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EB-PVDによる遮熱コーティングの残留応力のX線評価

Residual stress in zirconia coating by EB-PVD method

鈴木 賢治*; 和田 国彦*; 松原 秀彰*; 菖蒲 敬久 ; 川村 昌志*; 田中 啓介*

Suzuki, Kenji*; Wada, Kunihiko*; Matsubara, Hideaki*; Shobu, Takahisa; Kawamura, Masashi*; Tanaka, Keisuke*

Niベースの超合金であるIN738LCは基質材料として使われ、CoNiCrAlYはその上にボンドコートとしてプラズマスプレーにより押し固められている。その上にZrがEV-PVD法によりトップコーティングされている。本試験では基盤回転数の異なる試料に関して、組織観察及び残留応力測定を行った。SEM観察の結果から、Zrコーティングは(111)方向に成長した柱状組織を有していることがわかった。また表面の残留応力は、基盤回転数が減少するに従い圧縮の残留応力が大きくなることがわかった。

The Ni-based superalloy IN738LC was used as the substrate material, and CoNiCrAlY powder was pressureless plasma-sprayed on the substrate as the bond coating. Zirconia was coated as the top coating by the electron beam-physical vapor deposition (EV-PVD) method. In the EB-PVD process, the specimens were kept at 1223 K and rotated with 5 rpm, 10 rpm and 20 rpm. According to the microscopic observation and the result of the pole figures, the top coatings had a columnar structure, which was made by the piling up of (111) planes. The cross section of the column had a diamond shape, and its diagonal was parallel to the rotation axis. The residual stress on the surface of the top coatings was evaluated by the X-ray diffraction method. Each diffraction profile was separated into the 133 and the 331 peak, and the residual stress was measured by the sin$$^{2}$$ $$psi$$ method. The measured residual stresses were -76.6 MPa for 5 rpm, -63.0 MPa for 10 rpm and -25.1 MPa for 20 rpm.

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