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${it In situ}$ X-ray diffraction measurement of the hydrogenation and dehydrogenation of aluminum and characterization of the recovered AlH$$_{3}$$

アルミニウムの水素化・脱水素化反応の放射光その場観察と回収されたAlH$$_{3}$$の分析

齋藤 寛之; 櫻井 陽子; 町田 晃彦; 片山 芳則; 青木 勝敏

Saito, Hiroyuki; Sakurai, Yoko; Machida, Akihiko; Katayama, Yoshinori; Aoki, Katsutoshi

Pristine aluminum was hydrogenated to form AlH$$_{3}$$ at 8.9 GPa and 600 $$^{circ}$$C. The cyclic formation and decomposition of the hydride were measured by ${it in situ}$ synchrotron X-ray diffraction measurement. AlH$$_{3}$$ synthesized under high pressure and temperature was recovered at ambient conditions. The recovered AlH$$_{3}$$ was characterized by the conventional powder X-ray diffraction measurement and Raman spectroscopy. The result of the characterizations was consistent with that obtained for chemically prepared AlH$$_{3}$$ and indicated that single phase $$alpha$$-AlH$$_{3}$$ was obtained.

使用言語

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English

掲載資料名

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Journal of Physics; Conference Series

巻

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215

号

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ページ数

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p.012127_1 - 012127_4

発行年月

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2010/03

発表会議名

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International Conference on High Pressure Science and Technology (Joint AIRAPT-22 & HPCJ-50)

開催年月

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2009/07

開催都市

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Tokyo

開催国

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Japan

キーワード

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no keyword

特許データ

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PDF

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論文URL

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https://doi.org/10.1088/1742-6596/215/1/012127

研究データの公開先DOI

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使用施設

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SPring-8(大型放射光施設)

広報プレスリリース

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論文解説記事
(成果普及情報誌)

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受委託・共同研究相手機関

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Access

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- Accesses

InCites™

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パーセンタイル：85.19

分野：Instruments & Instrumentation

Altmetrics

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