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粒界制御技術を適用したニッケル基合金PE16の高温引張強度特性評価

High-temperature tensile properties of the grain boundary engineered NIMONIC PE16

関尾 佳弘; 山下 真一郎; 坂口 紀史*; 柴山 環樹*; 渡辺 精一*; 鴇田 駿*; 藤井 啓道*; 佐藤 裕*; 粉川 博之*

Sekio, Yoshihiro; Yamashita, Shinichiro; Sakaguchi, Norihito*; Shibayama, Tamaki*; Watanabe, Seiichi*; Tokita, Shun*; Fujii, Hiromichi*; Sato, Yutaka*; Kokawa, Hiroyuki*

高温安定性が期待されるニッケル基合金の高性能化を目的に、高温・高照射線量に曝される際に問題となる粒界脆化による延性低下が「粒界制御技術」の適用で抑制可能であることを実証する研究の一環として、粒界制御型PE16を試作し、本技術適用による高温引張強度特性(非照射下)への影響を調査した。その結果、粒界制御型PE16とPE16標準材の降伏応力の温度依存性は同様の傾向を示すものの、粒界制御型PE16の降伏応力はPE16標準材と比べて低下し、一様伸びはわずかに増加した。これは本技術熱処理工程に伴う結晶粒粗大化に起因した強度変化であると推察され、結晶粒径を同程度に調整できた場合、粒界制御型PE16の強度特性はPE16標準材と同程度以上に改善されるものと考えられ、本技術適用により良好な高温強度特性を維持しつつ、耐粒界割れ特性の改善が可能となる見通しが得られた。

In order to improve ductility loss by helium embrittlement (or grain boundary embrittlement) induced under high temperature and neutron irradiation dose in nickel alloys which are expected to have high-temperature phase stability under non-irradiation, the grain boundary engineering was applied for NIMONIC PE16 to enhance the grain boundary strength. And, its high temperature tensile properties under non-irradiation were investigated as the first approach. As a result, the temperature dependence of the yield stress in the grain boundary engineered (GBE) PE16 was similar to that in NIMINIC PE16, but the yield stress was slightly lower and the uniform elongation was slightly higher at each temperature in GBE PE16 comparing to NIMINIC PE16. This would be caused by grain coarsening due to some heat treatments. If the gain size of GBE PE16 is optimized, tensile properties of GBE PE16 would be the same or more than that of NIMONIC PE16.

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