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論文

The $$^{59}$$Fe(n,$$gamma$$)$$^{60}$$Fe cross section from the surrogate ratio method and its effect on the $$^{60}$$Fe nucleosynthesis

Yan, S. Q.*; Li, X. Y.*; 西尾 勝久; Lugaro, M.*; Li, Z. H.*; 牧井 宏之; Pignatari, M.*; Wang, Y. B.*; Orlandi, R.; 廣瀬 健太郎; et al.

Astrophysical Journal, 919(2), p.84_1 - 84_7, 2021/10

https://doi.org/10.3847/1538-4357/ac12ce
 被引用回数：0

The long-lived $$^{60}$$Fe (with a half-life of 2.62 Myr) is a crucial diagnostic of active nucleosynthesis in the Milky Way galaxy and in supernovae near the solar system. The neutron-capture reaction $$^{59}$$Fe(n,$$gamma$$)$$^{60}$$Fe on $$^{59}$$Fe (half-life=44.5 days) is the key reaction for the production of $$^{60}$$Fe in massive stars. This reaction cross section has been previously constrained by the Coulomb dissociation experiment, which offered partial constraint on the E1 $$gamma$$-ray strength function but a negligible constraint on the M1 and E2 components. In this work, for the first time, we use the surrogate ratio method to experimentally determine the $$^{59}$$Fe(n,$$gamma$$)$$^{60}$$Fe cross sections in which all the components are included. We derived a Maxwellian-averaged cross section of 27.5$$pm$$3.5 mb at $$kT$$ = 30 keV and 13.4$$pm$$1.7 mb at $$kT$$ = 90 keV, roughly 10%-20% higher than previous estimates. We analyzed the impact of our new reaction rates in nucleosynthesis models of massive stars and found that uncertainties in the production of $$^{60}$$Fe from the $$^{59}$$Fe(n,$$gamma$$)$$^{60}$$Fe rate are at most 25$$%$$. We conclude that stellar physics uncertainties now play a major role in the accurate evaluation of the stellar production of $$^{60}$$Fe.

論文

Anisotropic thermal lattice expansion and crystallographic structure of strontium aluminide within Al-10Sr alloy as measured by in-situ neutron diffraction

Liss, K.-D.*; Harjo, S.; 川崎 卓郎; 相澤 一也; 徐 平光

Journal of Alloys and Compounds, 869, p.159232_1 - 159232_9, 2021/07

https://doi.org/10.1016/j.jallcom.2021.159232
 被引用回数：0 パーセンタイル：0(Chemistry, Physical)

The aluminium strontium master alloy Al-10Sr has been investigated by in-situ neutron diffraction upon a heating-cooling cycle, revealing composition, crystallographic structure, lattice evolution and linear thermal expansion coefficients. Expansion of the Al matrix between (23.5 ... 26.7)$$times$$10$$^{-6}$$ K$$^{-1}$$ depends on temperature and fits well to the literature values, extrapolating to higher temperature at 800 K. Thermal expansion is highly anisotropic for tetragonal Al$$_{4}$$Sr by a factor of 1.86 with values of 20.8 and 11.1$$times$$10$$^{-6}$$ K$$^{-1}$$ in ${it a}$ and ${it c}$-axis. The even large discrepancy to the Al matrix is prone to residual intergranular phase stresses, explaining the brittleness of such composite material. Upon first heating, recovery of the initially plastically deformed materials is observed until 600 K and 700 K, for Al$$_{4}$$Sr and Al. Rietveld analysis refines the 4${it e}$ Wyckoff positions of the ${it I}$ 4/${it m m m}$ crystal structure to ${it z}$ = 0.39 revealing that local tetrahedrons are regular while local hexagons are stretched, in contrast to the literature. Its lattice parameters report to $$a_{rm I}$$ = 4.44240(48) ${AA}$, $$c_{rm I}$$ = 11.0836(15) ${AA}$ at 300 K. Furthermore, the manuscript demonstrates full technical analysis of the neutron data. Findings feed into data bases and an outlook for improving mechanical properties of Al$$_{4}$$Sr composites is given.

論文

Multiple wavelengths texture measurement using angle dispersive neutron diffraction at WOMBAT

徐 平光; Liss, K.-D.*

Quantum Beam Science (Internet), 5(2), p.11_1 - 11_14, 2021/06

https://doi.org/10.3390/qubs5020011

In contrast to conventional angle dispersive neutron diffractometers with a single-tube detector or a small-size linear position-sensitive detector, the WOMBAT diffractometer at Australian Nuclear Science and Technology Organisation (ANSTO) is equipped with a large-area curved position-sensitive detector, spanning 120$$^{circ}$$ for the scattering angle 2$$theta$$ and 15$$^{circ}$$ for the azimuth ${it $eta$}$, respectively. Here, WOMBAT was employed to establish a texture measurement environment for complex textured samples, through measuring neutron diffractograms at two selected wavelengths on a typical reference sample of martensite-austenite multilayered steel sheet. All neutron patterns were simultaneously Rietveld analyzed using the software, Materials Analysis Using Diffraction (MAUD). The shorter wavelength enabled to collect the martensite diffraction peaks 110, 200, 211, 220, 310, 222 as well as the austenite diffraction peaks 111, 200, 220, 311, 222, 331 diffraction peaks simultaneously by pre-setting the detector range to 2$$theta$$ = 30$$sim$$150$$^{circ}$$. The longer wavelength enabled to separate the overlapping strong martensite peak 110 and austenite peak 111 more reliably. Moreover, the detector panel division along the vertical direction covers a good stereographic coverage in the azimuthal angle. Such combination of multiple wavelength neutron diffraction combined with simultaneous Rietveld texture analysis was confirmed much valuable to realize high precision measurements for complex textured samples at an orientation distribution function (ODF) graticule of 5$$^{circ}$$, and in a much shorter beam time than the conventional angle dispersive method.

論文

小型加速器中性子源RANSを使用した鋼材特性の分析技術開発; ものづくり現場で中性子線を使った材料分析が可能に

徐 平光; 高村 正人*; 岩本 ちひろ*; 箱山 智之*; 大竹 淑恵*; 鈴木 裕士

Isotope News, (774), p.7 - 10, 2021/04

https://www.jrias.or.jp/books/cat3/2021/774.html

近年、地球温暖化対策として、自動車などの軽量化に求められている中、高張力鋼板の成形性向上は重要な開発課題となっている。破断まで優れた伸び特性を持たせた高張力鋼板の開発には、オーステナイト組織の相分率と各構成相の集合組織を正しく制御することは極めて重要である。透過能に優れた中性子回折法は、鋼材内部の結晶情報をバルク平均で得られる特徴を持つことから、相分率と集合組織を測定する上で有力な手段である。しかし、現状では中性子回折測定が可能な中性子源は、研究用原子炉や大型加速器施設などの大型実験施設に限られ、これらは共用施設のため利用者が頻繁に測定する機会を得ることは困難である。そこで、理化学研究所では、大学や企業の研究室、工場などの現場で手軽に使える小型中性子源として「理研小型加速器中性子源RANS」を構築し、日本原子力研究開発機構と協力しながら鋼材特性の分析技術に関する一連の研究開発を進めてきた。本解説論文では、大型実験施設と比べるとビーム強度の低い小型加速器中性子源を用いて実施した、中性子回折法による相分率と集合組織測定に関する共同研究成果と、今後の展望を紹介する。

論文

In-house texture measurement using a compact neutron source

徐 平光; 池田 義雅*; 箱山 智之*; 高村 正人*; 大竹 淑恵*; 鈴木 裕士

Journal of Applied Crystallography, 53(2), p.444 - 454, 2020/04

AA2019-0242.pdf:2.9MB

https://doi.org/10.1107/S1600576720002551
 被引用回数：2 パーセンタイル：37.3(Chemistry, Multidisciplinary)

In order to improve the instrumental accessibility of neutron diffraction technique, the emerging compact neutron sources and in-house neutron diffractometers as a good complementary way have caused wide attention while their analysis precision seems problematic for the practical application. As a challenging project, the RIKEN accelerator-driven compact neutron source (RANS) was employed to establish the technical environment for texture measurement, and the recalculated pole figures and the orientation distribution function (ODF) of an interstitial-free (IF) steel sheet obtained from RANS were compared with the results from another two neutron diffractometers well-established for texture measurement. Moreover, the parameter "square integration of ODF difference" originally for evaluating the numerical error between the measured and simulated textures was generalized here to examine the reliability of RANS texture measurement. These quantitative comparisons revealed that the precise neutron diffraction texture measurement at RANS has been realized successfully and the following technical optimizations are much valuable, including the thickness selection of polyethylene moderator, the sample-to-detector distance, the B$$_{4}$$C shielding sheets for the reduced background noise, and the fine region division of the neutron detector panel. Moreover, the Rietveld texture analysis improves the texture reliability through avoiding the unfavorable influence of the uncertain diffraction intensity involved in the low counting, long wavelength incident neutrons at large scattering angles. Above technical results may accelerate the development of other easily accessible engineering materials evaluation techniques using compact neutron source, and also help to improve the data-collecting efficiency for various time-sliced scattering experiments at large neutron facilities.

論文

Shell structure of the neutron-rich isotopes $$^{69,71,73}$$Co

Lokotko, T.*; Leblond, S.*; Lee, J.*; Doornenbal, P.*; Obertelli, A.*; Poves, A.*; Nowacki, F.*; 緒方 一介*; 吉田 数貴; Authelet, G.*; et al.

Physical Review C, 101(3), p.034314_1 - 034314_7, 2020/03

https://doi.org/10.1103/PhysRevC.101.034314
 被引用回数：4 パーセンタイル：79.36(Physics, Nuclear)

中性子過剰核である$$^{69,71,73}$$Coに対する($$p,2p$$)ノックアウト反応が理化学研究所RIBFで測定された。$$gamma-gamma$$ coincidenceの方法で準位構造が決定され、測定された包括的断面積および排他的断面積から暫定的ではあるがスピン・パリティが決定された。殻模型計算との比較により、$$^{69,71,73}$$Coの低励起状態には球形核と変形核が共存することが示唆された。

論文

Microstructural features and ductile-brittle transition behavior in hot-rolled lean duplex stainless steels

高橋 治*; 渋井 洋平*; 徐 平光; Harjo, S.; 鈴木 徹也*; 友田 陽*

Quantum Beam Science (Internet), 4(1), p.16_1 - 16_15, 2020/03

https://doi.org/10.3390/qubs4010016

The characteristics of texture and microstructure of lean duplex stainless steels with low Ni content produced through hot rolling followed by annealing were investigated locally with electron backscatter diffraction and globally with neutron diffraction. Then, the ductile-brittle transition (DBT) behavior was studied by Charpy impact test. It is found that the DBT temperature (DBTT) is strongly affected by the direction of crack propagation, depending on crystallographic texture and microstructural morphology; the DBTT becomes extremely low in the case of fracture accompanying delamination. A high Ni duplex stainless steel examined for comparison, shows a lower DBTT compared with the lean steel in the same crack propagating direction. The obtained results were also discussed through comparing with those of cast duplex stainless steels reported previously (Takahashi et al., Tetsu-to-Hagane, 100(2014), 1150).

論文

Strong local moment antiferromagnetic spin fluctuations in V-doped LiFeAs

Xu, Z.*; Dai, G.*; Li, Y.*; Yin, Z.*; Rong, Y.*; Tian, L.*; Liu, P.*; Wang, H.*; Xing, L.*; Wei, Y.*; et al.

npj Quantum Materials (Internet), 5(1), p.11_1 - 11_7, 2020/02

https://doi.org/10.1038/s41535-020-0212-x
 被引用回数：3 パーセンタイル：55.89(Materials Science, Multidisciplinary)

We use neutron scattering to study Vanadium (hole)-doped LiFe$$_{1-x}$$V$$_{x}$$As. In the undoped state, LiFeAs exhibits superconductivity at $$T_mathrm{c} = 18$$ K and transverse incommensurate spin excitations similar to electron overdoped iron pnictides. Upon Vanadium doping to form LiFe$$_{0.955}$$V$$_{0.045}$$, the transverse incommensurate spin excitations in LiFeAs transform into longitudinally elongated ones in a similar fashion to that of potassium (hole)-doped Ba$$_{0.7}$$K$$_{0.3}$$Fe$$_{2}$$As$$_{2}$$ but with dramatically enhanced magnetic scattering and elimination of superconductivity. This is different from the suppression of the overall magnetic excitations in hole-doped BaFe$$_{2}$$As$$_{2}$$ and the enhancement of superconductivity near optimal hole doping. These results are consistent with density function theory plus dynamic mean field theory calculations, suggesting that Vanadium doping in LiFeAs may induce an enlarged effective magnetic moment $$S_mathrm{eff}$$ with a spin crossover ground state arising from the inter-orbital scattering of itinerant electrons.

論文

IAEA Photonuclear Data Library 2019

河野 俊彦*; Cho, Y. S.*; Dimitriou, P.*; Filipescu, D.*; 岩本 信之; Plujko, V.*; Tao, X.*; 宇都宮 弘章*; Varlamov, V.*; Xu, R.*; et al.

Nuclear Data Sheets, 163, p.109 - 162, 2020/01

https://doi.org/10.1016/j.nds.2019.12.002
 被引用回数：16 パーセンタイル：98.22(Physics, Nuclear)

We report our coordinated efforts to address these data needs such as radiation shielding design and radiation transport analyses, and present the results of the new evaluations of more than 200 nuclides included in the new updated IAEA Photonuclear Data Library, where the photon energy goes up to 200 MeV. We discuss the new assessment method and make recommendations to the user community in cases where the experimental data are discrepant and the assessments disagree. In addition, in the absence of experimental data, we present model predictions for photon-induced reaction cross section on nuclides of potential interest to medical radioisotope production.

論文

Nagasaki sediments reveal that long-term fate of plutonium is controlled by select organic matter moieties

Lin, P.*; Xu, C.*; Kaplan, D. I.*; Chen, H.*; Yeager, C. M.*; Xing, W.*; Sun, L.*; Schwehr, K. A.*; 山崎 秀夫*; 國分 陽子; et al.

Science of the Total Environment, 678, p.409 - 418, 2019/08

https://doi.org/10.1016/j.scitotenv.2019.04.375
 被引用回数：3 パーセンタイル：20.11(Environmental Sciences)

日本原子力研究開発機構等により長崎原爆由来のプルトニウムが含まれると明らかにされた堆積物を用いて、プルトニウムの存在形態を調べた。選択抽出後、エレクトロスプレーイオン化フーリエ変換イオンサイクロトロン共鳴質量分析装置により分子的特性を調べた結果、55%のプルトニウムが難分解性有機物と結合し、31%が他の有機物、残り20%以下が鉱物粒子に固定化されていることがわかった。現在の長期的なプルトニウムの処分や環境汚染修復のモデルでは、溶解が制限されることや鉱物表面への吸着が表層でのPuの移動性を制御していると考えられていたが、本研究により有機物がPuの隔離に重要な役割を果たしていることが明らかとなった。

論文

Nuclear structure of $$^{76}$$Ni from the ($$p$$,$$2p$$) reaction

Elekes, Z.*; Kripk$'o$, $'A$*; Sohler, D.*; Sieja, K.*; 緒方 一介*; 吉田 数貴; Doornenbal, P.*; Obertelli, A.*; Authelet, G.*; 馬場 秀忠*; et al.

Physical Review C, 99(1), p.014312_1 - 014312_7, 2019/01

https://doi.org/10.1103/PhysRevC.99.014312
 被引用回数：7 パーセンタイル：80.58(Physics, Nuclear)

($$p$$,$$2p$$)反応による$$^{76}$$Niの核構造の探索実験を行った。Lenzi, Nowacki, Poves, Sieja相互作用を用いた殻模型計算では実験結果を説明しうる陽子空孔状態が得られており、理論的な断面積計算は実験値とよい一致を与えた。実験で得られたすべての状態を理論的に一意に決定することはできなかったが、過去の実験結果と同様にNi同位体でのZ = 28の大きなshell gapを示す結果が得られた。

論文

Evaluation of residual stress relaxation in a rolled joint by neutron diffraction

林 眞琴*; Root, J. H.*; Rogge, R. B.*; 徐 平光

Quantum Beam Science (Internet), 2(4), p.21_1 - 21_16, 2018/12

https://doi.org/10.3390/qubs2040021

The rolled joint of pressure tube, consisting of three axial symmetric parts, modified SUS403 stainless steel, Zr-2.5Nb pressure tube and Inconel-718, has been examined by neutron diffraction for residual stresses. It was heat treated at 350$$^{circ}$$C for 30, 130 and 635 hours to simulate the thermal aging of the rolled joint over the lifetime of the advanced thermal reactor at 288$$^{circ}$$C for 1, 5 and 30 years. The crystal lattice strains at various locations in the rolled joint before and after the aging treatments were measured by neutron diffraction and the residual stress distribution in the rolled joint was evaluated by using the Kroner elastic model and the generalized Hooke's law. In the crimp region of the rolled joint, it was found that the aging treatment had weak effect on the residual stresses in the Inconel and the SUS403. In the non-aged Zr-2.5Nb, the highest residual stresses were found near its interface with the SUS430. In the Zr-2.5Nb in the crimp region near its interface with the SUS430, the average compressive axial stress was -440 MPa, having no evident change during the long-time aging. In the Zr-2.5Nb outside closest to the crimp region, the tensile axial and hoop stresses were relieved during the 30 hours aging. The hoop stresses in the crimp region evolved from an average tensile stress of 80 MPa to an average compressive stress of 230 MPa after the 635 hours aging, suggesting that the rolled joint had a good long-term sealing ability against the leakage of high temperature water.

論文

Nuclear moments of the low-lying isomeric $$1^+$$ state of $$^{34}$$Al; Investigation on the neutron $$1p1h$$ excitation across $$N=20$$ in the island of inversion

Xu, Z. Y.*; Heylen, H.*; 旭 耕一郎*; Boulay, F.*; Daugas, J. M.*; de Groote, R. P.*; Gins, W.*; Kamalou, O.*; Koszor$'u$s, $'A$.*; Lykiardopoupou, M.*; et al.

Physics Letters B, 782, p.619 - 626, 2018/07

https://doi.org/10.1016/j.physletb.2018.06.009
 被引用回数：5 パーセンタイル：56.63(Astronomy & Astrophysics)

GANIL研究所において、$$^{36}$$Sからのフラグメンテーション反応によって中性子過剰核$$^{34}$$Alにおける核異性体である$$1^+$$状態を生成し、その磁気双極子モーメントと電気的四重極モーメント(Qモーメント)をそれぞれ$$beta$$-NMR法および$$beta$$-NQR法を用いて測定した。この状態は中性子数20の殻ギャップを越えて励起したものであり、その性質を実験的に押さえることは、この原子核の周辺で知られている逆転の島(基底状態で既に殻ギャップを越えた励起が起こるとされる原子核の一団)の発現のメカニズムを解明するための有益な情報を与える。測定されたg因子の絶対値は$$1.757pm 0.014$$、Qモーメントの絶対値は38(5)mbとなった。これらの値は、大規模殻模型計算による予言値に近く、模型の高い記述能力を確かめることができた。

論文

High stereographic resolution texture and residual stress evaluation using time-of-flight neutron diffraction

徐 平光; Harjo, S.; 小島 真由美*; 鈴木 裕士; 伊藤 崇芳*; Gong, W.; Vogel, S. C.*; 井上 純哉*; 友田 陽*; 相澤 一也; et al.

Journal of Applied Crystallography, 51(3), p.746 - 760, 2018/06

https://doi.org/10.1107/S1600576718004004
 被引用回数：18 パーセンタイル：92.35(Chemistry, Multidisciplinary)

Neutron diffraction texture measurements provide bulk textures with excellent grain statistics even for large grained materials, together with the crystallographic parameters and microstructure information such as phase fractions, coherent crystallite size, root mean square microstrain, macroscopic/intergranular stress/strain. The procedure for high stereographic resolution texture and residual stress evaluation was established at the TAKUMI engineering materials diffractometer. The pole figure evaluation of a limestone standard sample with a trigonal crystal structure suggested that the obtained precision for texture measurement is comparable with the oversea well-established neutron beam lines utilized for texture measurements. A high strength martensite-austenite multilayered steel was employed for further verification of the reliability of simultaneous Rietveld analysis of multiphase textures and macro stress tensors. By using a geometric mean micro-mechanical model, the macro stress tensor analysis with a plane stress assumption showed a RD-TD in-plane compressive stress (about -330 MPa) in martensite layers and a RD-TD in-plane tensile stress (about 320 MPa) in austenite layers. The phase stress partitioning was ascribed to the additive effect of volume expansion during martensite transformation and the linear contraction misfit during water quenching.

論文

Shell evolution beyond $$Z$$=28 and $$N$$=50; Spectroscopy of $$^{81,82,83,84}$$Zn

Shand, C. M.*; Podoly$'a$k, Zs.*; G$'o$rska, M.*; Doornenbal, P.*; Obertelli, A.*; Nowacki, F.*; Otsuka, T.*; Sieja, K.*; Tostevin, J. A.*; Tsunoda, T.*; et al.

Physics Letters B, 773, p.492 - 497, 2017/10

https://doi.org/10.1016/j.physletb.2017.09.001
 被引用回数：18 パーセンタイル：88.47(Astronomy & Astrophysics)

Low-lying states in neutron-rich $$^{81,82.83.84}$$Zn nuclei were measured for the first time via in-beam $$gamma$$-ray spectroscopy at RIKEN. These include the 4$$_1^+$$ to 2$$_1^+$$ in $$^{82}$$Zn and the 2$$_1^+$$ to 0$$_1^+$$ and 4$$_1^+$$ to 2$$_1^+$$ in $$^{84}$$Zn. The reduced E($$2^+$$) energies and increased E(4$$^+$$)/E(2$$^+$$) ratios at $$N$$=52,54 compared to $$^{80}$$Zn attest that the magicity is confined just on the neutron number $$N$$=50 only. The levels observed in $$^{84}$$Zn suggest the onset of deformation towards heavier Zn isotopes. The data were compared to state-of-the-art shell model calculations.

論文

種々な方法によるMn-Si-C鋼の残留オーステナイト体積率測定の比較

友田 陽*; 関戸 信彰*; 徐 平光; 川崎 卓郎; Harjo, S.; 田中 雅彦*; 篠原 武尚; Su, Y.; 谷山 明*

鉄と鋼, 103(10), p.570 - 578, 2017/10

https://doi.org/10.2355/tetsutohagane.TETSU-2017-045
 被引用回数：11 パーセンタイル：62.6(Metallurgy & Metallurgical Engineering)

Various methods were employed to measure the austenite volume fraction in a 1.5Mn-1.5Si-0.2C steel. It has been confirmed that the volume fractions determined by transmission electron microscopy, scanning electron microscopy/electron back scatter diffraction, X-ray diffraction and neutron diffraction exhibit a general trend to become larger in this order, although the values obtained by X-ray and neutron diffraction are similar in the present steel because austenite is relatively stable. The austenite volume fractions determined by diffraction methods have been found to be affected by the measuring specimen direction, i.e., texture, even by applying the conventional correcting procedure. To avoid this influence, it is recommended to measure both of volume fraction and texture simultaneously using neutron diffraction. Although synchrotron X-ray shows higher angle resolution, its small incident beam size brings poor statistic reliability. The influence of texture cannot be avoided for transmission Bragg edge measurement, either, which must be overcome to realize 2D or 3D volume fraction mapping.

論文

Observation of a $$gamma$$-decaying millisecond isomeric state in $$^{128}$$Cd$$_{80}$$

Jungclaus, A.*; Grawe, H.*; 西村 俊二*; Doornenbal, P.*; Lorusso, G.*; Simpson, G. S.*; S$"o$derstr$"o$m, P.-A.*; 炭竃 聡之*; Taprogge, J.*; Xu, Z. Y.*; et al.

Physics Letters B, 772, p.483 - 488, 2017/09

https://doi.org/10.1016/j.physletb.2017.07.006
 被引用回数：7 パーセンタイル：61.99(Astronomy & Astrophysics)

A new high-spin isomer in the neutron-rich nucleus $$^{128}$$Cd was populated in the projectile fission of a $$^{238}$$U beam at the Radioactive Isotope Beam Factory at RIKEN. A half-life of T$$_{1/2}$$ = 6.3(8) ms was measured for the new state which was tentatively assigned a spin/parity of (15$$^-$$). The isomeric state decays via the emission of a 309-keV $$gamma$$ ray with $$E3$$ multipolarity. The experimental results are compared to shell model calculations performed using state-of-the-art realistic effective interactions and to the neighbouring nucleus $$^{129}$$Cd. The comparison with calculations shows that adjustments of the pairing and multipole parts of the effective interaction derived from the CD-Bonn nucleon-nucleon potential are required in order to describe the properties of nuclei in the region around $$^{132}$$Sn.

論文

Quantitative evaluation of texture and dislocations during annealing after hot deformation in austenitic steel using neutron diffraction

友田 陽*; 佐藤 成男*; Uchida, M.*; 徐 平光; Harjo, S.; Gong, W.; 川崎 卓郎

Materials Science Forum, 905, p.25 - 30, 2017/08

https://doi.org/10.4028/www.scientific.net/MSF.905.25

Microstructural change during hot compressive deformation at 700 $$^{circ}$$C followed by isothermal annealing for a Fe-32Ni austnitic alloy was monitored using ${it in situ}$ neutron diffraction. The evolution of deformation texture with 40% compression and its change to recrystallization texture during isothermal annealing were presented by inverse pole figures for the axial and radial directions. The change in dislocation density was tracked using the convolutional muli-profile whole profile fitting method. To obtain the fitting results with good statistics, at least 60 s time-slicing for the event-mode recorded data was needed. The average dislocation density in 60 s after hot compression was determined to be 2.8 $$times$$ 10$$^{14}$$ m$$^{-2}$$ that decreased with increasing of annealing time.

論文

Shape evolution in neutron-rich krypton isotopes beyond N=60; First spectroscopy of $$^{98,100}$$Kr

Flavigny, F.*; Doornenbal, P.*; Obertelli, A.*; Delaroche, J.-P.*; Girod, M.*; Libert, J.*; Rodriguez, T. R.*; Authelet, G.*; 馬場 秀忠*; Calvet, D.*; et al.

Physical Review Letters, 118(24), p.242501_1 - 242501_6, 2017/06

https://doi.org/10.1103/PhysRevLett.118.242501
 被引用回数：27 パーセンタイル：88.56(Physics, Multidisciplinary)

The first $$gamma$$-ray spectroscopy of very neutron rich $$^{98,100}$$Kr isotopes was carried out at the RIBF at RIKEN Nishina center. Excited states in these isotopes were populated via (p,2p) reactions using radioactive $$^{99,101}$$Rb beams accelerated to 220 MeV/nucleon. The new data show a significant increase in deformation beyond N=60, as well as competing configurations (shape-coexistence) at low energy. The data were compared with beyond-mean-field calculations which predict level energies in good agreement with observation, and suggest oblate-prolate shape coexistence.

論文

放射光X線回折法を用いた積層型高強度鋼板におけるマルテンサイト層の局所変形挙動評価

小島 真由美*; 城 鮎美*; 鈴木 裕士; 井上 純哉*; 菖蒲 敬久; 徐 平光; 秋田 貢一; 南部 将一*; 小関 敏彦*

材料, 66(6), p.420 - 426, 2017/06

https://doi.org/10.2472/jsms.66.420

The strain distribution in a multilayered steel composite, which consists of martensite and austenite layers, was evaluated by energy dispersive X-ray diffraction to investigate the homogeneity of deformation in the martensite layer under uniaxial loading. A dog-bone shape specimen with a martensite layer with 0.2 mm in a thickness, sandwiching by austenite layers with 0.4 mm in thickness, was utilized in this study. A change in strains as a function of tensile loading was measured at the center of the martensite layer as well as near the interface between the martensite and austenite layers. Furthermore, the residual strain distributions were measured in the martensite layer of the unloaded specimens after different applied strains. As a result, slight inhomogeneous deformation was found at the beginning of the plastic deformation in the martensite layer although no local deformation was recognized even near the interface between austenite and martensite layers. After further deformation, mismatch of plastic deformation between austenite and martensite layers was reduced, and the martensite layer deformed homogeneously. Therefore, an unstable interface phenomenon might not be caused by the intrinsic factors with a mesoscopic scale discussed in this experiment.

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