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Identification of hydrogen species on Pt/Al$$_{2}$$O$$_{3}$$ by ${it in situ}$ inelastic neutron scattering and their reactivity with ethylene

山添 誠司*; 山本 旭*; 細川 三郎*; 福田 良一*; 原 賢二*; 中村 充孝; 蒲沢 和也*; 佃 達哉*; 吉田 寿雄*; 田中 庸裕*

Catalysis Science & Technology, 11(1), p.116 - 123, 2021/01

 被引用回数:3 パーセンタイル:81.22(Chemistry, Physical)

Hydrogen (H) species adsorbed on catalyst surfaces are key intermediates in catalytic hydrogenation reactions over supported metal catalysts. However, individual identification of H species on the metal catalysts has not been established to date. Here, we elucidated the H species on Pt/Al$$_{2}$$O$$_{3}$$ by the combination of ${it in situ}$ inelastic neutron scattering (INS) and density functional theory (DFT). Several H species in the presence of H$$_{2}$$ were successfully identified at different sites on the Pt surface and Al$$_{2}$$O$$_{3}$$ support. The ${it in situ}$ INS and FT-IR measurements revealed that the hydride/atop Pt-H, bridged perimeter/terrace Pt-H-Pt, and threefold Pt$$_{3}$$-H are active intermediates in the C$$_{2}$$H$$_{4}$$ hydrogenation reaction, whereas the edge Pt-H-Pt is a rather inert species. In addition, the ${it in situ}$ measurements indicate that the Al$$_{2}$$O$$_{3}$$ itself acts as hydrogen storage material by mediating AlO-H and Al-H-Al species, which serve H species in the C$$_{2}$$H$$_{4}$$ hydrogenation reaction.


The $$f$$-electron state of the heavy fermion superconductor NpPd$$_5$$Al$$_2$$ and the isostructural family

目時 直人; Aczel, A. A.*; 青木 大*; Chi, S.*; Fernandez-Baca, J. A.*; Griveau, J.-C.*; 萩原 雅人*; Hong, T.*; 芳賀 芳範; 池内 和彦*; et al.

JPS Conference Proceedings (Internet), 30, p.011123_1 - 011123_6, 2020/03



Implementation of random sampling for ACE-format cross sections using FRENDY and application to uncertainty reduction

近藤 諒一*; 遠藤 知弘*; 山本 章夫*; 多田 健一

Proceedings of International Conference on Mathematics and Computational Methods applied to Nuclear Science and Engineering (M&C 2019) (CD-ROM), p.1493 - 1502, 2019/00




西森 信行; 永井 良治; 森 道昭; 羽島 良一; 山本 将博*; 本田 洋介*; 宮島 司*; 内山 隆司*; Jin, X.*; 帯名 崇*; et al.

Proceedings of 12th Annual Meeting of Particle Accelerator Society of Japan (インターネット), p.511 - 515, 2015/09



Development of a high-brightness and high-current electron gun for high-flux $$gamma$$-ray generation

西森 信行; 永井 良治; 松葉 俊哉; 羽島 良一; 山本 将博*; 本田 洋介*; 宮島 司*; 内山 隆司*; 栗木 雅夫*

Nuclear Physics and $$gamma$$-ray sources for Nuclear Security and Nonproliferation, p.321 - 326, 2014/12

The quantification of fissile materials such as uranium-235 and plutonium-239 in spent fuel assemblies requires isotope-specific identification. We propose the use of nuclear resonance fluorescence (NRF) to identify the isotopic composition of sample materials nondestructively. The proposed nondestructive isotope identification system requires a high-intensity mono-energetic $$gamma$$-ray beam. Although a mono-energetic $$gamma$$-ray beam can be generated using a conventional laser Compton scattering technique, the generation of a high-intensity $$gamma$$-ray beam requires an electron beam of unprecedentedly high brightness, which can be generated with an advanced accelerator system known as the energy recovery linac (ERL). A technological challenge of the ERL system, which we have addressed, is the development of a high-brightness, high-current electron gun. Our current status of development and operational experience of our gun is presented.


Analysis on effects of transverse electric field in an injector cavity of compact-ERL at KEK

Hwang, J.-G.*; Kim, E.-S.*; 宮島 司*; 本田 洋介*; 原田 健太郎*; 島田 美帆*; 高井 良太*; 久米 達哉*; 長橋 進也*; 帯名 崇*; et al.

Nuclear Instruments and Methods in Physics Research A, 753, p.97 - 104, 2014/07

 被引用回数:7 パーセンタイル:50.1(Instruments & Instrumentation)

For a future synchrotron light source based on a linac, e.g. an X-ray free electron laser and an energy recovery linac (ERL), an injector is a key component to generate a high brightness electron beam. For the acceleration and transportation of the electron beam in the injector, the adjustment of beam orbit inside the cavity is important to avoid the deterioration of the beam quality due to the transverse electric field of it, which causes the transverse emittance growth. To adjust the beam orbit, an investigation of the electromagnetic center of the cavity is required in the beam operation. This paper shows a new method for measuring the electromagnetic center of the cavity, and describes an analytical model of emittance growth due to a combination of transverse electric field and orbit offset. The validation of the method was confirmed by the emittance measurement in the compact ERL (cERL) injector at KEK.



西森 信行; 永井 良治; 松葉 俊哉; 羽島 良一; 山本 将博*; 宮島 司*; 本田 洋介*; 内山 隆司*; 飯島 北斗*; 栗木 雅夫*; et al.

Proceedings of 10th Annual Meeting of Particle Accelerator Society of Japan (インターネット), p.174 - 178, 2014/06



Experimental investigation of an optimum configuration for a high-voltage photoemission gun for operation at $$geq$$ 500 kV

西森 信行; 永井 良治; 松葉 俊哉; 羽島 良一; 山本 将博*; 本田 洋介*; 宮島 司*; 飯島 北斗*; 栗木 雅夫*; 桑原 真人*

Physical Review Special Topics; Accelerators and Beams, 17(5), p.053401_1 - 053401_17, 2014/05

 被引用回数:18 パーセンタイル:78.97(Physics, Nuclear)

We have demonstrated generation of a 500-keV electron beam from a high DC voltage photoemission gun for an energy recovery linac light source. This demonstration was achieved by addressing two discharge problems that lead to vacuum breakdown of the DC gun. One is field emission generated from a central stem electrode. The other is microdischarge at an anode electrode or a vacuum chamber, which is triggered by microparticle transfer or field emission from a cathode electrode. An experimental investigation has revealed that larger acceleration gap optimized to mainly reduce surface electric field of anode electrode results in suppression of the microdischarge events which accompany gas desorption. It has also been found that non evaporable getter pumps placed around the acceleration gap greatly help suppress those microdischarge events. The applied voltage as a function of the total gas desorption is shown to be a good measure to find the optimum DC gun configuration.


超深地層研究所計画 年度報告書(2012年度)

濱 克宏; 見掛 信一郎; 西尾 和久; 松岡 稔幸; 石橋 正祐紀; 笹尾 英嗣; 引間 亮一*; 丹野 剛男*; 真田 祐幸; 尾上 博則; et al.

JAEA-Review 2013-050, 114 Pages, 2014/02




超深地層研究所計画 年度報告書(2011年度)

國丸 貴紀; 見掛 信一郎; 西尾 和久; 鶴田 忠彦; 松岡 稔幸; 石橋 正祐紀; 笹尾 英嗣; 引間 亮一; 丹野 剛男; 真田 祐幸; et al.

JAEA-Review 2013-018, 169 Pages, 2013/09


日本原子力研究開発機構東濃地科学センターでは、「地層処分技術に関する研究開発」のうち深地層の科学的研究(地層科学研究)の一環として、結晶質岩(花崗岩)を対象とした超深地層研究所計画を進めている。本計画は、「第1段階; 地表からの調査予測研究段階」、「第2段階; 研究坑道の掘削を伴う研究段階」、「第3段階; 研究坑道を利用した研究段階」の3段階からなり、2011年度は、第2段階及び第3段階の調査研究を進めた。本報告書は、2010年度に改訂した「超深地層研究所地層科学研究基本計画」に基づいた、超深地層研究所計画の第2段階及び第3段階の調査研究のうち2011年度に実施した(1)調査研究、(2)施設建設、(3)共同研究等の成果を取りまとめたものである。


Progress in a photocathode DC gun at the compact ERL

西森 信行; 永井 良治; 松葉 俊哉; 羽島 良一; 山本 将博*; 本田 洋介*; 宮島 司*; 飯島 北斗*; 栗木 雅夫*; 桑原 真人*

Proceedings of 35th International Free-Electron Laser Conference (FEL 2013) (Internet), p.184 - 188, 2013/08

Photocathode DC gun to produce a train of electron bunch at high-average current and small emittance is a key component of advanced accelerators for high-power beams. However, DC guns operated at a voltage above 350 kV have suffered from field emitted electrons from a support rod since the development of Lasertron in 1980's. This critical issue has been resolved by a novel configuration, segmented insulator and guard rings, adopted in a DC gun at JAEA and stable application of high voltage at 550 kV has been demonstrated. The gun has been installed at the Compact ERL at KEK and ready for the beam generation. Similar type of DC guns are under development at KEK, Cornell, JLAB and IHEP. In this talk, we present progress in photocathode DC gun for high voltage and small emittance.



西森 信行; 永井 良治; 松葉 俊哉; 羽島 良一; 山本 将博*; 宮島 司*; 本田 洋介*; 飯島 北斗*; 栗木 雅夫*; 桑原 真人*; et al.

Proceedings of 9th Annual Meeting of Particle Accelerator Society of Japan (インターネット), p.255 - 259, 2013/08



Generation of a 500-keV electron beam from a high voltage photoemission gun

西森 信行; 永井 良治; 松葉 俊哉; 羽島 良一; 山本 将博*; 宮島 司*; 本田 洋介*; 飯島 北斗*; 栗木 雅夫*; 桑原 真人*

Applied Physics Letters, 102(23), p.234103_1 - 234103_4, 2013/06

 被引用回数:15 パーセンタイル:59.37(Physics, Applied)

High-brightness and high-current electron guns for the future light sources such as energy recovery linac light sources and high repetition rate X-ray free electron lasers require exit beam energy of 500 keV or more to reduce space charge induced emittance growth in a drift space from the gun exit to the following superconducting accelerator entrance. At Japan Atomic Energy Agency, we have developed a DC photoemission gun employing a segmented insulator to mitigate the field emission problem, that is a major obstacle for the DC gun from being operated at 500 kV or more. Recent results of generating 500 keV electron beam with current up to 1.8 mA is presented.


Magnetic Compton scattering studies of magneto-dielectric Ba(Co$$_{0.85}$$Mn$$_{0.15}$$)O$$_{3-delta}$$

篠田 遼一*; 伊藤 真義*; 櫻井 吉晴*; 山本 博之; 平尾 法恵; 馬場 祐治; 岩瀬 彰宏*; 松井 利之*

Journal of Applied Physics, 113(17), p.17E307_1 - 17E307_3, 2013/05

 被引用回数:8 パーセンタイル:38.93(Physics, Applied)



Beam generation from a 500 kV DC photoemission electron gun

西森 信行; 永井 良治; 松葉 俊哉; 羽島 良一; 山本 将博*; 本田 洋介*; 宮島 司*; 飯島 北斗*; 栗木 雅夫*; 桑原 真人*

Proceedings of 4th International Particle Accelerator Conference (IPAC '13) (Internet), p.321 - 323, 2013/05

The next generation light sources such as energy recovery linac (ERL) light sources and X-ray FEL oscillator requires high brightness electron gun with megahertz repetition rate. We have developed a DC photoemission electron gun at JAEA for the Japanese ERL light source project. This DC gun employs a segmented insulator with guard rings to protect the insulator from field emission generated from central stem electrode. We have successfully applied 500 kV on the ceramics with a cathode electrode in place and generated beam from the 500 kV DC photoemission gun in October 2012. Details of the beam generation test at 440 kV as well as 500 kV are presented.


超深地層研究所計画 年度計画書(2012年度)

國丸 貴紀; 見掛 信一郎; 西尾 和久; 鶴田 忠彦; 松岡 稔幸; 石橋 正祐紀; 窪島 光志; 竹内 竜史; 水野 崇; 佐藤 稔紀; et al.

JAEA-Review 2012-028, 31 Pages, 2012/08


日本原子力研究開発機構東濃地科学センターでは、地層処分技術に関する研究開発のうち深地層の科学的研究(地層科学研究)の一環として、結晶質岩(花崗岩)を対象とした超深地層研究所計画を進めている。本計画は、「第1段階; 地表からの調査予測研究段階」、「第2段階; 研究坑道の掘削を伴う研究段階」、「第3段階; 研究坑道を利用した研究段階」の3段階からなる。2012年度は、第2段階及び第3段階の調査研究を進めていく。本計画書は、2010年に改訂した「超深地層研究所地層科学研究基本計画」に基づいた2012年度の超深地層研究所計画の調査研究計画,施設建設計画,共同研究計画などを示したものである。


Development of a photoemission DC Gun at JAEA

西森 信行; 永井 良治; 松葉 俊哉; 羽島 良一; 山本 将博*; 本田 洋介*; 宮島 司*; 飯島 北斗*; 栗木 雅夫*; 桑原 真人*; et al.

Proceedings of 34th International Free Electron Laser Conference (FEL 2012) (Internet), p.161 - 164, 2012/08

The next generation light source such as X-ray FEL oscillator requires high brightness electron gun with megahertz repetition rate. We have developed a photoemission DC gun at JAEA. By employing a segmented insulator with rings which guard the ceramics from field emission, we successfully applied 500-kV on the ceramics with a center stem electrode for eight hours without any discharge in 2009. This high voltage testing was performed with a simple configuration without NEG pumps and electrodes. In 2011 we reached 526-kV with NEG pumps and electrodes, before suffering another field emission problem from the cathode electrode. The problem may be attributed to small dust inside our gun chamber. We found wiping the cathode electrode with a lint free tissue could remove the field emission site effectively. Noble gas conditioning is also planned to remove the emission site without air exposure of the gun chamber.


超深地層研究所計画 年度報告書(2010年度)

國丸 貴紀; 見掛 信一郎; 西尾 和久; 鶴田 忠彦; 松岡 稔幸; 石橋 正祐紀; 上野 孝志; 徳安 真吾; 大丸 修二; 竹内 竜史; et al.

JAEA-Review 2012-020, 178 Pages, 2012/06


日本原子力研究開発機構東濃地科学センターでは、「地層処分技術に関する研究開発」のうち深地層の科学的研究(地層科学研究)の一環として、結晶質岩(花崗岩)を対象とした超深地層研究所計画を進めている。本計画は、「第1段階; 地表からの調査予測研究段階」、「第2段階; 研究坑道の掘削を伴う研究段階」、「第3段階; 研究坑道を利用した研究段階」の3段階からなり、2010年度は、第2段階である「研究坑道の掘削を伴う研究段階」を進めるとともに、第3段階(研究坑道を利用した研究段階)の調査研究を開始した。本報告書は、2002年2月に改訂した「超深地層研究所地層科学研究基本計画」に基づき、超深地層研究所計画の第2段階「研究坑道の掘削を伴う研究段階」及び第3段階(研究坑道を利用した研究段階)における2010年度に実施した(1)調査研究、(2)施設建設、(3)共同研究等の成果を取りまとめたものである。



西森 信行; 永井 良治; 羽島 良一; 山本 将博*; 宮島 司*; 本田 洋介*; 飯島 北斗*; 栗木 雅夫*; 桑原 真人*; 奥見 正治*; et al.

Proceedings of 8th Annual Meeting of Particle Accelerator Society of Japan (インターネット), p.20 - 23, 2011/08



Development of a 500-kV photocathode DC gun for ERLs

西森 信行; 永井 良治; 山本 将博*; 本田 洋介*; 宮島 司*; 飯島 北斗*; 栗木 雅夫*; 桑原 真人*; 奥見 正治*; 中西 彊*; et al.

Journal of Physics; Conference Series, 298, p.012005_1 - 012005_6, 2011/06

An electron gun capable of delivering high current and high brightness electron beam is indispensable for ERL light sources. A high voltage photocathode DC gun is a promising gun for such new light sources. It is however difficult to apply DC high voltage on a ceramic insulator with a rod supporting cathode electrode because of field emission from the rod. In order to mitigate the problem, we have employed a segmented insulator with rings which guard the ceramics from the field emission. We have recently succeeded in applying 500-kV on the ceramics for eight hours without any discharge. Our recent development will be presented at the workshop.

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