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論文

Assessment of failure life evaluation methods for structural discontinuities with fatigue and creep-fatigue tests on multiperforated plate made of Mod.9Cr-1Mo steel

安藤 勝訓; 廣瀬 悠一*; 高野 雅仁*

Journal of Pressure Vessel Technology, 143(6), p.061505_1 - 061505_9, 2021/12

本研究では、改良9Cr-1Mo鋼製の多孔板試験体の疲労及びクリープ疲労試験の行い、その結果を用いて種々の構造物の疲労およびクリープ疲労寿命の評価方法を比較・検証を行った。具体的には、多孔板試験体の試験では550$$^{circ}$$Cにおいて機械的繰り返し荷重を加え、孔の表面における亀裂の発生と伝播を観察するとともに、一連の有限要素解析に基づいて、種々の破損寿命評価方法により破損繰返し数を予測して、試験結果と予測結果の比較検証を行た。

論文

Chemical characterization of a volatile dubnium compound, DbOCl$$_3$$

Chiera, N. M.*; 佐藤 哲也; Eichler, R.*; 富塚 知博; 浅井 雅人; 安達 サディア*; Dressler, R.*; 廣瀬 健太郎; 井上 浩樹*; 伊藤 由太; et al.

Angewandte Chemie; International Edition, 60(33), p.17871 - 17874, 2021/08

 被引用回数:0 パーセンタイル:0(Chemistry, Multidisciplinary)

等温ガスクロマトグラフ法を用いて、105番元素ドブニウム(Db)の単一原子を対象として、揮発性オキシ塩化物を合成し、化学的性質を調べた。同一条件下で同族元素ニオブおよびタンタルの揮発性と比較したところ、NbOCl$$_3 > $$ TaOCl$$_3 geq$$ DbOCl$$_3$$の関係が得られた。これはDb分子中の共有結合性が周期表からの予想よりも強くなっているためと考えられる。本成果により、超アクチノイド元素の化学的性質に関する理論計算に対する信頼できる実験データを与えることができた。

論文

新材料・新製品開発のための先端解析技術

佐々木 宏和*; 西久保 英郎*; 西田 真輔*; 山崎 悟志*; 中崎 竜介*; 磯松 岳己*; 湊 龍一郎*; 衣川 耕平*; 今村 明博*; 大友 晋哉*; et al.

古河電工時報, (138), p.2 - 10, 2019/02

電子顕微鏡や放射光等の先端解析技術は、試料の構造や化学状態について多くの有用な情報をもたらし、材料研究に欠かせないツールとなっている。本稿では、これらの先端解析技術の中から、電子線ホログラフィや放射光を用いたX線小角散乱法(SAXS)等の手法を中心に、材料研究への応用事例を紹介する。これらの手法を活用することにより、未知であった材料の本質を明らかにすることができ、新製品開発の指針を定める上で重要な知見を得ることができる。

論文

Study of fission using multi-nucleon transfer reactions

西尾 勝久; 廣瀬 健太郎; Vermeulen, M. J.; 牧井 宏之; Orlandi, R.; 塚田 和明; 浅井 雅人; 豊嶋 厚史; 佐藤 哲也; 永目 諭一郎; et al.

EPJ Web of Conferences, 163, p.00041_1 - 00041_6, 2017/11

 被引用回数:1 パーセンタイル:69.68

We are promoting a study of fission using multi-nucleon transfer (MNT) reactions, where excited states in neutron-rich actinide nuclei, which cannot be accessed by particle capture and/or fusion reactions, are populated. Also, the excited states in the fissioning nucleus are widely populated by the MNT reactions, from which effects of excitation energy on fission properties can be investigated. Experiments were carried out at the JAEA tandem facility in Tokai, Japan. We studied reactions using the $$^{18}$$O beam and several actinide target nuclei such as $$^{232}$$Th, $$^{238}$$U, $$^{237}$$Np, $$^{248}$$Cm. Ejectile nucleus was identified by a silicon $$Delta$$E-E telescope to identify transfer channel and hence the compound nucleus. Fission fragments were detected by multi-wire proportional counters, and fission fragment mass distributions (FFMDs) were measured for each isotope. Measured FFMDs are reproduced by a calculation based on the fluctuation-dissipation model, and importance of multi-chance fission concept is investigated. Fission fragment angular distribution relative to the recoil direction suggested the increase of the spin of the fissioning nucleus with the number of transferred nucleons.

論文

Creep-fatigue tests of double-end notched bar made of Mod.9Cr-1Mo steel

下村 健太; 加藤 章一; 若井 隆純; 安藤 勝訓; 廣瀬 祐一*; 佐藤 健一郎*

Proceedings of 23rd International Conference on Nuclear Engineering (ICONE-23) (DVD-ROM), 9 Pages, 2015/05

本研究は、SFR機器の設計基準が考えうるすべての破損様式をカバーしていることを確認するための実験的・解析的研究である。現行の設計基準におけるクリープ疲労損傷評価法は、従来のオーステナイト系ステンレス鋼(例えばSUS304)の実験や数値解析に基づいて構築されている。改良9Cr-1Mo鋼の材料特性はオーステナイト系ステンレス鋼のそれらとはかなり異なるので、現行の設計基準の改良9Cr-1Mo鋼製機器への適用性を確認する必要がある。両側切欠きを有する改良9Cr-1Mo鋼試験片に対する30分のひずみ保持を伴う単軸クリープ疲労試験を実施した。キリカキ底の半径は、1.6mm, 11.2mmと40.0mm。1.6mmと11.2mmの切欠き試験片は切欠き底から破損したが、40.0mmの切欠き試験片は明らかに内部から破損した。また、保持時間は合計わずか2,000時間程度であるにもかかわらず、多くのクリープボイドと、粒状界き裂成長が観察された。このような特異な破損様式の原因を究明するため、いくつかの追加実験と数値解析を実施した。それらの結果から、このような特異な破損様式の原因を絞り込むことができた。最大の要因をはっきりさせるための将来の計画も提案した。

論文

Comparison and assessment of the creep-fatigue evaluation methods with notched specimens made of Mod.9Cr-1Mo steel

安藤 勝訓; 廣瀬 悠一*; 唐戸 孝典*; 渡邊 壮太*; 井上 修*; 川崎 信史; 江沼 康弘*

Journal of Pressure Vessel Technology, 136(4), p.041406_1 - 041406_10, 2014/08

 被引用回数:8 パーセンタイル:43.99(Engineering, Mechanical)

構造不連続部のクリープ疲労評価法の比較評価のため、改良9Cr-1Mo鋼切り欠き試験体によるクリープ疲労試験を実施した。試験は単軸の引張り-圧縮試験及びインダクションコイルを用いた熱荷重による試験を行った。応力集中部の応力は切り欠き半径により調整した。種々のクリープ疲労評価法により寿命評価を行うために有限要素法解析を実施するとともに、その予測寿命と試験寿命の比較検証を行った。クリープ疲労評価法としては応力再配分軌跡法(SRL法),弾性追従法,高速炉規格による方法等を採用した。これらの比較によりすべての試験結果に対してSRL法が最も適切な予測寿命を与えることが確認された。高速炉規格については繰り返し数で70倍以上安全側の評価を与えることが確認された。

論文

Unique Fermi surface and emergence of charge density wave in EuGa$$_4$$ and EuAl$$_4$$

仲村 愛*; 平仲 裕一*; 辺土 正人*; 仲間 隆男*; 三浦 泰直*; 堤 泰樹*; 森 晶宣*; 石田 一裕*; 三田村 勝哉*; 広瀬 雄介*; et al.

JPS Conference Proceedings (Internet), 3, p.011012_1 - 011012_6, 2014/06

Two europium compounds with the same structure EuGa$$_4$$ and EuAl$$_4$$ have been investigated. The Fermi surfaces revealed experimentally show a peculiar feature: flat Fermi surface sheets appear parallel to the tetragonal [110] planes. Reflecting this, a charge density wave transition due to the nesting of Fermi surface sheets has been observed in EuAl$$_4$$.

論文

Fermi surface and magnetic properties of antiferromagnet EuBi$$_3$$

仲村 愛*; 平仲 裕一*; 辺土 正人*; 仲間 隆男*; 立津 慶幸*; 眞榮平 孝裕*; 三浦 泰直*; 森 晶宣*; 堤 泰樹*; 広瀬 雄介*; et al.

Journal of the Physical Society of Japan, 82(12), p.124708_1 - 124708_6, 2013/12

 被引用回数:18 パーセンタイル:72.91(Physics, Multidisciplinary)

Fermi surfaces and magnetic properties of an antiferromagnet EuBi$$_3$$ were investigated on a flux-grown single crystal. A critical magnetic field of 225 kOe where the magnetic moments are forced to align ferromagnetically was well explained by the magnetic exchange interaction based on a two-sublattice model. The Fermi surface characteristics are in agreement with the theoretical prediction indicating a fully magnetic divalent state in Eu atoms.

論文

Magnetic and Fermi surface properties of EuGa$$_4$$

仲村 愛*; 平仲 裕一*; 辺土 正人*; 仲間 隆男*; 三浦 泰直*; 堤 泰樹*; 森 晶宣*; 石田 一裕*; 三田村 勝哉*; 広瀬 雄介*; et al.

Journal of the Physical Society of Japan, 82(10), p.104703_1 - 104703_10, 2013/10

 被引用回数:29 パーセンタイル:82(Physics, Multidisciplinary)

High quality single crystals of EuGa$$_4$$ have been grown from Ga flux. Electrical resistivity, magnetic susceptibility, high-field magnetization, specific heat, thermoelectric power and de Haas-van Alphen effect were investigated. Antiferromagnetic transition due to divalent Eu atoms were observed at 16.5 K. A charge density wave transition was also found under high pressure accompanied by a Fermi surface reconstruction. These observations were fully accounted for by the Fermi surface topology and corresponding band calculations.

論文

Proposal of assessment of structural integrity on severe accidents for JSFR

廣瀬 悠一*; 安藤 勝訓; 鬼澤 高志; 若井 隆純; 佐藤 健一郎*

Proceedings of 2013 International Congress on Advances in Nuclear Power Plants (ICAPP 2013) (USB Flash Drive), 6 Pages, 2013/04

JSFRのシビアアクシデント時において設計温度を超えた場合の構造健全性評価法について提案する。JSFRで想定するシビアアクシデント時の650度を超える超高温環境下において、ナトリウムバウンダリの健全性を担保することは、シビアアクシデントマネジメントの観点より重要となる。このため本件では冷却系設備の構造健全性評価法として、シビアアクシデント時のバウンダリ健全性評価手法とその評価に必要となる材料特性を得るための試験計画を提案する。

論文

Verification of the estimation methods of strain range in notched specimens made of Mod.9Cr-1Mo steel

安藤 勝訓; 廣瀬 悠一*; 伊達 新吾*; 渡邊 壮太*; 江沼 康弘*; 川崎 信史

Journal of Pressure Vessel Technology, 134(6), p.061403_1 - 061403_12, 2012/12

 被引用回数:5 パーセンタイル:27.83(Engineering, Mechanical)

2種類の改良9Cr-1Mo鋼切り欠き試験体の疲労試験を実施し、その試験結果と有限要素法解析に基づき評価されるひずみ範囲により算定される予測寿命を比較検討した。ひずみ範囲評価法としてはSRL法,SEF法,ノイバー則及び日本の高速炉規格で適用されている手法を採用し、比較検討の結果に基づき種々のひずみ範囲予測法に関して、その適用性や保守性について検討した。ひずみ範囲評価法としてはSRL法が最も合理的な評価を与える。一方でSRL法を規格として採用するためには適用範囲についての検討が必要であることが明らかとなった。

論文

Investigation of fission properties and evaporation residue measurement in the reactions using $$^{238}$$U target nucleus

西尾 勝久; 池添 博; Hofmann, S.*; Ackermann, D.*; Antalic, S.*; 有友 嘉浩; Comas, V. F.*; D$"u$llmann, Ch. E.*; Gorshkov, A.*; Graeger, R.*; et al.

EPJ Web of Conferences, 17, p.09005_1 - 09005_4, 2011/10

 被引用回数:1 パーセンタイル:48.7

Fission fragment mass distributions after full momentum transfer of the projectile were measured in the reactions using a $$^{238}$$U target nucleus bombarded by $$^{30}$$Si, $$^{31}$$P, $$^{34,36}$$S, $$^{40}$$Ar, $$^{40,48}$$Ca projectiles. We observed a strong variation of the distribution as function of bombarding energy. The results were interpreted by the effects of nuclear deformation of the target nucleus on the competition between fusion and quasifission. The symmetric fission includes fusion-fission, wheres as the asymmetric fission represents quasifission. The fusion probabilities were determined with the help of fluctuation-dissipation model. The estimated evaporation residue cross sections ($$^{263,264}$$Sg and $$^{267,268}$$Hs) produced in $$^{30}$$Si + $$^{238}$$U and $$^{34}$$S+$$^{238}$$U reproduced the experimental data.

論文

Comparison of creep-fatigue evaluation methods with notched specimens made of Mod.9Cr-1Mo steel

安藤 勝訓; 廣瀬 悠一*; 唐戸 孝典*; 渡邊 壮太*; 井上 修*; 川崎 信史; 江沼 康弘*

Proceedings of 2011 ASME Pressure Vessels and Piping Conference (PVP 2011) (CD-ROM), 11 Pages, 2011/07

To compare and evaluate these estimation methods, a series of creep-fatigue test was carried out with notched specimens. All the specimens were made of Mod.9Cr-1Mo steel. Deformation controlled creep-fatigue tests and temperature controlled creep-fatigue tests were performed and creep-fatigue lives, crack initiation and propagation processes were observed by digital micro-scope and replica method. A series of elastic Finite Element Analysis were carried out and number of cycles to failure was predicted by several creep-fatigue damage evaluation methods. Then these results were compared with test results. Four types of evaluation methods which are stress reduction locus method, simple elastic-follow up method, the method using conventional Neuber's rule and the methods described in JSME FBR design code were applied. In addition that, experimental based estimation were also compared.

論文

Nuclear orientation in the reaction $$^{34}$$S+$$^{238}$$U and synthesis of the new isotope $$^{268}$$Hs

西尾 勝久; Hofmann, S.*; He${ss}$berger, F. P.*; Ackermann, D.*; Antalic, S.*; 有友 嘉浩; Comas, V. F.*; D$"u$llmann, Ch. E.*; Gorshkov, A.*; Graeger, R.*; et al.

Physical Review C, 82(2), p.024611_1 - 024611_9, 2010/08

 被引用回数:72 パーセンタイル:96.12(Physics, Nuclear)

Synthesis of isotopes of the element hassium was studied using the reaction $$^{34}$$S+$$^{238}$$U$$rightarrow$$$$^{272}$$Hs*. At a kinetic energy of 163.0 MeV in the center of mass system we observed one $$alpha$$-decay chain starting at the isotope $$^{267}$$Hs. The cross-section was 1.8$$^{+4.2}_{-1.5}$$pb. At 152.0 MeV one decay of the new isotope $$^{268}$$Hs was observed. It decays with a half-life of 0.38$$^{+1.8}_{-0.17}$$s by 9479$$pm$$16 keV $$alpha$$-particle emission. Spontaneous fission of the daughter nucleus $$^{264}$$Sg was confirmed. The measured cross-section was 0.54$$^{+1.3}_{-0.45}$$pb. In-beam measurements of fission fragment mass distributions were performed to obtain information on the fusion probability at various orientation of the deformed target nucleus. The distributions changed from symmetry to asymmetry when the beam energy was changed from above-barrier to sub-barrier values, indicating orientation effects on fusion and/or quasifission. It was found that the distribution of symmetric mass fragments originates not only from fusion-fission, but has a strong component from quasifission. This result significantly influences the interpretation of data obtained from measurements of symmetric mass distributions with respect to extracting evaporation residue cross-sections.

論文

Verification of the prediction methods of strain range in notched specimens made of Mod.9Cr-1Mo

安藤 勝訓; 廣瀬 悠一*; 伊達 新吾*; 渡邊 壮太*; 江沼 康弘*; 川崎 信史

Proceedings of 2010 ASME Pressure Vessels and Piping Conference (PVP 2010) (CD-ROM), 11 Pages, 2010/07

高温における構造物のひずみ範囲予測法の妥当性を検証するため、切り欠き試験片による低サイクル疲労試験を実施した。試験はJSFRの冷却系機器・配管材として採用される予定の改良9Cr-1Mo鋼により実施し、疲労試験中のき裂の発生及び進展状況を観察した。この試験結果と有限要素法解析に基づくひずみ範囲予測法であるSRL法,弾性追従による予測法,ノイバー則による予測法及び既往の高温構造設計方針における評価法を比較し、その適用性等について述べる。

論文

Effects of nuclear orientation on fusion and fission process for reactions using uranium target nuclei

西尾 勝久; 池添 博; 光岡 真一; 西中 一朗; 牧井 宏之; 渡辺 裕*; 永目 諭一郎; 大槻 勤*; 廣瀬 健太郎*; Hofmann, S.*

AIP Conference Proceedings 1224, p.301 - 310, 2010/04

 被引用回数:5 パーセンタイル:85.67

Results on the measurements of (1) evaporation residue (ER) cross-sections for $$^{30}$$Si, $$^{34}$$S + $$^{238}$$U and of (2) fission fragment mass distributions for $$^{30}$$Si,$$^{34,36}$$S, $$^{40}$$Ar + $$^{238}$$U will be discussed. Measurement of ER cross-section was carried out at GSI by using the velocity filter SHIP. Measurement of fission fragment mass distributions was made by using the JAEA tandem accelerator. In the reaction $$^{30}$$Si + $$^{238}$$U, the ER cross-section for $$^{263}$$Sg(5n) suggested no fusion hindance at above-barrier energy, whereas the one for $$^{264}$$Sg(4n) suggested competition between fusion and quasi-fission at sub-barrier energy. This conclusion is consistent with the measured fragment mass distributions, where the asymmetric fission component associated with quasi-fission appears only at sub-barrier energies. In the reaction of $$^{34}$$S + $$^{238}$$U, the ER cross-sections for $$^{267}$$Hs(5n) and $$^{268}$$Hs(4n, new isotope) suggested fusion hindrance both for above- and sub-barrier energies. With the results of fission fragment mass distributions, it is found that quasi-fission has symmetric fission components when projectile mass is relatively large. We will also discuss the variation of the fragment mass distributions for $$^{30}$$Si,$$^{34,36}$$S, $$^{40}$$Ar + $$^{238}$$U.

論文

Effects of nuclear orientation on fusion and fission in the reaction using $$^{238}$$U target nucleus

西尾 勝久; 池添 博; 光岡 真一; 西中 一朗; 永目 諭一郎; 大槻 勤*; 廣瀬 健太郎*; Hofmann, S.*

EPJ Web of Conferences, 2, p.10001_1 - 10001_3, 2010/03

 被引用回数:1 パーセンタイル:49.12

We have measured the (1) evaporation residue (ER) cross-sections for $$^{30}$$Si, $$^{34}$$S + $$^{238}$$U and (2) fission fragment mass distributions for $$^{30}$$Si,$$^{34,36}$$S, $$^{40}$$Ar. Measurement of ER cross-section was carried out at GSI by using the velocity filter SHIP. Measurement of fission fragment mass distribution was made by using the JAEA tandem accelerator. In the reaction $$^{30}$$Si + $$^{238}$$U, the ER cross-section for $$^{263}$$Sg(5n) suggested no fusion hindrance at above-barrier energy, whereas the one for $$^{264}$$Sg(4n) suggested competition between fusion and fission at sub-barrier energy. This conclusion is consistent with the measured fragment mass distributions, where the asymmetric fission component associated with quasi-fission appears only at sub-barrier energies. In the reaction of $$^{34}$$S + $$^{238}$$U, the ER cross-sections for $$^{267}$$Hs(5n) and $$^{268}$$Hs(4n, new isotope) suggested fusion hindrance both for above- and sub-barrier energies. With the results of fission fragment mass distributions, it is found that quasi-fission has symmetric fission components when projectile mass is relatively large. We will also discuss the variation of the fragment mass distributions for $$^{30}$$Si,$$^{34,36}$$S, $$^{40}$$Ar + $$^{238}$$U.

論文

Effects of nuclear orientation on fission fragment mass distributions in the reactions using actinide target nuclei

西尾 勝久; 池添 博; 光岡 真一; 西中 一朗; 牧井 宏之; 渡辺 裕*; 永目 諭一郎; 大槻 勤*; 廣瀬 健太郎*; Hofmann, S.*

AIP Conference Proceedings 1175, p.111 - 118, 2009/10

Fission fragment properties for the reactions involving actinide target nuclei have been investigated at the JAEA tandem facility. The results showed firstly the appearance of new fission channels. The experimental data are useful for the theoretical study to produce super heavy elements. Also the new fission channels suggested the possible production of the neutron rich nuclei by taking advantage of the new fission channels.

論文

Effects of nuclear orientation on fission fragment mass distributions in the reactions using actinide target nuclei

西尾 勝久; 池添 博; 光岡 真一; 西中 一朗; 牧井 宏之; 渡辺 裕*; 永目 諭一郎; 大槻 勤*; 廣瀬 健太郎*; Hofmann, S.*

AIP Conference Proceedings 1175, p.111 - 118, 2009/10

The influence of nuclear deformation of $$^{238}$$U target nucleus on fusion and fission process was investigated. The study was motivated by larger cross-sections to produce super-heavy nuclei in reactions using actinide target nuclei, compared to those using lead or bismuth target nuclei. We have measured fission fragment mass distributions in the reaction of $$^{30}$$Si,$$^{31}$$P,$$^{34,36}$$S,$$^{40}$$Ar + $$^{238}$$U at JAEA tandem facility. We observed strong variation of the distributions on bombarding energy of projectiles, which indicates that competition between fusion and fission is sensitive to the colliding angle of the projectile to the symmetric axis of $$^{238}$$U. We also measured the evaporation residue cross-sections for $$^{30}$$Si+$$^{238}$$U and $$^{34}$$S+$$^{238}$$U as a direct evidence for fusion. The experiment was carried out at GSI. The results showed that fusion is much hindered in the subbarrier energy, where projectile collides only on the pollar side of the $$^{238}$$U nucleus, whereas the equatorial collision has smaller fusion hindrance. These results indicate that the initial touching configuration influence the subsequent reaction process.

論文

Effects of nuclear orientation on fusion and fission process in heavy ion reactions

西尾 勝久; 池添 博; 光岡 真一; 西中 一朗; 渡辺 裕*; 永目 諭一郎; 大槻 勤*; 廣瀬 健太郎*; Hofmann, S.*

AIP Conference Proceedings 1120 (Internet), p.275 - 279, 2009/05

Effects of nuclear deformation of $$^{238}$$U on fusion and fission was investigated in the reactions of $$^{30}$$Si+$$^{238}$$U and $$^{36}$$S + $$^{238}$$U. From the measurement of evaporation residue cross-sections for $$^{30}$$Si+$$^{238}$$U, carried out at GSI, it is concluded that in the sub-barrier region competition between fusion and quasi-fission was suggested whereas at the above barrier region fusion is the main process after the system is captured inside the Coulomb barrier. The fission fragment mass distributions were measured in $$^{30}$$Si+$$^{238}$$U and $$^{36}$$S+$$^{238}$$U at the JAEA tandem facility. Symmetric fission was observed at the above-barrier region, showing the fusion-fission character. In decreasing the energy to the sub-barrier, the asymmetric fission starts to dominate, showing the signature of quasi-fission. The results suggest that the equatorial collision results in fusion whereas the polar collision results in quasi-fission.

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