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Rechargeable batteries based on stable redox reactions of disulfide included in a metal-organic framework as ligands

清水 剛志*; Wang, H.*; 谷藤 尚貴*; 松村 大樹; 吉村 真史*; 中西 康次*; 太田 俊明*; 吉川 浩史*

Chemistry Letters, 47(5), p.678 - 681, 2018/05

 被引用回数:1 パーセンタイル:61(Chemistry, Multidisciplinary)

Disulfide, which is a sub-group of organosulfides, has been studied as a promising cathode active material. Herein, to improve battery performance, we inserted disulfide into Cu-based metal organic framework (MOF) as a ligand. As a result, the disulfide inserted MOF exhibited a high capacity based on dual redox reactions of Cu ions and disulfide ligands, and a stable cycle performance. The S $$K$$-edge X-ray absorption fine structure analyses revealed a reversible cleavage and formation of S-S bond in the MOF during discharge and charge process.


Comprehensive seismic evaluation of HTTR against the 2011 off the Pacific coast of Tohoku Earthquake

小野 正人; 飯垣 和彦; 澤畑 洋明; 島崎 洋祐; 清水 厚志; 猪井 宏幸; 近藤 俊成; 小嶋 慶大; 高田 昌二; 沢 和弘

Journal of Nuclear Engineering and Radiation Science, 4(2), p.020906_1 - 020906_8, 2018/04

2011年3月11日、地震の規模を示すマグニチュード9.0の東北地方太平洋沖地震が発生した。地震発生時、HTTRは定期点検及び機器の保守管理のため停止していた。HTTRで観測された最大加速度は設計基準地震を超えていたため、総合的な健全性評価を実施した。総合的な健全性評価の考えは2つに分けられる。1つは機器の目視点検であり、1つは観測波を用いた耐震解析である。運転に関わる全ての機器は目視点検を実施した。設備の健全性は点検結果や解析結果により確認した。機器の耐震解析や目視点検の結果、損傷や機能低下は無く、原子炉の運転に関わる問題は無かった。HTTRの健全性は2011年, 2013年, 2015年のコールド状態の運転によっても裏付けられた。さらに、2015年に中性子源を交換するために3つの制御棒案内ブロックと6つの可動反射体ブロックを原子炉から取り出したとき、制御棒案内ブロックの健全性を目視により確認した。


In-beam $$gamma$$-ray spectroscopy of $$^{35}$$Mg via knockout reactions at intermediate energies

籾山 悟至*; Doornenbal, P.*; Scheit, H.*; 武内 聡*; 新倉 潤*; 青井 考*; Li, K.*; 松下 昌史*; Steppenbeck, D.*; Wang, H.*; et al.

Physical Review C, 96(3), p.034328_1 - 034328_8, 2017/09

 被引用回数:2 パーセンタイル:72.32(Physics, Nuclear)

理化学研究所の不安定核実験施設RIBFにて、中性子過剰核$$^{35}$$Mgの励起状態を$$^{36}$$Mgおよび$$^{37}$$Alからのノックアウト反応によって生成し、そこからの脱励起$$gamma$$線を観測した。$$^{35}$$Mgは中性子数20魔法数が消滅するとされる「逆転の島」と呼ばれる領域に含まれると考えられており、また、奇核であることから、一粒子状態と集団的状態が結合した興味深い核構造が出現すると期待されている。この実験によって、206keV, 443keV, 616keV, 670keVの4本の$$gamma$$線を観測し、これらを全て基底状態へ脱励起する$$gamma$$線であると仮定して励起準位を構成した。この準位構造、ノックアウト反応の断面積、移行運動量分布を殻模型計算および反対称化分子動力学計算と比較した。二つの計算は、基底状態近傍の高い準位密度などいくつかの特徴的な核構造を再現することに成功し、$$^{35}$$Mgは「逆転の島」に含まれるという描像と無矛盾であることがわかった。


Microscopic analyses of complexes formed in adsorbent for Mo and Zr separation chromatography

安倍 諒治*; 名越 航平*; 新井 剛*; 渡部 創; 佐野 雄一; 松浦 治明*; 高木 秀彰*; 清水 伸隆*; 江夏 昌志*; 佐藤 隆博*

Nuclear Instruments and Methods in Physics Research B, 404, p.173 - 178, 2017/08

 パーセンタイル:100(Instruments & Instrumentation)

Molybdenum and zirconium obstruct the efficient recovery of minor actinides (MA(III): Am(III) and Cm(III)) by extraction chromatography; hence, the removal of these elements prior to MA(III) recovery is desirable. The use of an adsorbent impregnated with bis(2-ethylhexyl) hydrogen phosphate (HDEHP) for Mo and Zr decontamination was evaluated in this report. The adsorption/elution and column separation experiments showed that Mo and Zr in the simulated HLLW were selectively adsorbed on the particles, and that Mo was eluted by H$$_{2}$$O$$_{2}$$. EXAFS analysis and SAXS patterns of the adsorbent containing Zr revealed that the Zr-HDEHP complex had a crystal-like periodic structure similar to the structure of the precipitate produced in the solvent extraction system. Micro-PIXE analysis revealed that distribution of the residual Zr on the adsorbent was uniform.



中野 政尚; 藤田 博喜; 河野 恭彦; 永岡 美佳; 井上 和美; 吉井 秀樹*; 大谷 和義*; 檜山 佳典*; 菊地 政昭*; 坂内 信行*; et al.

JAEA-Review 2017-001, 115 Pages, 2017/03





平野 史生; 大谷 芳輝*; 京川 裕之*; 三原 守弘; 清水 浩之*; 本田 明

日本原子力学会和文論文誌, 15(2), p.97 - 114, 2016/06



22A beam production of the uniform negative ions in the JT-60 negative ion source

吉田 雅史; 花田 磨砂也; 小島 有志; 柏木 美恵子; Grisham, L. R.*; 畑山 明聖*; 柴田 崇統*; 山本 崇史*; 秋野 昇; 遠藤 安栄; et al.

Fusion Engineering and Design, 96-97, p.616 - 619, 2015/10

 被引用回数:7 パーセンタイル:28.02(Nuclear Science & Technology)



Analysis of tungsten transport in JT-60U plasmas

清水 友介*; 藤田 隆明*; 有本 英樹*; 仲野 友英; 星野 一生; 林 伸彦

Plasma and Fusion Research (Internet), 10(Sp.2), p.3403062_1 - 3403062_4, 2015/07

In JT-60U, it has been observed that accumulation of tungsten is enhanced with increasing the toroidal rotation in the opposite direction (CTR-rotation) to the plasma current in H-mode plasmas. Two models for convective transport, pinch due to the toroidal rotation (PHZ pinch) and the radial electric field (Er pinch) were proposed. We introduce these two pinch models into integrated transport code TOTAL, and study dependence of the tungsten accumulation on the toroidal rotation. In the high toroidal rotation velocity, we obtained the tungsten accumulation four times as large as in the low one. The model reproduces the trend observed in the experiment.


Advance in integrated modelling towards prediction and control of JT-60SA plasmas

林 伸彦; 本多 充; 白石 淳也; 宮田 良明; 若月 琢馬; 星野 一生; 藤間 光徳; 鈴木 隆博; 浦野 創; 清水 勝宏; et al.

Europhysics Conference Abstracts (Internet), 39E, p.P5.145_1 - P5.145_4, 2015/06

Towards prediction and control of JT-60SA plasmas, we are developing codes/models which can describe physics/engineering factors, and integrating them to one code TOPICS. Physics modelling: Coupling with MINERVA/RWMaC code showed that MHD equilibrium variation by centrifugal force largely affects RWM stability and the toroidal rotation shear stabilizes RWM. Coupling with OFMC code for NB torques, 3D MHD equilibrium code VMEC and drift-kinetic code FORTEC-3D for NTV torque, and toroidal momentum boundary model, predicted the core rotation of $$sim$$2% of Alfv$'e$n speed for a ITER hydrogen L-mode plasma. Coupling with core impurity transport code IMPACT showed the accumulation of Ar seeded to reduce the divertor heat load is so mild that plasma performance can be recovered by additional heating in JT-60SA steady-state (SS) scenario. Simulations coupled with MARG2D code showed that plasma current can be ramped-up to reach $$beta_N ge$$3 with MHD modes stabilized by ideal wall and with no additional flux consumption of central solenoid in JT-60SA. Engineering modelling: Coupling with integrated real-time controller showed that simultaneous control of $$beta_N$$ and $$V_{loop}$$ is possible at $$beta_N ge$$4 in JT-60SA SS scenarios. MHD equilibrium control simulator MECS demonstrated equilibrium control during heating phase and collapse induced events within power supply capability of PF coils in JT-60SA.


Low-lying structure of $$^{50}$$Ar and the $$N$$=32 subshell closure

Steppenbeck, D.*; 武内 聡*; 青井 考*; Doornenbal, P.*; 松下 昌史*; Wang, H.*; 宇都野 穣; 馬場 秀忠*; 郷 慎太郎*; Lee, J.*; et al.

Physical Review Letters, 114(25), p.252501_1 - 252501_6, 2015/06

 被引用回数:18 パーセンタイル:15.72(Physics, Multidisciplinary)

理化学研究所の不安定核施設RIBFにて、中性子過剰核$$^{50}$$Arを$$^{54}$$Ca, $$^{55}$$Sc, $$^{56}$$Tiからの核破砕反応によって生成し、その脱励起$$gamma$$線を初めて観測した。最も強度の強い$$gamma$$線エネルギーから、$$^{50}$$Arの第一励起$$2^+$$状態の励起エネルギーが1178(18)keVであることがわかった。この実験結果および周辺核の$$2^+$$状態の励起エネルギーを大規模殻模型計算と比較した結果、$$^{50}$$Arでは中性子数32のサブシェルギャップが$$^{52}$$Caと同じくらい大きくなることによってその第一励起エネルギーが$$^{48}$$Arよりも高くなることがわかった。また、殻模型計算によって、中性子数34のサブシェルギャップがCaからArにかけて増大することを予言し、その影響は今後行われるであろう$$^{52}$$Arの励起状態の測定で確かめ得ることを示した。


Operation and maintenance experience from the HTTR database

清水 厚志; 古澤 孝之; 本間 史隆; 猪井 宏幸; 梅田 政幸; 近藤 雅明; 磯崎 実; 藤本 望; 伊与久 達夫

Journal of Nuclear Science and Technology, 51(11-12), p.1444 - 1451, 2014/11

 被引用回数:1 パーセンタイル:85.45(Nuclear Science & Technology)



Development of operation and maintenance technology for HTGRs by using HTTR (High Temperature engineering Test Reactor)

清水 厚志; 川本 大樹; 栃尾 大輔; 齋藤 賢司; 澤畑 洋明; 本間 史隆; 古澤 孝之; 七種 明雄; 高田 昌二; 篠崎 正幸

Nuclear Engineering and Design, 271, p.499 - 504, 2014/05

 被引用回数:3 パーセンタイル:61.51(Nuclear Science & Technology)



Simultaneous saccharification and fermentation from ionic liquid-pretreated biomass using ionic liquid-tolerant yeast mutant

仁宮 一章*; 表 小百合*; 佐藤 勝也; 鳴海 一成*; 清水 宣明*

JAEA-Review 2013-059, JAEA Takasaki Annual Report 2012, P. 115, 2014/03

In simultaneous saccharification and fermentation of biomass, pretreatment using ionic liquid has received a lot of attention in recent years. A enormous quantities of wastewater become a problem in washing from ionic liquid-pretreated biomass because ionic liquid is highly poisonous. In this study, simultaneous saccharification and fermentation from ionic liquid-pretreated biomass was carried out using ionic liquid-tolerant yeast that was obtained from the mutant population prepared by irradiation with carbon ion beams (220 MeV $$^{12}$$C$$^{5+}$$, 100 Gy). By using the ionic liquid-tolerant yeast strain, we could simplify the washing procedure of ionic liquid-pretreated biomass prior to the simultaneous saccharification and fermentation.



山田 克典; 藤井 克年; 神田 浩志; 東 大輔; 小林 稔明; 中川 雅博; 深見 智代; 吉田 圭佑; 上野 有美; 中嶌 純也; et al.

JAEA-Review 2013-033, 51 Pages, 2013/12




Clinical significance of L-type amino acid transporter 1 expression as a prognostic marker and potential of new targeting therapy in biliary tract cancer

解良 恭一*; 須納瀬 豊*; 大島 康宏; 石岡 典子; 荒川 和久*; 小川 哲史*; 砂長 則明*; 清水 公裕*; 富永 英之*; 織内 昇*; et al.

BMC Cancer, 13, p.482_1 - 482_12, 2013/10

 被引用回数:31 パーセンタイル:18.23(Oncology)

The expression of L-type amino acid transporter 1 (LAT1) has been described to play essential roles in tumor growth and survival. However, it remains unclear about the clinicopathological significance of LAT1 expression in biliary tract cancer. This study was conducted to determine clinical significance of LAT1 expression and investigate whether LAT1 could be a new therapeutic target for biliary tract cancer. A total of 139 consecutive patients with resected pathologic stage I-IV biliary tract adenocarcinoma were retrospectively reviewed. Tumor sections were stained by immunohistochemistry for LAT1, CD98, Ki-67, microvessel density determined by CD34 and p53. Further, anti-tumor activity of LAT inhibitor, 2-aminobicyclo-(2,2,1)-heptane-2-carboxylic acid (BCH) was investigated using cholangiocarcinoma cell line. The expression of LAT1 was recognized in 64% of total patients, and closely correlated with CD98 expression, lymphatic metastases, cell proliferation and angiogenesis, and was a significant indicator for predicting poor outcome after surgery. Experiments showed that BCH significantly suppressed the tumor growth and BCH yielded an additive therapeutic efficacy to gemcitabine and 5-FU. A cooperative high expression of LAT1 with CD98 is a promising pathological marker to predict the outcome in biliary tract adenocarcinoma. Inhibition of LAT1 may be an effective targeted therapy for this distressing disease.


The Possible interplanetary transfer of microbes; Assessing the viability of ${it Deinococcus}$ spp. under the ISS environmental conditions for performing exposure experiments of microbes in the Tanpopo mission

河口 優子*; Yang, Y.*; 川尻 成俊*; 白石 啓祐*; 高須 昌子*; 鳴海 一成*; 佐藤 勝也; 橋本 博文*; 中川 和道*; 谷川 能章*; et al.

Origins of Life and Evolution of Biospheres, 43(4-5), p.411 - 428, 2013/10

 被引用回数:15 パーセンタイル:27.08(Biology)

In the Tanpopo mission, we have proposed to carry out experiments on capture and space exposure of microbes at the Exposure Facility of the Japanese Experimental Module of the International Space Station (ISS). Microbial candidates for the exposure experiments in space include ${it Deinococcus}$ spp. We have examined the survivability of ${it Deinococcus}$ spp. under the environmental conditions in ISS in orbit. A One-year dose of heavy-ion beam irradiation did not affect the viability of ${it Deinococcus}$ spp. within the detection limit. Exposure of various thicknesses of deinococcal cell aggregates to UV radiation revealed that a few hundred micrometer thick aggregate of deinococcal cells would be able to withstand the solar UV radiation on ISS for 1 year. We concluded that aggregated deinococcal cells will survive the yearlong exposure experiments. We propose that microbial cells can aggregate as an ark for the interplanetary transfer of microbes, and we named it "massapanspermia".


Optimization of JT-60SA plasma operational scenario with capabilities of installed actuators

井手 俊介; 相羽 信行; Bolzonella, T.*; Challis, C. D.*; 藤田 隆明; Giruzzi, G.*; Joffrin, E.*; 濱松 清隆; 林 伸彦; 本多 充; et al.

Proceedings of 24th IAEA Fusion Energy Conference (FEC 2012) (CD-ROM), 8 Pages, 2013/03

Assessment of capabilities in controlling key plasma parameters to access and sustain a high normalized pressure plasma in JT-60SA has been carried out using predictive simulations with emphasis on controllability with actuators, including not only heating and current drive but also fueling and pumping system. It is confirmed that the safety factor profile, which is believed to play an important role for confinement improvement, can be prepared appropriately at the plasma current ramp-up phase in a wide extent within capability of the installed ECRF system. At the flat-top of a high pressure and high bootstrap current plasma, it is also confirmed that the installed NB system can modify the safety factor profile and the confinement property within the planned capabilities. It is confirmed that impurity seeding in the SOL and the divertor region can maintain the heat flux within the divertor heat tolerance keeping the separatrix density level acceptable.



仁宮 一章*; 野村 知世*; 佐藤 勝也; 鳴海 一成; 清水 宣明*

JAEA-Review 2012-046, JAEA Takasaki Annual Report 2011, P. 108, 2013/01

By using immunocytochemistry and fluorescence-activated cell sorter (FACS), yeast population highly expressing cellulase on the cell surface was enriched from the mutant population prepared by irradiation with carbon ion beams (220 MeV $$^{12}$$C$$^{5+}$$, 100 Gy). Enzymatic activity of the enriched clones was quantified in vitro by a conventional biochemical method. Repeated FACS after irradiation with carbon ion beams was effective for selecting yeast population of interest.


Development of operation and maintenance technology of HTTR (High Temperature engineering Test Reactor)

清水 厚志; 川本 大樹; 栃尾 大輔; 齋藤 賢司; 澤畑 洋明; 本間 史隆; 古澤 孝之; 七種 明雄; 篠崎 正幸

Proceedings of 6th International Topical Meeting on High Temperature Reactor Technology (HTR 2012) (USB Flash Drive), 8 Pages, 2012/10



A New method for evaluating the specificity of indirect readout in protein-DNA recognition

山崎 智*; 寺田 透*; 河野 秀俊; 清水 謙多郎*; 皿井 明倫*

Nucleic Acids Research, 40(17), p.e129_1 - e129_7, 2012/09

 被引用回数:14 パーセンタイル:50.45(Biochemistry & Molecular Biology)

Proteins recognize a specific DNA sequence not only through direct contact (direct readout) with base pairs but also through sequence-dependent conformation and/or flexibility of DNA (indirect readout). However, it is difficult to assess the contribution of indirect readout to the sequence specificity. What is needed is a straightforward method for quantifying its contributions to specificity. Using Bayesian statistics, we derived the probability of a particular sequence for a given DNA structure from the trajectories of molecular dynamics (MD) simulations of DNAs containing all possible tetramer sequences. Then, we quantified the specificity of indirect readout based on the information entropy associated with the probability. We tested this method with known structures of protein-DNA complexes. This method enabled us to correctly predict those regions where experiments suggested the involvement of indirect readout. The results also indicated new regions where the indirect readout mechanism makes major contributions to the recognition. The present method can be used to estimate the contribution of indirect readout without approximations to the distributions in the conformational ensembles of DNA, and would serve as a powerful tool to study the mechanism of protein-DNA recognition.

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