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${it Operando}$ structure observation of pyroelectric ceramics during power generation cycle

川崎 卓郎; 福田 竜生; 山中 暁*; 坂本 友和*; 村山 一郎*; 加藤 孝典*; 馬場 将亮*; 橋本 英樹*; Harjo, S.; 相澤 一也; et al.

Journal of Applied Physics, 131(13), p.134103_1 - 134103_7, 2022/04

The microscopic origin of the pyroelectric power generation using ferroelectric ceramics for energy harvesting from time-varying waste heat can be understood by conducting ${it operando}$ neutron diffraction measurements. The behavior of the domain orientation and lattice strain in the lead zirconate titanate (PZT)-based ceramics with a tetragonal structure during the novel power generation cycle combining electric field and temperature change were investigated. The [001] domains and the lattice strain of the (111) plane in the direction of parallel to the electric field increase in the process of simultaneous rise in the electric field and temperature, and rapidly decrease in the process of the field drop. The alignment of the domain orientation by the electric field and its randomization by the higher temperature during the cycle are critical features of the current power generation system.


Quasifree neutron knockout reaction reveals a small $$s$$-Orbital component in the Borromean nucleus $$^{17}$$B

Yang, Z. H.*; 久保田 悠樹*; Corsi, A.*; 吉田 数貴; Sun, X.-X.*; Li, J. G.*; 木村 真明*; Michel, N.*; 緒方 一介*; Yuan, C. X.*; et al.

Physical Review Letters, 126(8), p.082501_1 - 082501_8, 2021/02

 被引用回数:10 パーセンタイル:98.7(Physics, Multidisciplinary)

ボロミアン核であり中性子ハロー構造が期待される$$^{17}$$Bに対する($$p$$,$$pn$$)反応実験を行った。断面積の運動量分布を分析することで、$$1s_{1/2}$$$$0d_{5/2}$$軌道の分光学的因子を決定した。驚くべきことに、$$1s_{1/2}$$の分光学的因子は9(2)%と小さいことが明らかになった。この結果は、連続状態を含むdeformed relativistic Hartree-Bogoliubov理論によってよく説明された。本研究の結果によると、現在知られているハロー構造を持つとされる原子核の中で$$^{17}$$Bは$$s$$および$$p$$軌道の成分が最も小さく、$$s$$または$$p$$軌道成分が支配的であることが必ずしもハロー構造の前提条件ではない可能性を示唆している。


Pyroelectric power generation from the waste heat of automotive exhaust gas

Kim, J.*; 山中 暁*; 村山 一郎*; 加藤 孝典*; 坂本 友和*; 川崎 卓郎; 福田 竜生; 関野 徹*; 中山 忠親*; 武田 雅敏*; et al.

Sustainable Energy & Fuels (Internet), 4(3), p.1143 - 1149, 2020/03

 被引用回数:3 パーセンタイル:51.8(Chemistry, Physical)

Waste heat is a potentially exploitable energy source but remains a problem awaiting a solution. To explore solutions for automobile applications, we investigate pyroelectric power generation from the temperature variation of exhaust gas using a novel electro-thermodynamic cycle. Niobium-doped lead zirconate titanate stannate (PNZST) ceramics were applied as pyroelectric materials, and their structural characteristics were investigated. In the driving cycle assessments (JC-08) using real exhaust gas, the maximum power generated was identified as 143.9 mW cm$$^{-3}$$ (777.3 J L$$^{-1}$$ per 1 cycle) over a temperature range of 150-220 $$^{circ}$$C and an electric field of 13 kV cm-1. The net mean generating power of the total driving cycle was 40.8 mW cm$$^{-3}$$, which is the most enhanced result in our power generating systems to date and 314 times greater than our first report. Materials with sharp transition behaviors with the temperature and electric field are worthy of study with regard to pyroelectric energy harvesting materials, and their corresponding crystal and domain structures were investigated to optimize performance.


Electrical and crystallographic study of an electrothermodynamic cycle for a waste heat recovery

Kim, J.*; 山中 暁*; 中島 啓*; 加藤 孝典*; Kim, Y.*; 福田 竜生; 吉井 賢資; 西畑 保雄; 馬場 将亮*; 武田 雅敏*; et al.

Advanced Sustainable Systems (Internet), 2(11), p.1800067_1 - 1800067_8, 2018/11

 被引用回数:1 パーセンタイル:11.84(Green & Sustainable Science & Technology)

An innovative electrothermodynamic cycle (pyroelectric effect with an external electric field) was recently presented, which is based on temporal temperature variations in wasted heat from engine exhaust gas. In this paper, for further improvement, a generating mechanism of the cycle is investigated using in-operando time-resolved synchrotron X-ray diffraction with generating assessment. The polarizations of the sample are gained from both crystal/domain changes and simultaneous electrical measurements. Three types of materials are prepared: soft and hard types of lead zirconate titanate (PZT) and lead magnesium niobate-lead titanate (PMN-PT). Among them, PMN-PT has the highest generating power. When an external electric field is applied, the PMN-PT exhibits only 180$$^circ$$ domain rotations, whereas PZTs exhibit both 90$$^circ$$ and 180$$^circ$$ rotations. A strong driving force for 180$$^circ$$ rotation depresses rotations in other angles and increases polarization changes. The results show that the material development, which has only 180$$^circ$$ switching domains, has potential for use in the establishment of a high-efficiency waste heat recovery system.


In-beam $$gamma$$-ray spectroscopy of $$^{35}$$Mg via knockout reactions at intermediate energies

籾山 悟至*; Doornenbal, P.*; Scheit, H.*; 武内 聡*; 新倉 潤*; 青井 考*; Li, K.*; 松下 昌史*; Steppenbeck, D.*; Wang, H.*; et al.

Physical Review C, 96(3), p.034328_1 - 034328_8, 2017/09

 被引用回数:5 パーセンタイル:51.78(Physics, Nuclear)

理化学研究所の不安定核実験施設RIBFにて、中性子過剰核$$^{35}$$Mgの励起状態を$$^{36}$$Mgおよび$$^{37}$$Alからのノックアウト反応によって生成し、そこからの脱励起$$gamma$$線を観測した。$$^{35}$$Mgは中性子数20魔法数が消滅するとされる「逆転の島」と呼ばれる領域に含まれると考えられており、また、奇核であることから、一粒子状態と集団的状態が結合した興味深い核構造が出現すると期待されている。この実験によって、206keV, 443keV, 616keV, 670keVの4本の$$gamma$$線を観測し、これらを全て基底状態へ脱励起する$$gamma$$線であると仮定して励起準位を構成した。この準位構造、ノックアウト反応の断面積、移行運動量分布を殻模型計算および反対称化分子動力学計算と比較した。二つの計算は、基底状態近傍の高い準位密度などいくつかの特徴的な核構造を再現することに成功し、$$^{35}$$Mgは「逆転の島」に含まれるという描像と無矛盾であることがわかった。


Pyroelectric power generation with ferroelectrics (1-x)PMN-xPT

Kim, J.*; 山中 暁*; 中島 啓*; 加藤 孝典*; Kim, Y.*; 福田 竜生; 吉井 賢資; 西畑 保雄; 馬場 将亮*; 武田 雅敏*; et al.

Ferroelectrics, 512(1), p.92 - 99, 2017/08

 被引用回数:6 パーセンタイル:41.1(Materials Science, Multidisciplinary)

We have been investigating a novel electrothermodynamic cycle based on temporal temperature variations using the pyroelectric effect to utilize the waste heat as renewable energy. An improved generating performance with relaxer ferroelectric ceramics was achieved using 75Pb(Mg$$_{2/3}$$Nb$$_{1/3}$$)O$$_3$$-25PbTiO$$_3$$ which is well known for the high dielectric and pyroelectric properties. The potential was evaluated by using the hysteresis loops and generating properties are analyzed both in laboratory and engine dynamometer. Results showed 0.48 mW/cm$$^3$$ in engine dynamometer assessment, which is 3 times larger than the previous study using Pb(Zr,Ti)O$$_3$$.


Relationship between the material properties and pyroelectric-generating performance of PZTs

山中 暁*; Kim, J.*; 中島 啓*; 加藤 孝典*; Kim, Y.*; 福田 竜生; 吉井 賢資; 西畑 保雄; 馬場 将亮*; 山田 昇*; et al.

Advanced Sustainable Systems (Internet), 1(3-4), p.1600020_1 - 1600020_6, 2017/04



Asymmetry dependence of reduction factors from single-nucleon knockout of $$^{30}$$Ne at $$sim$$ 230 MeV/nucleon

Lee, J.*; Liu, H.*; Doornenbal, P.*; 木村 真明*; 蓑茂 工将*; 緒方 一介*; 宇都野 穣; 青井 考*; Li, K.*; 松下 昌史*; et al.

Progress of Theoretical and Experimental Physics (Internet), 2016(8), p.083D01_1 - 083D01_7, 2016/08


 被引用回数:5 パーセンタイル:47.01(Physics, Multidisciplinary)



Novel electrothermodynamic power generation

Kim, Y.*; Kim, J.*; 山中 暁*; 中島 啓*; 小川 孝*; 芹沢 毅*; 田中 裕久*; 馬場 将亮*; 福田 竜生; 吉井 賢資; et al.

Advanced Energy Materials, 5(13), p.1401942_1 - 1401942_6, 2015/07

 被引用回数:8 パーセンタイル:41.84(Chemistry, Physical)




能田 洋平; 小泉 智; 橋本 竹治; 下野 智史*; 馬場 正昭*; 山内 淳*; 伊熊 直彦*; 内田 幸明*; 田村 類*; 飯間 義雄*

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