreversible damage and has 4.4 times larger neutron transmission at 3.14 meV (5.10 in wavelength) than that of a conventional CuBe monobloc cylinder. Combined with the sample assembly devised for suppressing multiple scattering, high quality QENS spectra of water were obtained up to 0.8 GPa. This study illustrates the efficacy of the hybrid cylinders not only for increasing maximum available pressure but also manipulating the available pressure and the signal intensity, depending on the purpose of the experiments.
Sano, Asami; Kakizawa, Sho*; Shito, Chikara*; Hattori, Takanori; Machida, Shinichi*; Abe, Jun*; Funakoshi, Kenichi*; Kagi, Hiroyuki*
High Pressure Research, 41(1), p.65 - 74, 2021/03
Times Cited Count:4 Percentile:40.44(Physics, Multidisciplinary)We applied Kawai-type multi-anvil assemblies (MA6-8) for time-of-flight neutron-diffraction experiments to achieve high pressures and high temperatures simultaneously. To achieve sufficient signal intensities, the angular access to the sample was enlarged using slits and tapers on the first-stage anvils. Using SiC-binder sintered diamond for the second-stage anvils that transmits neutrons, sufficient signal intensities were achieved at a high-pressure of 23.1 GPa. A high-temperature experiment was also conducted at 16.2 GPa and 973 K, validating the use of tungsten carbide for the second-stage anvils. The present study reveals the capability of the MA6-8 cells in neutron-diffraction experiments to attain pressures and temperatures beyond the limits of the conventional MA6-6 cells used in the high-pressure neutron diffractometer PLANET at the MLF, J-PARC.
Hattori, Takanori; Sano, Asami; Machida, Shinichi*; Ouchi, Keiichi*; Kira, Hiroshi*; Abe, Jun*; Funakoshi, Kenichi*
High Pressure Research, 40(3), p.325 - 338, 2020/09
Times Cited Count:4 Percentile:33.34(Physics, Multidisciplinary)To understand the practical effects of pressure-transmitting media (PTM) on neutron diffraction using Paris-Edinburgh presses, diffraction patterns of MgO were collected to approximately 20 GPa using PTMs of Pb, AgCl, 4:1 methano-ethanol (ME) mixture with and without heating, N, and Ar. Hydrostaticity in the sample chamber estimated from the MgO 220 peak width improves in the order of Pb, AgCl, Ar, ME mixture, N
, and the heated ME mixture. Unlike previous results using a diamond anvil cell, the unheated ME mixture is superior to Ar even after freezing, probably due to the cup on the anvil face. Considering these results and the sizable coherent scattering of Ne, which would show good hydrostaticity, we conclude that the ME mixture (preferably the heated one) is the best PTM in neutron experiments up to 20 GPa, while Ar can be substituted when a sample is reactive to alcohols.
Komatsu, Kazuki*; Klotz, S.*; Nakano, Satoshi*; Machida, Shinichi*; Hattori, Takanori; Sano, Asami; Yamashita, Keishiro*; Irifune, Tetsuo*
High Pressure Research, 40(1), p.184 - 193, 2020/02
Times Cited Count:14 Percentile:68.19(Physics, Multidisciplinary)A new high pressure cells for neutron diffraction experiments using nano-polycrystalline anvil is presented. The cell design, off-line pressure generation tests and a gas-loading procedure for this cell are described. The performance is illustrated by powder neutron diffraction patterns of ice VII to 82 GPa. We also demonstrate the feasibility of single crystal neutron diffraction experiments of Fe
O
at ambient conditions using this cell and discuss the current limitation and future developments.
Hattori, Takanori; Sano, Asami; Machida, Shinichi*; Abe, Jun*; Funakoshi, Kenichi*; Arima, Hiroshi*; Okazaki, Nobuo*
High Pressure Research, 39(3), p.417 - 425, 2019/06
Times Cited Count:26 Percentile:80.41(Physics, Multidisciplinary)We have developed a technique for neutron diffraction experiments at pressures up to 40 GPa using a Paris-Edinburgh press at the PLANET beamline in J-PARC. To increase the maximum accessible pressure, the diameter of the dimple for sample chamber at the top of the sintered diamond anvils is sequentially reduced from 4.0 mm to 1.0 mm. As a result, the maximum pressure increased and finally reached 40 GPa. By combining this technique with the beam optics which defines the gauge volume, diffraction patterns sufficient for full-structure refinements are obtainable at such pressures.
Yagafarov, O.; Katayama, Yoshinori; Brazhkin, V. V.*; Lyapin, A. G.*; Saito, Hiroyuki
High Pressure Research, 33(1), p.191 - 195, 2013/01
Times Cited Count:5 Percentile:37.97(Physics, Multidisciplinary)Saito, Hiroyuki; Abe, Jun
High Pressure Research, 31(3), p.407 - 412, 2011/09
Times Cited Count:0 Percentile:0.00(Physics, Multidisciplinary)Matsuoka, Takehiro*; Kitayama, Takayasu*; Shimizu, Katsuya*; Nakamoto, Yuki*; Kagayama, Tomoko*; Aoki, Katsutoshi; Oishi, Yasuo*; Takemura, Kenichi*
High Pressure Research, 26(4), p.391 - 394, 2006/12
Times Cited Count:3 Percentile:26.23(Physics, Multidisciplinary)The electrical and structural properties of yttrium hydride YHx was studied by the in-situ measurements of the electrical resistance and X-ray diffraction up to 86 GPa. The electrical resistivity increased with applying pressure up to 10 GPa and showed a maximum which accompanied with the structural transition of metal lattice from hcp to fcc structure. In fcc phase the resistivity decreased significantly, however the value still remained larger by 4 orders of magnitude that that of pure yttrium metal. We could not confirm the insulator to metal transition up to 23 GPa. The resistivity showed another maximum in the large pressure region 40 60 GPa without the structural phase transition of metal lattice.
Tateiwa, Naoyuki; Haga, Yoshinori; Matsuda, Tatsuma; Yamamoto, Etsuji; Ikeda, Shugo; Onuki, Yoshichika*
High Pressure Research, 26(4), p.471 - 474, 2006/12
Times Cited Count:0 Percentile:0.00(Physics, Multidisciplinary)We investigated non-centrosymmetric compounds CePtSi and UIr by the ac heat capacity measurement under pressures. The pressure phase diagrams are determined. In CePt
Si, the N
el temperature
= 2.2 K decreases with increasing pressure and becomes zero at the critical pressure
0.6 GPa. On the other hand, the superconducting phase exists in a wider pressure region from ambient pressure to about 1.5 GPa. The phase diagram of CePt
Si is thus very unique. In the ferromagnetic compound UIr where successive ferromagnetic transitions appear under pressure, the heat capacity shows an anomaly at the Curie temperature
and this anomaly shifts to lower temperatures with increasing pressure. The present pressure dependence of
was consistent with the previous works by the resistivity and magnetization measurements.
Okube, Maki*; Yoshiasa, Akira*; Otaka, Osamu*; Katayama, Yoshinori
High Pressure Research, 23(3), p.247 - 251, 2003/09
Times Cited Count:5 Percentile:38.47(Physics, Multidisciplinary)In order to examine the pressure effect on anharmonic thermal vibrations of Pt, Extended X-ray Absorption Fine Structure (EXAFS) spectra near Pt K-edge and L-edge were measured in the temperature range from 300 to 800K under pressures up to 6vGPa, using large volume high-pressure devices and synchrotron radiation. We have investigated the anharmonic interatomic potentials by a cumulant expansion method. The values of EXAFS Debye-Waller factors,
2 and
3, become smaller with increase of pressure. The anharmonic effective pair potential
was evaluated and the potential coefficient a at 0.1MPa and 6GPa are 4.8 and 5.0eV/
, respectively. The anharmonic potential parameter
decreases with increasing pressure.
Otaka, Osamu*; Fukui, Hiroyuki*; Funakoshi, Kenichi*; Utsumi, Wataru; Irifune, Tetsuo*; Kikegawa, Takumi*
High Pressure Research, 22(1), p.221 - 226, 2002/01
Times Cited Count:30 Percentile:76.25(Physics, Multidisciplinary)no abstracts in English
Urakawa, Satoru*; Hasegawa, Masayuki*; Yamakawa, Junji*; Funakoshi, Kenichi*; Utsumi, Wataru
High Pressure Research, 22(2), p.491 - 494, 2002/01
Times Cited Count:5 Percentile:39.16(Physics, Multidisciplinary)no abstracts in English
Urakawa, Satoru*; Igawa, Naoki; Umesaki, Norimasa*; Igarashi, Kazuo*; Shimomura, Osamu*; Ono, Hideo
High Pressure Research, 14(4-6), p.375 - 382, 1996/12
Times Cited Count:6 Percentile:52.86(Physics, Multidisciplinary)no abstracts in English