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オーステナイト系ステンレス鋼の中性子照射による磁気特性変化に関する研究

Study on magnetic property change on neutron irradiated austenitic stainless steel

根本 義之; 大石 誠; 伊藤 正泰; 加治 芳行; 欅田 理*

Nemoto, Yoshiyuki; Oishi, Makoto; Ito, Masayasu; Kaji, Yoshiyuki; Keyakida, Satoshi*

これまで中性子照射したオーステナイトステンレス合金の照射誘起応力腐食割れ(IASCC)感受性と、渦電流法,交流磁化法で測定した磁気データの間に相関性があることを報告してきた。この相関性のメカニズムを検討するため、本研究では当該試験片の微細組織観察を行い、結晶粒界に沿った強磁性のパーマロイ(FeNi$$_{3}$$)の生成を確認した。この結果から照射による磁気特性変化の原因は結晶粒界での照射誘起の磁性相生成によるものであり、IASCC感受性と磁気データの相関に関連しているものと考えられる。また高感度,高位置分解能の新規センサープローブの開発を行い、SUS304オーステナイトステンレス鋼照射材の磁気測定に適用した。SUS304の試験片には照射前からフェライト相が存在していたため、照射後の材料の磁気測定に悪影響を及ぼす可能性が懸念されたが、実験結果においては照射量に依存した磁気データの上昇が捉えられた。そのため本研究で開発した磁気測定の技術は照射前からフェライト相を含むオーステナイトステンレス鋼照射材にも適用可能であることが示されたと考えられる。

Authors previously reported that magnetic data obtained by using Eddy current method and AC magnetization method showed correlation with the increase of susceptibility of the irradiation assisted stress corrosion cracking (IASCC) on neutron irradiated austenitic stainless alloy specimens. To discuss the mechanism of the correlation, microstructure observation was conducted on the irradiated specimen, and magnetic permalloy phase (FeNi$$_{3}$$) formation along grain boundary was revealed in this work. From this result, the radiation induced magnetic phase formation along grain boundary seems to be a factor of the magnetic property change of the irradiated materials, and related to the correlation between magnetic data and IASCC susceptibility. In addition, sensor probe development was conducted in this work to obtain higher sensitivity and resolution. It was applied for magnetic measurement on type304 stainless steel irradiated up to different doses. In this case, magnetic ferrite phase was existed in the type304 stainless steel sample before irradiation therefore it was concerned that magnetic measurement on the irradiated ones would be disturbed by the magnetic signal from the pre-existing ferrite phase. In the magnetic measurements, increase of the magnetic data was clearly seen on the irradiated specimens. Thus, it was thought that the developed magnetic measurement technics can be applied for the irradiated austenite stainless steels which contain certain quantity of ferrite phase before irradiation.

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