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論文

Application of energy-resolving neutron imaging to major-component analyses of materials using four-channel superconducting detector

Vu, TheDang*; 宍戸 寛明*; 相澤 一也; 奥 隆之; 及川 健一; 原田 正英; 小嶋 健児*; 宮嶋 茂之*; 曽山 和彦; 小山 富男*; et al.

IEEJ Transactions on Electrical and Electronic Engineering, 19(11), p.1888 - 1894, 2024/11

 被引用回数:0 パーセンタイル:0.00(Engineering, Electrical & Electronic)

We proposed a novel superconducting detector called the current-biased kinetic inductance detector (CB-KID) for constructing a neutron transmission imager. We systematically studied the characteristics of the CB-KID to improve spatial resolution down to 10 $$mu$$m in transmission imaging. By analyzing neutron transmission spectra from 1 meV to 500 keV, we identified copper (Cu) and iron (Fe) as major components in commercial nuts and screws. Additionally, we successfully mapped the distribution of the SmSn$$_{3}$$ compound using selective energy regions of pulsed neutrons and the CB-KID detector. It can reveal transmission spectra across a wide range of energies, from cold-neutron energies (meV) to higher neutron energies (up to 500 keV).

論文

Neutron transmission imaging system with a superconducting kinetic inductance detector

Vu, TheDang*; 宍戸 寛明*; 相澤 一也; 奥 隆之; 及川 健一; 原田 正英; 小嶋 健児*; 宮嶋 茂之*; 曽山 和彦; 小山 富男*; et al.

Journal of Physics; Conference Series, 2776, p.012009_1 - 012009_9, 2024/06

We optimized the design and operating conditions of our superconducting neutron detector to improve spatial resolution. We obtained the best spatial resolution of 10 $$mu$$m when a Gd Siemens star pattern was mounted at close contact with the detector in the cryostat. We compared the effect of a different sample-detector distance on a spatial resolution when the samples were placed either at cryogenic temperature or at room temperature. We found the appearance of clear Bragg dips by the measurements of natural FeS$$_{2}$$ single crystals and succeeded in mapping the distribution of differently-oriented crystals by choosing several Bragg dips of the FeS$$_{2}$$ crystals to compose the transmission images.

論文

Neutron transmission CB-KID imager using samples placed at room temperature

石田 武和*; Vu, TheDang*; 宍戸 寛明*; 相澤 一也; 奥 隆之; 及川 健一; 原田 正英; 小嶋 健児*; 宮嶋 茂之*; 小山 富男*; et al.

Journal of Low Temperature Physics, 214(3-4), p.152 - 157, 2024/02

 被引用回数:0 パーセンタイル:0.00(Physics, Applied)

We built a new cryostat to apply a current-biased kinetic inductance detector (CB-KID) for conducting neutron transmission imaging of room temperature samples under pulsed neutrons. A Wood's metal alloy of melting temperature 75.2$$^{circ}$$C was placed at room temperature to inspect the measurement system at J-PARC. Since one of the four phases of Wood's metal is a fine Cd-rich needle phase (width $$sim$$ 25 $$mu$$m and length $$sim$$ 5 mm), it is suitable for observing fine mosaic structure selectively by neutron imaging. The spatial resolution of the CB-KID imager was estimated as $$sim$$ 10 $$mu$$m by using a Gd Siemens-star pattern. The CB-KID system is useful to conduct transmission imaging for various materials rather easily at room temperature.

論文

Orientation mapping of YbSn$$_{3}$$ single crystals based on Bragg-dip analysis using a delay-line superconducting sensor

宍戸 寛明*; Vu, TheDang*; 相澤 一也; 小嶋 健児*; 小山 富男*; 及川 健一; 原田 正英; 奥 隆之; 曽山 和彦; 宮嶋 茂之*; et al.

Journal of Applied Crystallography, 56(4), p.1108 - 1113, 2023/08

 被引用回数:1 パーセンタイル:37.25(Chemistry, Multidisciplinary)

Recent progress in high-power pulsed neutron sources has stimulated the development of the Bragg dip and Bragg edge analysis methods using a two-dimensional neutron detector with high temporal resolution to resolve the neutron energy by the time-of-flight method. A delay-line current-biased kinetic inductance detector (CB-KID) is a two-dimensional superconducting sensor with a high temporal resolution and multi-hit capability. Here, it is demonstrated that a delay-line CB-KID with a $$^{10}$$B neutron conversion layer can be applied to high-spatial-resolution neutron transmission imaging and spectroscopy up to 100 eV. Dip structures are observed in the transmission spectra of YbSn$$_{3}$$ single crystals, induced by Bragg diffraction and nuclear resonance absorption. The orientation mapping of YbSn$$_{3}$$ crystals is successfully drawn based on the analysis of observed Bragg dip positions in the transmission spectra.

論文

High spatial resolution neutron transmission imaging using a superconducting two-dimensional detector

宍戸 寛明*; 西村 和真*; Vu, TheDang*; 相澤 一也; 小嶋 健児*; 小山 富男*; 及川 健一; 原田 正英; 奥 隆之; 曽山 和彦; et al.

IEEE Transactions on Applied Superconductivity, 31(9), p.2400505_1 - 2400505_5, 2021/12

 被引用回数:0 パーセンタイル:0.00(Engineering, Electrical & Electronic)

中性子イメージングは、重金属に対する高透過性、軽元素に対する高感度、同位体と中性子との特異な核反応による同位体選択性などの中性子ビームの特徴を活かした非破壊検査の有力な手段の一つである。本研究では、超伝導検出器である電流バイアス運動インダクタンス検出器(CB-KID)を用いて、パルス中性子源を用いた飛行時間法による波長分解中性子イメージングを行った。遅延時間型CB-KIDを用いて、GdAl$$_{3}$$単結晶を成長させたGd-Al合金試料の中性子透過像を取得した。その結果、単結晶はAl-Gd合金全体に渡って、形状,分布ともに良好に観察することができた。また、中性子の波長0.03nm以上でGdによる特徴的な中性子の吸収を確認した。さらに、15$$mu$$m$$ times$$ 12$$mu$$mという限られた検出面で、同位体と中性子の核反応によって生じる$$^{155}$$Gd共鳴ディップを観測することができた。また、$$^{155}$$Gdの共鳴ディップを用いてGd選択的イメージングを行ったところ、中性子の波長幅が1pmという限られた範囲で、明確なGd核の元素選択イメージング像を取得することに成功した。

論文

Practical tests of neutron transmission imaging with a superconducting kinetic-inductance sensor

Vu, TheDang; 宍戸 寛明*; 相澤 一也; 小嶋 健児*; 小山 富男*; 及川 健一; 原田 正英; 奥 隆之; 曽山 和彦; 宮嶋 茂之*; et al.

Nuclear Instruments and Methods in Physics Research A, 1006, p.165411_1 - 165411_8, 2021/08

 被引用回数:1 パーセンタイル:15.62(Instruments & Instrumentation)

We found that the sizes of the Gd islands determined from the transmission image correlated strongly with those determined from the SEM image. We demonstrated the CB-KID could be used to identify (1) tiny voids in a thermally sprayed continuous Gd$$_2$$O$$_3$$ film in and (2) various mosaic morphologies and different eutectic microstructures in Wood's metal samples. The fact that the CB-KID system could be used to identify features of samples with a wide distribution of sizes and thicknesses is promising for real application of the device for imaging samples of interest to material scientists. Operating the CB-KID at higher temperatures appreciably improved the efficiency for simultaneously identifying the X and Y positions of hotspots. We also compared the detection efficiency with the PHITS simulations. We now plan to improve the detection efficiency by increasing the thickness of the $$^{10}$$B neutron conversion layer

論文

Homogeneity of neutron transmission imaging over a large sensitive area with a four-channel superconducting detector

Vu, TheDang; 宍戸 寛明*; 小嶋 健児*; 小山 富男*; 及川 健一; 原田 正英; 宮嶋 茂之*; 奥 隆之; 曽山 和彦; 相澤 一也; et al.

Superconductor Science and Technology, 34(1), p.015010_1 - 015010_10, 2021/01

 被引用回数:4 パーセンタイル:29.17(Physics, Applied)

We demonstrated that a four-readout superconducting neutron imaging system shows good spatial heterogeneity and linearity using the delay-line method. We examined the precise pattern of a $$^{10}$$B-dot-array absorber and found the X-direction pitch (Px) = 250.7 um with a scatter of (Hx)= 5.4 um and the Y-direction pitch (Py)= 249.1 um with a scatter of (Hy)= 3.4 um while the $$^{10}$$B dot array was fully extended toward the X direction across the detector sensitive area. We consider that this demonstrates detection with good spatial homogeneity and conclude. The transmission-imaging system is suitable for use at pulsed neutron facilities. We also reported a clear transmission image of tiny screws and nuts, and ladybug (insect). We recognize that further efforts to improve the detection efficiency are necessary to make using the detector more practical.

論文

Energy-resolved neutron imaging using a delay line current-biased kinetic-inductance detector

宍戸 寛明*; 西村 和真*; Vu, TheDang*; 小嶋 健児*; 小山 富男*; 及川 健一; 原田 正英; 宮嶋 茂之*; 日高 睦夫*; 奥 隆之; et al.

Journal of Physics; Conference Series, 1590, p.012033_1 - 012033_8, 2020/10

 被引用回数:0 パーセンタイル:0.00(Engineering, Electrical & Electronic)

We demonstrate the development of an energy resolved neutron transmission imaging system via a solid-state superconducting detector, called current-biased kinetic-inductance detector (CB-KID). CB-KIDs comprise X and Y superconducting Nb meanderlines with Nb ground plane and a $$^{10}$$B conversion layer, which converts a neutron to two charged particles. CB-KID uses the delay-line method, and allows us to reconstruct the two-dimensional neutron transmission image of a test sample with four signal readout lines. We examined the capability of high spatial and energy (wavelength) resolved neutron transmission imaging over the sensor active area of 15 $$times$$ 15 mm$$^{2}$$ for various samples, including biological and metal ones. We also demonstrated the capability for the Bragg edge transmission and an energy-resolved neutron image in which stainless-steel specimens were discriminating from other specimens.

論文

Kinetic inductance neutron detector operated at near critical temperature

Vu, TheDang; 西村 和真*; 宍戸 寛明*; 原田 正英; 及川 健一; 宮嶋 茂之*; 日高 睦夫*; 奥 隆之; 曽山 和彦; 相澤 一也; et al.

Journal of Physics; Conference Series, 1590, p.012036_1 - 012036_9, 2020/07

 被引用回数:1 パーセンタイル:64.95(Engineering, Electrical & Electronic)

Our CB-KID neutron imager detects high spatial resolution neutrons transmission images by using a delay-line technique. We found that the number of events was remarkably increased with increasing the detector temperature until close to the critical temperature Tc. We investigated the properties of CB-KID at near Tc. We observed systematic changes of neutron signals as a function of the detector temperature from 4 K to Tc. The simulations modeled the sequential physical processes for $$^{10}$$B(n,$$alpha$$)$$^{7}$$Li reactions and energy deposition by particles within CB-KID, including neutrons, $$^{4}$$He particles, $$^{7}$$Li particles, photon and electron transport.

論文

Energy-resolved neutron imaging with high spatial resolution using a superconducting delay-line kinetic inductance detector

飯澤 侑貴*; 宍戸 寛明*; 西村 和真*; Vu, TheDang*; 小嶋 健児*; 小山 富男*; 及川 健一; 原田 正英; 宮嶋 茂之*; 日高 睦夫*; et al.

Superconductor Science and Technology, 32(12), p.125009_1 - 125009_8, 2019/12

 被引用回数:14 パーセンタイル:57.59(Physics, Applied)

Neutron imaging is one of the key technologies for non-destructive transmission testing. Recent progress in the development of intensive neutron sources allows us to perform energy-resolved neutron imaging with high spatial resolution. We have been developing a neutron imager aiming at conducting high spatial and temporal resolution imaging based on a delay-line neutron detector, called the current-biased kinetic-inductance detector, with a conversion layer $$^{10}$$B. The detector allowed us to obtain a neutron transmission image with four signal readout lines. Herein, we expanded the sensor active area, and improved the spatial resolution of the detector. We examined the capability of high spatial resolution neutron imaging over the sensor active area of 15 $$times$$ 15 mm$$^{2}$$ for various samples, including biological and metal ones. We also demonstrated an energy-resolved neutron image in which stainless-steel specimens were discriminating of other specimens with the aid of the Bragg edge transmission.

論文

Temperature dependent characteristics of neutron signals from a current-biased Nb nanowire detector with $$^{10}$$B converter

Vu, TheDang; 飯澤 侑貴*; 西村 和真*; 宍戸 寛明*; 小嶋 健児*; 及川 健一; 原田 正英; 宮嶋 茂之*; 日高 睦夫*; 奥 隆之; et al.

Journal of Physics; Conference Series, 1293, p.012051_1 - 012051_9, 2019/10

 被引用回数:6 パーセンタイル:94.28(Materials Science, Multidisciplinary)

We succeeded in designed and fabricated a neutron detector by using a superconducting current-biased kinetic inductance detector (CB-KID), which is constructed by two perpendicular Nb-based superconducting meander-lines and an enriched $$^{10}$$B neutron conversion layer. We rebuilt completely a neutron image of a $$^{10}$$B dot array contain in the stainless-steel mesh. To improve the resolution of neutron images, the characteristics of a superconducting neutron detector have been studied carefully. In this study, we present the dependence of neutron signals in the temperature of detector. We found that when the temperature of a neutron detector is as close as the critical temperature of superconductivity, the intensity of signal increase as a function of temperature. We consider that the ratio of noise and signal is decrease which is very useful to improve the resolution of neutron images.

論文

Multiple-wavelength neutron holography with pulsed neutrons

林 好一*; 大山 研司*; 八方 直久*; 松下 智裕*; 細川 伸也*; 原田 正英; 稲村 泰弘; 仁谷 浩明*; 宍戸 統悦*; 湯葢 邦夫*

Science Advances (Internet), 3(8), p.e1700294_1 - e1700294_7, 2017/08

Local structures around impurities in solids provide important information for understanding the mechanisms of material functions, because most of them are controlled by dopants. For this purpose, the X-ray absorption fine structure method, which provides radial distribution functions around specific elements, is most widely used. However, a similar method using neutron techniques has not yet been developed. If one can establish a method of local structural analysis with neutrons, then a new frontier of materials science can be explored owing to the specific nature of neutron scattering-that is, its high sensitivity to light elements and magnetic moments. Multiple-wavelength neutron holography using the time-of-flight technique with pulsed neutrons has great potential to realize this. We demonstrated multiple-wavelength neutron holography using a Eu-doped CaF$$_{2}$$ single crystal and obtained a clear three-dimensional atomic image around trivalent Eu substituted for divalent Ca, revealing an interesting feature of the local structure that allows it to maintain charge neutrality. The new holography technique is expected to provide new information on local structures using the neutron technique.

論文

Neutron flux spectrum revealed by Nb-based current-biased kinetic inductance detector with a $$^{10}$$B conversion layer

宮嶋 茂之*; 宍戸 寛明*; 鳴神 吉人*; 吉岡 直人*; 藤巻 朗*; 日高 睦夫*; 及川 健一; 原田 正英; 奥 隆之; 新井 正敏*; et al.

Nuclear Instruments and Methods in Physics Research A, 842, p.71 - 75, 2017/01

 被引用回数:13 パーセンタイル:75.48(Instruments & Instrumentation)

We successfully derived the time-dependent flux of pulsed neutrons using a superconducting Nb-based current biased kinetic inductance detector (CB-KID) with a $$^{10}$$B conversion layer at Japan Proton Accelerator Research Complex. Our CB-KID is a meander line made of a 40-nm-thick Nb thin film with 1-$$mu$$m line width, which is covered with a 150-nm-thick $$^{10}$$B conversion layer. The detector works at a temperature below 4 K. The evaluated detection efficiency of the CB-KID in this experiment is 0.23% at the neutron energy of 25.4 meV. The time-dependent flux spectra of pulsed neutrons thus obtained are in good agreement with the results obtained by the Monte Carlo simulations.

論文

Cyclotron resonance study of quasiparticle mass and scattering rate in the hidden-order and superconducting phases of URu$$_2$$Si$$_2$$

利根川 翔*; 橋本 顕一郎*; 井加田 洸輔*; 鶴原 悠悟*; Lin, Y.-H.*; 宍戸 寛明*; 芳賀 芳範; 松田 達磨; 山本 悦嗣; 大貫 惇睦; et al.

Physical Review B, 88(24), p.245131_1 - 245131_13, 2013/12

 被引用回数:12 パーセンタイル:47.67(Materials Science, Multidisciplinary)

Detailed analyses of the cyclotron resonance lines in a uranium compound URu$$_2$$Si$$_2$$ are reported. The analyses of the resonance profiles reveals that the heavier branch of the split line has a larger scattering rate, providing evidence for the existence of hot-spot along the [110] direction. The result is consistent with the broken fourfold symmetry in the hidden-order phase.

論文

Cyclotron resonance in the hidden-order phase of URu$$_2$$Si$$_2$$

利根川 翔*; 橋本 顕一郎*; 井加田 洸輔*; Lin, Y.-H.*; 宍戸 寛明*; 芳賀 芳範; 松田 達磨; 山本 悦嗣; 大貫 惇睦; 池田 浩章*; et al.

Physical Review Letters, 109(3), p.036401_1 - 036401_5, 2012/07

 被引用回数:53 パーセンタイル:87.04(Physics, Multidisciplinary)

First observation of cyclotron resonance in the hidden-order phase of ultra clean URu$$_2$$Si$$_2$$ is reported. An anomalous splitting of the sharpest resonance line under in-plane magnetic field rotation was found. This is most naturally explained by the domain formation, which breaks the fourfold rotational symmetry of the underlying tetragonal lattice. The result is consistent with the "nematic" Fermi liquid state, in which itinerant electrons have unidirectional correlations.

論文

Anomalous low-field diamagnetic response in ultraclean URu$$_2$$Si$$_2$$ superconductor

岡崎 竜二*; 下澤 雅明*; 宍戸 寛明*; Konczykowski, M.*; 芳賀 芳範; 松田 達磨; 山本 悦嗣; 大貫 惇睦; 柳瀬 陽一*; 芝内 孝禎*; et al.

Journal of Physics; Conference Series, 273, p.012081_1 - 012081_4, 2011/02

 被引用回数:3 パーセンタイル:62.16(Physics, Condensed Matter)

The low critical field $$H_{rm c1}$$ in ultraclean URu$$_2$$Si$$_2$$ single crystals with residual resistivity ration exceeding 700 is precisely determined. The whole $$H_{rm c1}$$ for $$H parallel a$$ can be explained by the two-gap with line and point nodes. In contrast, for $$H parallel c$$ a distinct kink in the slope of $$H_{rm c1}$$ was found at 1.2 K, which cannot be accounted for by the two-gap. This outstanding anomaly demonstrates a highly unusual superconducting state embedded in the hidden order state possibly related to the time reversal symmetry breaking.

論文

Lower critical fields and the anisotropy in PrFeAsO$$_{1-y}$$ single crystals

岡崎 竜二*; Konczykowski, M.*; Van der Beek, C. J.*; 加藤 智成*; 橋本 顕一郎*; 下澤 雅明*; 宍戸 寛明*; 山下 穣*; 石角 元志; 鬼頭 聖*; et al.

Physica C, 470(Suppl.1), p.S485 - S486, 2010/12

 被引用回数:0 パーセンタイル:0.00(Physics, Applied)

鉄系オキシニクタイドPrFeAsO$$_{1-y}$$単結晶における$$H$$ $$parallel$$ $$c$$$$H$$ $$parallel$$ $$ab$$-planesのより下部臨界磁場$$H_{c1}$$を報告する。磁束ピン止めによって$$H_{c1}$$決定の困難さを回避することで、センサーの位置ごとの局所の磁気誘導を評価できる小型のホールセンサーアレイを使った新方式を開発した。結晶の縁に置かれたホールセンサーは、マイスナーの状態から最初の磁束侵入を明瞭に解明した。$$H$$ $$parallel$$ $$c$$による$$H_{c1}$$の温度依存性は、面内侵入の深さによって計測され、完全ギャップの超伝導状態と一致する。低温での$$H_{c1}$$の異方性は$$sim$$3であると評価され、それは$$H_{c2}$$よりさらに小さいものである。これは、マルチバンド超伝導性を意味し、超伝導性のアクティヴバンドはより二次元的である。

論文

Disorder and flux pinning in superconducting pnictide single crystals

Van der Beek, C. J.*; Rizza, G.*; Konczykowski, M.*; Fertey, P.*; Monnet, I.*; 岡崎 竜二*; 加藤 智成*; 橋本 顕一郎*; 下澤 雅明*; 宍戸 寛明*; et al.

Physica C, 470(Suppl.1), p.S385 - S386, 2010/12

 被引用回数:1 パーセンタイル:6.06(Physics, Applied)

ニクタイド超伝導体PrFeAsO$$_{1-x}$$中の結晶の乱れが、磁束の新入の磁気光学可視化,透過型電子顕微鏡,放射光X線回折を用いて調べられた。磁束分布の臨界状態,臨界電流の大きさと温度依存性が、すべての温度で酸素欠陥によるバルクの磁束ピン止めを示す。

論文

Fermi surface properties of ferromagnet UCu$$_2$$Si$$_2$$

松田 達磨; 池田 修悟*; 山本 悦嗣; 芳賀 芳範; 宍戸 寛明*; 山上 浩志; 摂待 力生*; 大貫 惇睦

Journal of the Physical Society of Japan, 79(11), p.114712_1 - 114712_4, 2010/11

 被引用回数:4 パーセンタイル:32.46(Physics, Multidisciplinary)

Snフラックス法により正方晶UCu$$_2$$Si$$_2$$の単結晶育成及びドハース・ファンアルフェン効果測定に成功した。UCu$$_2$$Si$$_2$$は、温度106K以下において反強磁性転移し、続く100K以下において強磁性転移する。この強磁性状態において、5$$times$$10$$^6$$から7$$times$$10$$^7$$ Oeのドハース・ファンアルフェンシグナルを観測した。それぞれに対応するサイクロトロン有効質量は、1.4から4.2$$m_0$$で、電子比熱係数の値$$gamma=$$20mJ/K$$^2cdot$$molと矛盾がない。これらの実験結果は、5$$f$$電子を遍歴とした、スピン及び軌道分極モデルでおおまかに説明される。

論文

Exotic superconducting state embedded in the hidden order state of URu$$_2$$Si$$_2$$

松田 祐司*; 岡崎 竜二*; 笠原 裕一*; 宍戸 寛明*; 芝内 孝禎*; 芳賀 芳範; 松田 達磨; 大貫 惇睦

Physica C, 470(20), p.1013 - 1017, 2010/11

 被引用回数:1 パーセンタイル:6.06(Physics, Applied)

We report charge and thermal transport measurements on ultra clean single crystals of the superconductor with the hidden-order state URu$$_2$$Si$$_2$$. The results provide strong evidence for a new type of unconventional superconductivity with two distinct gaps having different nodal topology. We propose a gap function with chiral $$d$$-wave form. We also demonstrate that a distinct flux line lattice melting transition with outstanding characters occurs well below the upper critical fields even at sub-Kelvin temperature.

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