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論文

Martensitic transformation behavior of Fe-Ni-C alloys monitored by ${it in-situ}$ neutron diffraction during cryogenic cooling

山下 享介*; Harjo, S.; 川崎 卓郎; 諸岡 聡; Gong, W.; 藤井 英俊*; 友田 陽*

ISIJ International, 64(2), p.192 - 201, 2024/01

${it In situ}$ neutron diffraction measurements were performed on Fe-33Ni-0.004C alloy (33Ni alloy) and Fe-27Ni-0.5C alloy (27Ni-0.5C alloy) during cooling from room temperature to the cryogenic temperature (4 K) to evaluate changes in the lattice constants of austenite and martensite, and changes in the tetragonality of martensite due to thermally induced martensitic transformation. As the martensitic transformation progressed, the lattice constants of austenite in both alloys deviated to smaller values than those predicted considering the thermal shrinkage, accompanied by an increase in the full width at half maximum of austenite. The fresh martensite formed in both alloys had a body-centered tetragonal (BCT) structure, regardless of the carbon content. The tetragonality of martensite decreased with progressive martensitic transformation during cooling in the 33Ni alloy, but was almost constant in the 27Ni-0.5C alloy. This suggests that carbon is necessary to maintain the tetragonality of martensite during cooling. The tetragonality of martensite in the 27Ni-0.5C alloy decreased during room temperature aging because of carbon mobility.

論文

Neutron stress measurement of W/Ti composite in cryogenic temperatures using time-of-flight method

西田 真之*; Harjo, S.; 川崎 卓郎; 山下 享介*; Gong, W.

Quantum Beam Science (Internet), 7(1), p.8_1 - 8_15, 2023/03

In this study, the thermal stress alterations generated in a tungsten fiber reinforced titanium composite (W/Ti composite) were evaluated by the neutron stress measurement method at cryogenic temperatures. The W/Ti composite thermal loads were repeated from room temperature to the cryogenic temperature (10 K), and alterations in thermal residual stress were evaluated using the neutron in situ stress measurement method. In this measurement, the stress alterations in the titanium matrix and the tungsten fibers were measured. This measurement was carried out by TAKUMI (MLF-BL19) of J-PARC, a neutron research facility in the Japan Atomic Agency. The measurement method of TAKUMI is the time-of-flight (TOF) method. Owing to this measurement method, the measurement time was significantly shortened compared to the angle-dispersion type measurement by a diffractometer. As a result of the measurement, large compressive stresses of about 1 GPa were generated in the tungsten fibers, and tensile stresses of about 100 MPa existed in the titanium matrix. The thermal stresses due to the temperature change between room temperature and cryogenic temperature is caused by the difference of thermal expansions between the tungsten fibers and the titanium matrix, and these stress values can be approximated by a simple elastic theory equation.

論文

Tough yet flexible superelastic alloys meet biomedical needs

Xu, X.*; 大平 拓実*; Xu, S.*; 平田 研二*; 大森 俊洋*; 植木 洸輔*; 上田 恭介*; 成島 尚之*; 長迫 実*; 貝沼 亮介*; et al.

Advanced Materials & Processes, 180(7), p.35 - 37, 2022/10

Metallic biomaterials are widely used to replace or support failing hard tissues due to excellent mechanical properties and high wear resistance, with demand increasing as the global population continues to age. It is widely accepted that successful metallic biomaterials should have good biocompatibility, high corrosion resistance, and strong wear resistance. In addition, a low Young's modulus similar to human bone is now recognized as another important factor, in order to avoid bone atrophy due to the stress shielding effect. While the Young's modulus of stainless steels and conventional fcc CoCr alloys is as high as 190-240 GPa, for $$beta$$-type Ti-base alloys it is generally in the range of 50-80 GPa. Young's modulus values are as low as 35 GPa for Ti-Nb-Ta-Zr, close to that of human bone at approximately 10-30 GPa. However, Ti-base alloys come with the compromise of low wear resistance. In fact, alloys that feature a low Young's modulus along with high wear resistance have been difficult to realize. This article explores the recently developed bcc CoCr-base alloy Co-Cr-Al-Si as a potential solution to these issues, i.e., the difficulty in combining a low Young's modulus with high wear resistance, and the challenge of realizing large superelastic strains.

論文

Microstructure and plasticity evolution during L$"u$ders deformation in an Fe-5Mn-0.1C medium-Mn steel

小山 元道*; 山下 享介*; 諸岡 聡; 澤口 孝宏*; Yang, Z.*; 北條 智彦*; 川崎 卓郎; Harjo, S.

ISIJ International, 62(10), p.2036 - 2042, 2022/10

 被引用回数:4 パーセンタイル:67.13(Metallurgy & Metallurgical Engineering)

The local plasticity and associated microstructure evolution in Fe-5Mn-0.1C medium-Mn steel (wt.%) were investigated in this study. Specifically, the micro-deformation mechanism during L$"u$ders banding was characterized based on multi-scale electron backscatter diffraction measurements and electron channeling contrast imaging. Similar to other medium-Mn steels, the Fe-5Mn-0.1C steel showed discontinuous macroscopic deformation, preferential plastic deformation in austenite, and deformation-induced martensitic transformation during L$"u$ders deformation. Hexagonal close-packed martensite was also observed as an intermediate phase. Furthermore, an in-situ neutron diffraction experiment revealed that the pre-existing body-centered cubic phase, which was mainly ferrite, was a minor deformation path, although ferrite was the major constituent phase.

論文

Hierarchical deformation heterogeneity during L$"u$ders band propagation in an Fe-5Mn-0.1C medium Mn steel clarified through ${it in situ}$ scanning electron microscopy

小山 元道*; 山下 享介*; 諸岡 聡; Yang, Z.*; Varanasi, R. S.*; 北條 智彦*; 川崎 卓郎; Harjo, S.

ISIJ International, 62(10), p.2043 - 2053, 2022/10

 被引用回数:2 パーセンタイル:34.75(Metallurgy & Metallurgical Engineering)

${it In situ}$ deformation experiments with cold-rolled and intercritically annealed Fe-5Mn-0.1C steel were carried out at ambient temperature to characterize the deformation heterogeneity during L$"u$ders band propagation. Deformation band formation, which is a precursor phenomenon of L$"u$ders band propagation, occurred even in the macroscopically elastic deformation stage. The deformation bands in the L$"u$ders front grew from both the side edges to the center of the specimen. After macroscopic yielding, the thin deformation bands grew via band branching, thickening, multiple band initiation, and their coalescence, the behavior of which was heterogeneous. Thick deformation bands formed irregularly in front of the region where the thin deformation bands were densified. The thin deformation bands were not further densified when the spacing of the bands was below $$sim$$10 $$mu$$m. Instead, the regions between the deformation bands showed a homogeneous plasticity evolution. The growth of the thin deformation bands was discontinuous, which may be due to the presence of ferrite groups in the propagation path of the deformation bands. Based on these observations, a model for discontinuous L$"u$ders band propagation has been proposed.

論文

Revisit deformation behavior of lath martensite

Harjo, S.; Gong, W.; 川崎 卓郎; 諸岡 聡; 山下 享介*

ISIJ International, 62(10), p.1990 - 1999, 2022/10

 被引用回数:0 パーセンタイル:0(Metallurgy & Metallurgical Engineering)

Two mechanisms inconsistent each other, a relaxation of type II internal stress and a presence of mobile dislocation, were previously proposed to describe the low elastic limit of as-quenched lath martensite steels. In this study, neutron diffraction experiments were performed to revisit the deformation behavior of lath martensite steel. The highly dense random arrangement dislocations easily moved at the beginning of deformation, then accumulated, annihilated and changed the arrangement differently depending on the orientation of the packet with respect to the deformation direction. The movement of highly dense random arrangement dislocations played an important role as a mechanism at the beginning of deformation, and can be a true feature of mobile dislocations.

論文

Flexible and tough superelastic Co-Cr alloys for biomedical applications

大平 拓実*; Xu, S.*; 平田 研二*; Xu, X.*; 大森 俊洋*; 植木 洸輔*; 上田 恭介*; 成島 尚之*; 長迫 実*; Harjo, S.; et al.

Advanced Materials, 34(27), p.2202305_1 - 2202305_11, 2022/07

 被引用回数:3 パーセンタイル:85.34(Chemistry, Multidisciplinary)

The demand for biomaterials has been increasing along with the increase in the population of elderly people worldwide. The mechanical properties and high wear resistance of metallic biomaterials makes them well-suited for use as substitutes or as support for damaged hard tissues. However, unless these biomaterials also have a low Young's modulus similar to that of human bones, bone atrophy inevitably occurs. Because a low Young's modulus is typically associated with poor wear resistance, it is difficult to realize a low Young's modulus and high wear resistance simultaneously. Also, the superelastic property of shape memory alloys makes them suitable for biomedical applications, like vascular stents and guide wires. However, due to the low recoverable strain of conventional biocompatible shape memory alloys, the demand for a new alloy system is high. The novel body-center-cubic cobalt-chromium-based alloys in this paper provide a solution to both of these problems. We believe our novel alloys are promising candidates for biomedical applications.

論文

In-situ neutron diffraction study of lattice deformation behaviour of commercially pure titanium at cryogenic temperature

Lee, M.-S.*; 川崎 卓郎; 山下 享介*; Harjo, S.; Hyun, Y.-T.*; Jeong, Y.*; Jun, T.-S.*

Scientific Reports (Internet), 12(1), p.3719_1 - 3719_10, 2022/03

 被引用回数:2 パーセンタイル:62.5(Multidisciplinary Sciences)

Titanium has a significant potential for the cryogenic industrial fields such as aerospace and liquefied gas storage and transportation due to its excellent low temperature properties. To develop and advance the technologies in cryogenic industries, it is required to fully understand the underlying deformation mechanisms of Ti under the extreme cryogenic environment. Here, we report a study of the lattice behaviour in grain families of Grade 2 CP-Ti during in-situ neutron diffraction test in tension at temperatures of 15-298 K. Combined with the neutron diffraction intensity analysis, EBSD measurements revealed that the twinning activity was more active at lower temperature, and the behaviour was complicated with decreasing temperature.

論文

Work hardening behavior of dual phase copper-iron alloy at low temperature

山下 享介*; 古賀 紀光*; 川崎 卓郎; 諸岡 聡; 友野 翔平*; 梅澤 修*; Harjo, S.

Materials Science & Engineering A, 819, p.141509_1 - 141509_10, 2021/07

 被引用回数:11 パーセンタイル:83.16(Nanoscience & Nanotechnology)

In-situ neutron diffraction measurements were performed on a cold-rolled copper-iron (Cu-Fe) alloy during tensile tests at 293 K and 150 K. The roles of Cu and Fe on the deformation behavior of alloys were discussed and clarified. The strength and work-hardening rate of the alloy increased with decreasing test temperature. Furthermore, the phase stress of Fe increased considerably with decreasing test temperature; however, the response of this stress to the applied true stress exhibited no dependence on the temperature. The phase stresses of Cu changed only slightly with decreasing test temperature. However, the Cu phase stress response to the applied true stress increased with decreasing test temperature, indicating an increase in the work-hardening rate. The strengthening of Fe and the increase in the work-hardening of Cu contributed to an increase in the strength and work-hardening rate of the Cu-Fe alloy at low temperatures.

論文

Stress partitioning behavior of duplex alloys consisting of BCC and FCC phases at low temperature

山下 享介; 友野 翔平*; 諸岡 聡; Harjo, S.; 川崎 卓郎; 行木 辰弥*; 古賀 紀光*; 梅澤 修*

JPS Conference Proceedings (Internet), 33, p.011064_1 - 011064_6, 2021/03

The tensile deformation and stress partitioning behavior of duplex phase alloys consisting of FCC and BCC at low temperatures were investigated using in-situ neutron diffraction during deformation. Cu-40mass%Fe alloy rolled sheet and JIS SUS329J4L duplex stainless steel were used. Both alloys showed a good balance of strength and elongation at low temperatures. In Cu-40mass%Fe alloy, the BCC phase stress at yield point increased by decreasing test temperature. The FCC phase stress at yield point was almost constant regardless of test temperature. The FCC phase started plastic deformation at a low applied true stress. When the BCC phase yielded, phase stress of FCC increased drastically at beginning, then, it increased to applied true stress with the same rate of BCC phase stress at latter regime. On the other hand, both BCC and FCC phase stresses in SUS329J4L increased by decreasing temperature.

論文

Neutron diffraction mapping measurement for Japanese nails in the ancient and present days

山下 享介; Harjo, S.; 梅澤 修*; 川崎 卓郎

JPS Conference Proceedings (Internet), 33, p.011063_1 - 011063_6, 2021/03

Japanese nails have been applied to various wooden building skeletons in Japanese temples and shrines over a period of one thousand years. Since most of Japanese nails in the ancient day are designated as an important cultural property, their destructive examinations can be hardly done. In order to discuss the material and its manufacturing process of the Japanese nails, we have done some experiments on both ancient and present Japanese nails. In this study, phase, texture and residual stress of the Japanese nails were investigated using neutron diffraction. Two types of Japanese nails were provided; one was an ancient nail obtained from Houryuji-temple; the other was a present nail forged by blacksmith. BCC iron peaks are identified in both. Although the cementite and ferrous oxide peaks are detected in the present nail, no cementite is detected in the ancient nail. The residual stresses of each nail were very low. The ferrite grains of each nail were randomly oriented.

論文

Effect of solute carbon on the characteristic hardening of steel at high temperature

古賀 紀光*; 梅澤 修*; 山本 正之*; 山本 卓*; 山下 享介; 諸岡 聡; 川崎 卓郎; Harjo, S.

Metallurgical and Materials Transactions A, 52(3), p.897 - 901, 2021/03

 被引用回数:3 パーセンタイル:26.82(Materials Science, Multidisciplinary)

Small ball rebound hardness tests demonstrated characteristic hardening at 700 K in the ultra-low carbon and pearlitic steels. The equilibrium phase diagram of Fe-C binary alloy calculated using Thermo-Calc exhibited dissolving of cementite above 700 K. Moreover, in-situ heating neutron diffraction measurement demonstrated the increase of lattice parameter by dissolving of cementite above 700 K. Therefore, it can be concluded that the characteristic hardening above 700 K can be attributed to the solid solute carbon.

論文

Role of retained austenite in low alloy steel at low temperature monitored by neutron diffraction

山下 享介; 諸岡 聡; Harjo, S.; 川崎 卓郎; 古賀 紀光*; 梅澤 修*

Scripta Materialia, 177, p.6 - 10, 2020/03

 被引用回数:29 パーセンタイル:90.87(Nanoscience & Nanotechnology)

${it In situ}$ neutron diffraction measurements during tensile tests at low temperatures of a low alloy steel containing retained austenite have been performed. Evolutions of phase fractions and phase stresses were analyzed and discussed with the progress of deformation. The role of austenite in the steel during deformation at low temperatures was observed not to directly in the contribution to the strengths but in the improvement of the elongation by transformation of austenite to martensite -and in the increasing of the work-hardening rate by an increase in the phase fraction of martensite and the work hardening of martensite.

報告書

捨石たい積場周辺環境の監視測定結果(平成28年度); 鳥取県内

小野 高行; 川崎 悟; 石森 有; 安藤 正樹

JAEA-Review 2017-044, 13 Pages, 2018/03

JAEA-Review-2017-044.pdf:1.17MB

人形峠環境技術センターでは、良好な自然環境の確保等を目的として岡山県・鳥取県と締結した環境保全協定に従って、センターやウラン鉱山跡の捨石たい積場周辺等の環境監視測定を実施している。これらの監視測定結果は、各々の県に定期的に報告するとともに、専門家で構成される岡山県環境放射線等測定技術委員会(岡山県)や鳥取県放射能調査専門家会議(鳥取県)において審議され、異常は見られないことが確認された。本資料は鳥取県に報告し、鳥取県放射能調査専門家会議において評価を受けた平成28年度の捨石たい積場周辺の環境監視結果についてまとめたものである。

報告書

人形峠周辺環境の監視測定結果(平成28年度); 岡山県内

小野 高行; 川崎 悟; 石森 有; 安藤 正樹

JAEA-Review 2017-043, 39 Pages, 2018/03

JAEA-Review-2017-043.pdf:1.92MB

人形峠環境技術センターでは、良好な自然環境の確保等を目的として岡山県・鳥取県と締結した環境保全協定に従って、センターやウラン鉱山跡の捨石たい積場周辺の環境監視測定を実施している。また、回収ウラン転換実用化試験(平成6年$$sim$$平成11年)に伴ってセンター周辺でのプルトニウムについての環境測定も実施している。これらの監視測定結果は、各々の県に定期的に報告するとともに、専門家で構成される岡山県環境放射線等測定技術委員会(岡山県)や鳥取県放射能調査専門家会議(鳥取県)において審議・評価を受けている。本資料は岡山県に報告し、岡山県環境放射線等測定技術委員会において評価を受けた平成28年度の環境監視測定結果についてまとめたものである。

論文

JSFR design progress related to development of safety design criteria for generation IV sodium-cooled fast reactors, 3; Progress of component design

江沼 康弘; 川崎 信史; 折田 潤一*; 衛藤 将生*; 宮川 高行*

Proceedings of 23rd International Conference on Nuclear Engineering (ICONE-23) (DVD-ROM), 6 Pages, 2015/05

第4世代炉のナトリウム冷却高速炉に関する安全設計クライテリアを現在開発中である。そのため、原子力機構,日本原子力発電および三菱FBRシステムズは、開発中の高速炉JSFRが、本クライテリアを満足するように設計検討を実施している。また、本クライテリアを満足するための安全対策のほかに、保守補修性の向上も同時に図っている。本論文は、主要機器の設計進捗を説明したものであり、原子炉構造においては、検査用アクセスルートを増加させ、ポンプ中間熱交換器合体機器においては、交換性の向上を図った内容を説明している。蒸気発生器に関しては、2重管の選定状況を説明している。

報告書

捨石たい積場周辺環境の監視測定結果,平成25年度; 鳥取県内

小野 高行; 辻中 秀介; 石森 有; 川崎 悟; 安藤 正樹

JAEA-Review 2014-025, 13 Pages, 2014/08

JAEA-Review-2014-025.pdf:2.44MB

人形峠環境技術センターでは、良好な自然環境の確保等を目的として岡山県・鳥取県と締結した環境保全協定に従って、センターやウラン鉱山跡の捨石たい積場周辺等の環境監視測定を実施している。これらの監視測定結果は、各々の県に定期的に報告するとともに、専門家で構成される岡山県環境放射線等測定技術委員会(岡山県)や鳥取県放射能調査専門家会議(鳥取県)において審議され、異常は見られないことが確認された。本資料は鳥取県に報告し、鳥取県放射能調査専門家会議において評価を受けた平成25年度の捨石たい積場周辺の環境監視結果についてまとめたものである。

報告書

捨石たい積場周辺環境の監視測定結果,平成24年度; 鳥取県内

伊藤 公雄; 小野 高行; 石森 有; 川崎 悟

JAEA-Review 2014-024, 19 Pages, 2014/08

JAEA-Review-2014-024.pdf:3.28MB

人形峠環境技術センターでは、良好な自然環境の確保等を目的として岡山県・鳥取県と締結した環境保全協定に従って、センターやウラン鉱山跡の捨石たい積場周辺等の環境監視測定を実施している。これらの監視測定結果は、各々の県に定期的に報告するとともに、専門家で構成される岡山県環境放射線等測定技術委員会(岡山県)や鳥取県放射能調査専門家会議(鳥取県)において審議され、異常は見られないことが確認された。本資料は鳥取県に報告し、鳥取県放射能調査専門家会議において評価を受けた平成24年度の捨石たい積場周辺の環境監視結果についてまとめたものである。

報告書

人形峠周辺環境の監視測定結果(平成23年度); 岡山県内

伊藤 公雄; 小野 高行; 石森 有; 川崎 悟

JAEA-Review 2013-020, 44 Pages, 2013/10

JAEA-Review-2013-020.pdf:5.03MB

人形峠環境技術センターでは、良好な自然環境の確保等を目的として岡山県・鳥取県と締結した環境保全協定に従って、センターやウラン鉱山跡の捨石たい積場周辺の環境監視測定を実施している。また、回収ウラン転換実用化試験(平成6年$$sim$$平成11年)に伴ってセンター周辺でのプルトニウムについての環境測定も実施している。また、県境鳥取県側において方面掘削土を原料としてレンガを製造する計画に伴い、県境周辺の環境測定を平成18年度より実施している。これらの監視測定結果は、各々の県に定期的に報告するとともに、専門家で構成される岡山県環境放射線等測定技術委員会(岡山県)や鳥取県放射能調査専門家会議(鳥取県)において審議・評価を受けている。本資料は岡山県に報告し、岡山県環境放射線等測定技術委員会において評価を受けた平成23年度の環境監視測定結果についてまとめたものである。

報告書

捨石たい積場周辺環境の監視測定結果,平成23年度; 鳥取県内

伊藤 公雄; 小野 高行; 石森 有; 川崎 悟

JAEA-Review 2013-019, 20 Pages, 2013/07

JAEA-Review-2013-019.pdf:1.93MB

人形峠環境技術センターでは、良好な自然環境の確保等を目的として岡山県・鳥取県と締結した環境保全協定に従って、センターやウラン鉱山跡の捨石たい積場周辺等の環境監視測定を実施している。これらの監視測定結果は、各々の県に定期的に報告するとともに、専門家で構成される岡山県環境放射線等測定技術委員会(岡山県)や鳥取県放射能調査専門家会議(鳥取県)において審議され、異常は見られないことが確認された。本資料は鳥取県に報告し、鳥取県放射能調査専門家会議において評価を受けた平成23年度の捨石たい積場周辺の環境監視結果についてまとめたものである。

48 件中 1件目~20件目を表示